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2-Amino-5-chlorobenzonitrile

Product Name
2-Amino-5-chlorobenzonitrile
CAS No.
5922-60-1
Chemical Name
2-Amino-5-chlorobenzonitrile
Synonyms
ACBN;TIMTEC-BB SBB004050;4-Chloro-2-cyanoaniline;5-CHLOROANTHRANILONITRILE;5-Chloro-2-aminobenzonitrile;2-AMINO-5-CHLOROBENZONITRILE;2-amino-5-chloro-benzonitril;AMINO(2-) 5-CHLORO-BENZONITRILE;1-CYANO-2-AMINO-5-CHLOROBENZENE;Benzonitrile, 2-amino-5-chloro-
CBNumber
CB2212100
Molecular Formula
C7H5ClN2
Formula Weight
152.58
MOL File
5922-60-1.mol
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2-Amino-5-chlorobenzonitrile Property

Melting point:
96-99 °C (lit.)
Boiling point:
132-135 °C/0.5 mmHg (lit.)
Density 
1.2763 (rough estimate)
refractive index 
1.5500 (estimate)
Flash point:
>230 °F
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
Chloroform (Slightly), DMSO (Slightly)
form 
Crystalline Needles
pka
1.18±0.10(Predicted)
color 
White to light beige
CAS DataBase Reference
5922-60-1(CAS DataBase Reference)
EPA Substance Registry System
Benzonitrile, 2-amino-5-chloro- (5922-60-1)
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Safety

Hazard Codes 
Xn,Xi
Risk Statements 
20/21/22-36/37/38
Safety Statements 
26-36-36/37/39
RIDADR 
3276
WGK Germany 
3
Hazard Note 
Irritant
TSCA 
Yes
HazardClass 
6.1
PackingGroup 
III
HS Code 
29269090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
174335
Product name
2-Amino-5-chlorobenzonitrile
Purity
98%
Packaging
5g
Price
$63.3
Updated
2024/03/01
TCI Chemical
Product number
A1572
Product name
2-Amino-5-chlorobenzonitrile
Purity
>98.0%(GC)
Packaging
5g
Price
$52
Updated
2024/03/01
TCI Chemical
Product number
A1572
Product name
2-Amino-5-chlorobenzonitrile
Purity
>98.0%(GC)
Packaging
25g
Price
$190
Updated
2024/03/01
Alfa Aesar
Product number
B22690
Product name
2-Amino-5-chlorobenzonitrile, 97%
Packaging
1g
Price
$19.65
Updated
2024/03/01
Alfa Aesar
Product number
B22690
Product name
2-Amino-5-chlorobenzonitrile, 97%
Packaging
5g
Price
$73.65
Updated
2024/03/01
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2-Amino-5-chlorobenzonitrile Chemical Properties,Usage,Production

Chemical Properties

white to light beige crystalline needles

Uses

2-Amino-5-chlorobenzonitrile was used to build up the 2,2-dioxide-1H-2,1,3-benzothiadiazine ring system.

Preparation

Synthesis of 2-amino-5-chlorobenzonitrile is reported in the literature by two methods. The first method involves synthesis from 2-aminobenzonitrile, N-chlorosuccinimide an d acetonitrile. The second method involves synthesis from 5-chloroisatin-β-oxime and bis(2-ethylhexyl)phthalate. Both the methods are not feasible commercially as far as the cost and availability of raw materials are concerned.

Synthesis Reference(s)

Synthetic Communications, 20, p. 71, 1990 DOI: 10.1080/00397919008054617

General Description

The vibrational spectra of 2-amino-5-chlorobenzonitrile was studied using density functinal theory.

2-Amino-5-chlorobenzonitrile Preparation Products And Raw materials

Raw materials

2-Aminobenzonitrile Acetonitrile N-Chlorosuccinimide Dichloromethane Sodium hydroxide Magnesium sulfate

Preparation Products

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2-Amino-5-chlorobenzonitrile Suppliers

Americas 1 Belgium 2 Canada 1 China 183 Europe 4 Germany 5 India 20 Japan 3 Slovakia 3 South Korea 1 Switzerland 4 The Netherlands 1 Ukraine 1 United Kingdom 23 United States 47 Global 299
Unachem Trading Co., Ltd.
Tel
--
Fax
--
Email
unachem@ktnet.co.kr
Country
South Korea
ProdList
1181
Advantage
30
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View Lastest Price from 2-Amino-5-chlorobenzonitrile manufacturers

Henan Fengda Chemical Co., Ltd
Product
2-Amino-5-chlorobenzonitrile 5922-60-1
Price
US $35.00-1.10/kg
Min. Order
1kg
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-19
Career Henan Chemical Co
Product
2-Amino-5-chlorobenzonitrile 5922-60-1
Price
US $2.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
ask
Release date
2018-12-20

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