2-Amino-5-chlorobenzonitrile

Product Name: 2-Amino-5-chlorobenzonitrile
CAS No.: 5922-60-1
Chemical Name: 2-Amino-5-chlorobenzonitrile
Synonyms: ACBN;TIMTEC-BB SBB004050;4-Chloro-2-cyanoaniline;5-CHLOROANTHRANILONITRILE;5-Chloro-2-aminobenzonitrile;2-AMINO-5-CHLOROBENZONITRILE;2-amino-5-chloro-benzonitril;AMINO(2-) 5-CHLORO-BENZONITRILE;1-CYANO-2-AMINO-5-CHLOROBENZENE;Benzonitrile, 2-amino-5-chloro-
CBNumber: CB2212100
Molecular Formula: C7H5ClN2
Formula Weight: 152.58
MOL File: 5922-60-1.mol

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2-Amino-5-chlorobenzonitrile Property

Melting point:: 96-99 °C (lit.)
Boiling point:: 132-135 °C/0.5 mmHg (lit.)
Density: 1.2763 (rough estimate)
refractive index: 1.5500 (estimate)
Flash point:: >230 °F
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: Chloroform (Slightly), DMSO (Slightly)
form: Crystalline Needles
pka: 1.18±0.10(Predicted)
color: White to light beige
CAS DataBase Reference: 5922-60-1(CAS DataBase Reference)
EPA Substance Registry System: Benzonitrile, 2-amino-5-chloro- (5922-60-1)

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Safety

Hazard Codes: Xn,Xi
Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36-36/37/39
RIDADR: 3276
WGK Germany: 3
Hazard Note: Irritant
TSCA: Yes
HazardClass: 6.1
PackingGroup: III
HS Code: 29269090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 174335
Product name: 2-Amino-5-chlorobenzonitrile
Purity: 98%
Packaging: 5g
Price: $63.3
Updated: 2024/03/01

TCI Chemical

Product number: A1572
Product name: 2-Amino-5-chlorobenzonitrile
Purity: >98.0%(GC)
Packaging: 5g
Price: $52
Updated: 2024/03/01

TCI Chemical

Product number: A1572
Product name: 2-Amino-5-chlorobenzonitrile
Purity: >98.0%(GC)
Packaging: 25g
Price: $190
Updated: 2024/03/01

Alfa Aesar

Product number: B22690
Product name: 2-Amino-5-chlorobenzonitrile, 97%
Packaging: 1g
Price: $19.65
Updated: 2024/03/01

Alfa Aesar

Product number: B22690
Product name: 2-Amino-5-chlorobenzonitrile, 97%
Packaging: 5g
Price: $73.65
Updated: 2024/03/01

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2-Amino-5-chlorobenzonitrile Chemical Properties,Usage,Production

Chemical Properties

white to light beige crystalline needles

Uses

2-Amino-5-chlorobenzonitrile was used to build up the 2,2-dioxide-1H-2,1,3-benzothiadiazine ring system.

Preparation

Synthesis of 2-amino-5-chlorobenzonitrile is reported in the literature by two methods. The first method involves synthesis from 2-aminobenzonitrile, N-chlorosuccinimide an d acetonitrile. The second method involves synthesis from 5-chloroisatin-β-oxime and bis(2-ethylhexyl)phthalate. Both the methods are not feasible commercially as far as the cost and availability of raw materials are concerned.

Synthesis Reference(s)

Synthetic Communications, 20, p. 71, 1990 DOI: 10.1080/00397919008054617

General Description

The vibrational spectra of 2-amino-5-chlorobenzonitrile was studied using density functinal theory.

2-Amino-5-chlorobenzonitrile Preparation Products And Raw materials

Raw materials

2-Aminobenzonitrile Acetonitrile N-Chlorosuccinimide Dichloromethane Sodium hydroxide Magnesium sulfate

Preparation Products

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2-Amino-5-chlorobenzonitrile Suppliers

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View Lastest Price from 2-Amino-5-chlorobenzonitrile manufacturers

Henan Fengda Chemical Co., Ltd

Product: 2-Amino-5-chlorobenzonitrile 5922-60-1
Price: US $35.00-1.10/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-19

Career Henan Chemical Co

Product: 2-Amino-5-chlorobenzonitrile 5922-60-1
Price: US $2.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: ask
Release date: 2018-12-20

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5922-60-1

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