Benzaldehyde, 2-broMo-4-hydroxy

Product Name: Benzaldehyde, 2-broMo-4-hydroxy
CAS No.: 22532-60-1
Chemical Name: Benzaldehyde, 2-broMo-4-hydroxy
Synonyms: 2-BroMo-4-Hydroxy benzaldehyde;Benzaldehyde, 2-broMo-4-hydroxy
CBNumber: CB22631185
Molecular Formula: C7H5BrO2
Formula Weight: 201.02
MOL File: 22532-60-1.mol

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Benzaldehyde, 2-broMo-4-hydroxy Property

Boiling point:: 292.4±20.0 °C(Predicted)
Density: 1.737±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 6.81±0.18(Predicted)
Appearance: Off-white to yellow Solid
InChI: InChI=1S/C7H5BrO2/c8-7-3-6(10)2-1-5(7)4-9/h1-4,10H
InChIKey: OCBOCCOUCDGNKX-UHFFFAOYSA-N
SMILES: C(=O)C1=CC=C(O)C=C1Br

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B997133
Product name: 2-Bromo-4-hydroxybenzaldehyde
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: B997133
Product name: 2-Bromo-4-hydroxybenzaldehyde
Packaging: 500mg
Price: $110
Updated: 2021/12/16

AK Scientific

Product number: Z4448
Product name: 2-Bromo-4-hydroxybenzaldehyde
Packaging: 1g
Price: $91
Updated: 2021/12/16

Matrix Scientific

Product number: 119817
Product name: 2-Bromo-4-hydroxybenzaldehyde
Purity: 95+%
Packaging: 1g
Price: $197
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142526
Product name: 2-Bromo-4-hydroxybenzaldehyde
Packaging: 2g
Price: $264
Updated: 2021/12/16

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Benzaldehyde, 2-broMo-4-hydroxy Chemical Properties,Usage,Production

Synthesis

64-17-5

591-20-8

22532-60-1

The general procedure for the synthesis of 2-bromo-4-hydroxybenzaldehyde from ethanol and m-bromophenol was as follows: 30% aqueous sodium hydroxide solution (160 mL) was mixed with 3-bromophenol (10.04 g, 58 mmol) and heated to 70-75 °C. Subsequently, ethanol (5 mL) was added all at once and chloroform (28 mL, 0.35 mol) was added slowly and dropwise. After maintaining the reaction at 75 °C for 1 hour, the reaction mixture was continued to be stirred at this temperature for 3 hours. Upon completion of the reaction, the mixture was cooled to room temperature and acidified with 10N hydrochloric acid. Most of the by-products were removed by steam distillation. The residue was cooled and the precipitate was separated by filtration. The crude product was purified by silica gel column chromatography using hexane/ethyl acetate (2:1, v/v) as eluent to give 1.75 g of 2-bromo-4-hydroxybenzaldehyde in 15% yield.

References

[1] Patent: WO2011/37731, 2011, A1. Location in patent: Page/Page column 111-112

Benzaldehyde, 2-broMo-4-hydroxy Preparation Products And Raw materials

Raw materials

Preparation Products

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Benzaldehyde, 2-broMo-4-hydroxy Suppliers

China 96 India 1 United Kingdom 2 United States 6 Global 105

Suzhou Laing Biological Technology Co., LTD

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View Lastest Price from Benzaldehyde, 2-broMo-4-hydroxy manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 2-Bromo-4-hydroxybenzaldehyde 22532-60-1
Price: US $3.00-9.00/kg
Min. Order: 1kg
Purity: 99%min
Supply Ability: 50kg
Release date: 2025-07-28

Career Henan Chemical Co

Product: POTASSIUM (4-CYANOPHENYL)TRIFLUOROBORATE 850623-36-8
Price: US $1.00/ASSAYS
Min. Order: 1ASSAYS
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-20

22532-60-1, Benzaldehyde, 2-broMo-4-hydroxyRelated Search:

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Benzaldehyde, 2-broMo-4-hydroxy

2-BroMo-4-Hydroxy benzaldehyde

22532-60-1