ChemicalBook > CAS DataBase List > 5-BROMOPYRIDINE-2-CARBONYL CHLORIDE

5-BROMOPYRIDINE-2-CARBONYL CHLORIDE

Product Name
5-BROMOPYRIDINE-2-CARBONYL CHLORIDE
CAS No.
137178-88-2
Chemical Name
5-BROMOPYRIDINE-2-CARBONYL CHLORIDE
Synonyms
5-Bromopicolinoyl Chloride;5-Bromo-2-(chlorocarbonyl)pyridine;5-BROMOPYRIDINE-2-CARBONYL CHLORIDE;5-Bromo-2-pyridinecarbonyl chloride;2-Pyridinecarbonyl chloride, 5-bromo-;5-BroMo-pyriMidine-2-carbonyl chloride;5-Bromopyridine-2-carbonyl chloride ,97%;5-Bromopyridine-2-carbonyl chloride, tech;5-BroMopyridine-2-carbonyl chloride, tech grade;5-BROMOPYRIDINE-2-CARBONYL CHLORIDE ISO 9001：2015 REACH
CBNumber
CB2480413
Molecular Formula
C6H3BrClNO
Formula Weight
220.45
MOL File
137178-88-2.mol
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5-BROMOPYRIDINE-2-CARBONYL CHLORIDE Property

Boiling point:
250 ºC
Density 
1.760
Flash point:
105 ºC
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
Solid
pka
-1.86±0.10(Predicted)
Sensitive 
Moisture Sensitive
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Safety

HazardClass 
IRRITANT
HazardClass 
8
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
B677998
Product name
5-Bromopyridine-2-carbonylChloride
Packaging
50mg
Price
$60
Updated
2021/12/16
SynQuest Laboratories
Product number
4H16-D-X1
Product name
5-Bromopyridine-2-carbonyl chloride, tech
Purity
tech%
Packaging
1g
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB147626
Product name
5-Bromopyridine-2-carbonylchloride
Packaging
100mg
Price
$55
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB147626
Product name
5-Bromopyridine-2-carbonylchloride
Packaging
250mg
Price
$110
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB147626
Product name
5-Bromopyridine-2-carbonylchloride
Packaging
500mg
Price
$190
Updated
2021/12/16
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5-BROMOPYRIDINE-2-CARBONYL CHLORIDE Chemical Properties,Usage,Production

Chemical Properties

Brown solid

Synthesis

30766-11-1

137178-88-2

General procedure for the synthesis of 5-bromo-pyridine-2-carbonyl chloride from 2-carboxylic acid-5-bromopyridine: To a solution of dichloromethane (80 mL) containing 5-bromo-pyridine-2-carboxylic acid (0.05 mmol), oxalyl chloride (0.24 mmol) and N,N-dimethylformamide (5 drops) were slowly added dropwise at room temperature. The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure to give 5.4 g (100% yield) of 5-bromo-pyridine-2-carbonyl chloride.

References

[1] Patent: CN103130792, 2016, B. Location in patent: Paragraph 0533
[2] Patent: WO2014/164749, 2014, A1. Location in patent: Page/Page column 312
[3] Patent: WO2017/221100, 2017, A1. Location in patent: Paragraph 00262
[4] Tetrahedron, 2005, vol. 61, # 45, p. 10748 - 10756
[5] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 7, p. 2074 - 2079

5-BROMOPYRIDINE-2-CARBONYL CHLORIDE Preparation Products And Raw materials

Raw materials

Toluene 2,5-Dibromopyridine Thionyl chloride n-Butyllithium

Preparation Products

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5-BROMOPYRIDINE-2-CARBONYL CHLORIDE Suppliers

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View Lastest Price from 5-BROMOPYRIDINE-2-CARBONYL CHLORIDE manufacturers

Dideu Industries Group Limited
Product
5-BROMOPYRIDINE-2-CARBONYL CHLORIDE 137178-88-2
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-23
Shaanxi Dideu Medichem Co. Ltd
Product
5-Bromopyridine-2-carbonyl chloride 137178-88-2
Price
US $0.00-0.00/Kg
Min. Order
1KG
Purity
99.0%
Supply Ability
500 MT
Release date
2020-05-12
Career Henan Chemical Co
Product
5-BROMOPYRIDINE-2-CARBONYL CHLORIDE 137178-88-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-03

137178-88-2, 5-BROMOPYRIDINE-2-CARBONYL CHLORIDERelated Search:

Ammonium chloride Choline chloride Benzoyl chloride 2,3,4,5-Tetrafluorobenzoyl chloride Calcium chloride PYRAZOPHOS Methylaminoformyl chloride 5-Bromo-2-methylpyridine Sodium chloride Polyvinyl chloride 1-Hexadecylpyridinium bromide o-Toluoyl chloride CARBONYL SULFIDE Potassium chloride 4-Nitrobenzoyl chloride 5-Bromopyridine-2-carbaldehyde Methanesulfonyl chloride Methylene Chloride

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  • 137178-88-2