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Pindolol

Product Name
Pindolol
CAS No.
13523-86-9
Chemical Name
Pindolol
Synonyms
lb46;LB-46;Visken;Vasken;dl-lb46;Decreten;Pinbetol;Pynastin;PINDOLOL;(+-)-lb46
CBNumber
CB3105373
Molecular Formula
C14H20N2O2
Formula Weight
248.32
MOL File
13523-86-9.mol
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Pindolol Property

Melting point:
167-171 °C(lit.)
Boiling point:
391.39°C (rough estimate)
Density 
1.0606 (rough estimate)
refractive index 
1.5110 (estimate)
storage temp. 
2-8°C
solubility 
0.1 M NaOH: 0.2 mg/mL
form 
powder
pka
pKa 9.26 (Uncertain)
color 
white to off-white
Water Solubility 
33mg/L(22.5 ºC)
Merck 
13,7525
CAS DataBase Reference
13523-86-9(CAS DataBase Reference)
NIST Chemistry Reference
Pindolol(13523-86-9)
EPA Substance Registry System
2-Propanol, 1-(1H-indol-4-yloxy)-3-[(1-methylethyl)amino]- (13523-86-9)
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Safety

Hazard Codes 
Xn
Risk Statements 
22-36/37/38
Safety Statements 
26-36
RIDADR 
3249
WGK Germany 
3
RTECS 
UB6660000
HazardClass 
6.1(b)
PackingGroup 
III
HS Code 
2933995300
Hazardous Substances Data
13523-86-9(Hazardous Substances Data)
Toxicity
LD50 oral in rabbit: 650mg/kg
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
PHR3224
Product name
Pindolol
Purity
pharmaceutical secondary standard, certified reference material
Packaging
500MG
Price
$229
Updated
2024/03/01
Sigma-Aldrich
Product number
P0778
Product name
Pindolol
Purity
≥98% (TLC), powder
Packaging
1g
Price
$132
Updated
2024/03/01
Sigma-Aldrich
Product number
1539701
Product name
Pindolol
Purity
United States Pharmacopeia (USP) Reference Standard
Packaging
200mg
Price
$436
Updated
2024/03/01
Cayman Chemical
Product number
21445
Product name
Pindolol
Purity
≥99%
Packaging
50mg
Price
$37
Updated
2024/03/01
Cayman Chemical
Product number
21445
Product name
Pindolol
Purity
≥99%
Packaging
100mg
Price
$68
Updated
2024/03/01
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Pindolol Chemical Properties,Usage,Production

Chemical Properties

White Solid

Originator

Betadren, Lagap

Uses

Mixed β-adrenergic blocker and serotonin 5HT1A-receptor antagonist. Antihypertensive; antianginal; antiarrhythmic; antiglaucoma.

Uses

Pindolol, like nadolol, is a nonselective β-adrenoblocker. It possesses antianginal, antihypotensive, and antiarrythmic action. It is used for arterial hypertension, angina stress (preventing attacks), supraventricular tachycardia, tachsystolic form of atrial fibrillation, and superventricular extrasystole.

Definition

ChEBI: A member of the class of indols which is the 2-hydroxy-3-(isopropylamino)propyl ether derivative of 1H-indol-4-ol.

Manufacturing Process

4-Hydroxyindole is obtained by debenzylation of 4-benzyloxyindole with hydrogen in the presence of a 5% palladium catalyst on aluminium oxide.
10.0 g of 4-hydroxyindole and subsequently 7.4 ml of epichlorohydrin are added while stirring in an atmosphere of nitrogen to a solution of 2.73 g of sodium hydroxide in 65 ml of water. Stirring is effected at room temperaturefor a further 15 h, the reaction mixture is extracted 4 times with 50 ml of methylene chloride and the combined organic layers which have been dried over magnesium sulfate are evaporated at reduced pressure. So 3-chloro-1(4-indolyloxy)-2-propanol is obtained.
The 3-chloro-1-(4-indolyloxy)-2-propanol is dissolved in 50 ml of toluene and 50 ml of isopropylamine and heated to the boil for 45 h. Evaporation to dryness is effected in a vacuum, the residue is shaken out thrice between ethyl acetate and a 1 N tartaric acid solution and a 5 N sodium hydroxide solution is then added to the combined tartaric acid phases until an alkaline reaction is obtained. The alkaline solution is shaken out thrice with 50 ml of methylene chloride, the extracts are dried over magnesium sulfate and the solvent evaporated in vacuum. The residue is crystallized from ethyl acetate/ether to give the 4-(2-hydroxy-3-isopropylaminopropoxy)indole.

brand name

Visken (Novartis).

Therapeutic Function

Beta-adrenergic blocker

Biological Activity

5-HT 1A/1B ? receptor antagonist, with roughly equal affinity for each subtype. A partial agonist at mouse and human β 3 -adrenoceptors.

Biochem/physiol Actions

β1-adrenoceptor antagonist; putative 5-HT1A serotonin receptor agonist; vasodilator.

Clinical Use

Beta-blocker:
Hypertension
Angina

Drug interactions

Potentially hazardous interactions with other drugs
Anaesthetics: enhanced hypotensive effect.
Analgesics: NSAIDs antagonise hypotensive effect.
Anti-arrhythmics: increased risk of myocardial depression and bradycardia; increased risk of bradycardia, myocardial depression and AV block with amiodarone; increased risk of myocardial depression and bradycardia with flecainide.
Antidepressants: enhanced hypotensive effect with MAOIs.
Antihypertensives; enhanced hypotensive effect; increased risk of withdrawal hypertension with clonidine; increased risk of first dose hypotensive effect with post-synaptic alpha-blockers such as prazosin.
Antimalarials: increased risk of bradycardia with mefloquine.
Antipsychotics: enhanced hypotensive effect with phenothiazines.
Calcium-channel blockers: increased risk of bradycardia and AV block with diltiazem; hypotension and heart failure possible with nifedipine and nisoldipine; asystole, severe hypotension and heart failure with verapamil.
Cytotoxics: possible increased risk of bradycardia with crizotinib.
Diuretics: enhanced hypotensive effect.
Fingolimod: possibly increased risk of bradycardia.
Moxisylyte: possible severe postural hypotension.
Sympathomimetics: severe hypertension with adrenaline and noradrenaline and possibly with dobutamine.

Metabolic pathway

Several metabolites of pindolol formed in vitro are detected after a 24 h incubation of human hepatocytes in both pure culture and co-culture by adding rat liver epithelial cells. The hepatocytes are able to oxidize the isopropyl amine moiety and the pyrrole ring of the indole moiety and conjugate pindolol as sulfates and glucuronides.

Metabolism

Pindolol (Visken) is extensively absorbed from the gastrointestinal tract. First-pass metabolism is estimated at about 15%, and its plasma half-life is on the order of 3 to 4 hours.The binding of pindolol to plasma proteins is approximately 50%.The metabolic fate of pindolol is not completely understood, although 50% of an administered dose is recovered, primarily in the urine, as unchanged drug.

Pindolol Preparation Products And Raw materials

Raw materials

Preparation Products

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Pindolol Suppliers

Tocris Bioscience
Tel
--
Fax
--
Email
customerservice@tocris.co.uk
Country
United Kingdom
ProdList
5726
Advantage
77
Whyte Chemicals
Tel
--
Fax
--
Email
sales@whytechemicals.co.uk
Country
United Kingdom
ProdList
3748
Advantage
50
Leancare Ltd.
Tel
--
Fax
--
Email
enquiry@leancare.co.uk
Country
United Kingdom
ProdList
6446
Advantage
42
MOLEKULA Ltd.
Tel
--
Fax
--
Email
kevinbanks@molekula.com
Country
United Kingdom
ProdList
6140
Advantage
66
CARBONE SCIENTIFIC CO.,LTD
Tel
--
Fax
--
Email
sales@carbonesci.com
Country
United Kingdom
ProdList
6666
Advantage
30
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View Lastest Price from Pindolol manufacturers

Zhuozhou Wenxi import and Export Co., Ltd
Product
Pindolol 13523-86-9
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
Pindolol 13523-86-9
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-08
Career Henan Chemical Co
Product
Pindolol 13523-86-9
Price
US $1.00/KG
Min. Order
1g
Purity
98%
Supply Ability
200kgs
Release date
2020-01-09

13523-86-9, PindololRelated Search:


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  • (+-)-lb46
  • (rs)-pindolol
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  • 1-(1H-INDOL-4-YLOXY)-3-[(1-METHYLETHYL)AMINO]-2-PROPANOL
  • 1-[1H-INDOL-4-YLOXY]-3-[ISOPROPYLAMINO]-2-PROPANOL
  • 1-(INDOL-4-YLOXY)-3-(ISOPROPYLAMINO)-2-PROPANOL
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  • 1-((1-methylethyl)amino)-3-(4-indolyloxy)-2-propanol
  • 1-(1h-indol-4-yloxy)-3-((1-methylethyl)amino)-2-propano
  • 1-(4-indolyloxy)-3-(isopropylamino)-2-propano
  • 1-(4-Indolyloxy)-3-(isopropylamino)-2-propanol
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  • 2-Propanol, 1-(4-indolyloxy)-3-(isopropylamino)-
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  • C14H21N2O2
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