ChemicalBook > CAS DataBase List > 3-Acetyl-2-bromopyridine

3-Acetyl-2-bromopyridine

Product Name
3-Acetyl-2-bromopyridine
CAS No.
84199-61-1
Chemical Name
3-Acetyl-2-bromopyridine
Synonyms
3-ACETYL-2-BROMOPYRIDINE;1-(2-Bromo-3-pyridyl)ethanone;1-(2-Bromo-3-pyridinyl)ethanone;3-(2-Bromopyridyl) methyl ketone;1-(2-BROMO-PYRIDIN-3-YL)-ETHANONE;1-(2-broMopyridin-3-yl)ethan-1-one;Ethanone, 1-(2-bromo-3-pyridinyl)-;3-Acetyl-2-bromopyridine ISO 9001：2015 REACH
CBNumber
CB3401246
Molecular Formula
C7H6BrNO
Formula Weight
200.03
MOL File
84199-61-1.mol
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3-Acetyl-2-bromopyridine Property

Boiling point:
115 °C(Press: 7 Torr)
Density 
1.552 g/mL at 25 °C
refractive index 
n20/D1.572
Flash point:
>110℃
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
liquid
pka
-1.01±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
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Safety

Hazard Codes 
Xn
Risk Statements 
22-36/37/38
Safety Statements 
26
WGK Germany 
1
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
706701
Product name
3-Acetyl-2-bromopyridine
Purity
97%
Packaging
250mg
Price
$298
Updated
2023/06/20
TRC
Product number
A168055
Product name
3-Acetyl-2-bromopyridine
Packaging
1g
Price
$95
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA51213
Product name
3-Acetyl-2-bromopyridine
Packaging
250mg
Price
$110
Updated
2021/12/16
Matrix Scientific
Product number
073528
Product name
3-Acetyl-2-bromopyridine
Purity
95+%
Packaging
250mg
Price
$278
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA51213
Product name
3-Acetyl-2-bromopyridine
Packaging
500mg
Price
$175
Updated
2021/12/16
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3-Acetyl-2-bromopyridine Chemical Properties,Usage,Production

Uses

3-Acetyl-2-bromopyridine is a chemical reagent used in nonquaternary reactivators of GF-inhibited human acetylcholinesterase. Also used in the synthesis of HIV-1 reverse transriptase inhibitors.

Synthesis

84199-57-5

84199-61-1

GENERAL METHOD: CrO3 (33.1 g, 0.331 mol) was slowly added in small portions to a solution of 1-(2-bromopyridin-3-yl)ethanol (30.5 g, 0.133 mol) in acetone (350 mL). The reaction mixture was stirred at room temperature for 18 hours. The solvent was evaporated under reduced pressure and hexane (1 L) was added, followed by a solution of NaOH (26.5 g, 0.662 mol) in water (150 mL). The mixture was stirred for 30 min. The organic layer was separated, dried with Na2SO4, filtered through a silica gel pad (40 g) and evaporated under reduced pressure.

References

[1] Journal of Chemical Research, Miniprint, 1982, # 10, p. 2863 - 2878
[2] Organic and Biomolecular Chemistry, 2011, vol. 9, # 22, p. 7836 - 7848
[3] Tetrahedron Letters, 2017, vol. 58, # 20, p. 1989 - 1991
[4] Journal of Organic Chemistry, 2017, vol. 82, # 21, p. 11585 - 11593
[5] Journal of Medicinal Chemistry, 1994, vol. 37, # 7, p. 999 - 1014

3-Acetyl-2-bromopyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Acetyl-2-bromopyridine manufacturers

Dideu Industries Group Limited
Product
3-Acetyl-2-bromopyridine 84199-61-1
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-23
Shaanxi Dideu Medichem Co. Ltd
Product
3-Acetyl-2-bromopyridine 84199-61-1
Price
US $0.00-0.00/Kg
Min. Order
1KG
Purity
99.0%
Supply Ability
500 MT
Release date
2020-05-12
Career Henan Chemical Co
Product
3-Acetyl-2-bromopyridine 84199-61-1
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-08

84199-61-1, 3-Acetyl-2-bromopyridineRelated Search:

2-Bromopyridine Acetylacetone Tetraacetylethylenediamine 3-Acetylpyridine N-ACETYL-L-TYROSINE ETHYL ESTER Acetylferrocene Acetyl chloride 1-Hexadecylpyridinium bromide 2-BROMO-3-FORMYLPYRIDINE 2-Acetyl-6-bromopyridine,2-ACETYL-6-BROMOPYRIDINE 97 2-Acetyl-5-bromopyridine 3-ACETYL-6-BROMOPYRIDINE,5-acetyl-2-bromopyridine,5-Acetyl-2-bromopyridine 97% 5-Acetyl-3-bromopyridine,3-ACETYL-5-BROMOPYRIDINE 4-ACETYL-2-BROMOPYRIDINE HYDROBROMIDE 3-(2-BROMO-PYRIDIN-3-YL)-3-OXO-PROPIONITRILE 1-(2-BROMO-PYRIDIN-3-YL)-2,2,2-TRIFLUORO-ETHANONE 3-Acetyl-2-bromopyridine 2-bromopyridine

  • 3-ACETYL-2-BROMOPYRIDINE
  • 1-(2-BROMO-PYRIDIN-3-YL)-ETHANONE
  • 1-(2-Bromo-3-pyridinyl)ethanone
  • 3-(2-Bromopyridyl) methyl ketone
  • Ethanone, 1-(2-bromo-3-pyridinyl)-
  • 1-(2-broMopyridin-3-yl)ethan-1-one
  • 3-Acetyl-2-bromopyridine ISO 9001：2015 REACH
  • 1-(2-Bromo-3-pyridyl)ethanone
  • 84199-61-1
  • Heterocycle-Pyridine series