3-METHOXY-PYRIDINE-2-CARBALDEHYDE
- Product Name
- 3-METHOXY-PYRIDINE-2-CARBALDEHYDE
- CAS No.
- 1849-53-2
- Chemical Name
- 3-METHOXY-PYRIDINE-2-CARBALDEHYDE
- Synonyms
- 3-Methoxypicolinaldehyde;3-METHOXY-PYRIDINECARBOXALDEHYDE;3-METHOXY-PYRIDINE-2-CARBALDEHYDE;3-Methoxypyridine-2-carboxaldehyde;3-METHOXY-2-PYRIDINECARBOXALDEHYDE;2-Pyridinecarboxaldehyde, 3-methoxy-;3-Methoxy-2-pyridinecarboxaldehyde ,97%
- CBNumber
- CB3713785
- Molecular Formula
- C7H7NO2
- Formula Weight
- 137.14
- MOL File
- 1849-53-2.mol
3-METHOXY-PYRIDINE-2-CARBALDEHYDE Property
- Melting point:
- 67-68 °C
- Boiling point:
- 239.4±20.0 °C(Predicted)
- Density
- 1.159±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- form
- solid
- pka
- 3.19±0.10(Predicted)
- Appearance
- Light yellow to green yellow Solid
- InChI
- InChI=1S/C7H7NO2/c1-10-7-3-2-4-8-6(7)5-9/h2-5H,1H3
- InChIKey
- GHKILJGWQPBQGL-UHFFFAOYSA-N
- SMILES
- C1(C=O)=NC=CC=C1OC
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-37/38-41
- Safety Statements
- 26-39
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M333003
- Product name
- 3-Methoxypyridine-2-carbaldehyde
- Packaging
- 500mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- OR901629
- Product name
- 3-methoxypyridine-2-carbaldehyde
- Purity
- 97%
- Packaging
- 5g
- Price
- $631
- Updated
- 2021/12/16
- Product number
- CHM0010623
- Product name
- 3-METHOXY-PYRIDINECARBOXALDEHYDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $724.5
- Updated
- 2021/12/16
- Product number
- 081628
- Product name
- 3-Methoxypyridine-2-carbaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $727
- Updated
- 2021/12/16
- Product number
- V3952
- Product name
- 3-methoxypyridine-2-carbaldehyde
- Packaging
- 10g
- Price
- $745
- Updated
- 2021/12/16
3-METHOXY-PYRIDINE-2-CARBALDEHYDE Chemical Properties,Usage,Production
Uses
3-Methoxypyridine-2-carbaldehyde is a useful reactant and reagent for organic reactions and synthesis.
Synthesis Reference(s)
Tetrahedron Letters, 29, p. 773, 1988 DOI: 10.1016/S0040-4039(00)80206-3
Synthesis
26395-26-6
1849-53-2
General procedure for the synthesis of 3-methoxypyridine-2-carbaldehyde using 3-methoxy-2-methylpyridine as starting material: selenium dioxide (478 mg, 4.30 mmol) was dissolved in dioxane (8 mL) and heated to 80 °C. Subsequently, a solution of 3-methoxy-2-methylpyridine (265 mg, 2.15 mmol) in dioxane (2 mL) was slowly added. The reaction mixture was continuously stirred at 80 °C for 18 hours. After completion of the reaction, the mixture was cooled to room temperature and filtered to remove insoluble impurities. The filtrate was concentrated under reduced pressure to remove the solvent to give the crude product. Finally, the crude product was purified by column chromatography to afford the target compound 3-methoxypyridine-2-carboxaldehyde as a yellow gel in 27% yield.
References
[1] Patent: CN103570683, 2018, B. Location in patent: Paragraph 0748; 0753; 0757; 0758
3-METHOXY-PYRIDINE-2-CARBALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-METHOXY-PYRIDINE-2-CARBALDEHYDE manufacturers
- Product
- 3-METHOXY-PYRIDINE-2-CARBALDEHYDE 1849-53-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-19