ChemicalBook > CAS DataBase List > Ethyl 3-Amino-4-methylbenzoate

Ethyl 3-Amino-4-methylbenzoate

Product Name
Ethyl 3-Amino-4-methylbenzoate
CAS No.
41191-92-8
Chemical Name
Ethyl 3-Amino-4-methylbenzoate
Synonyms
AKOS BB-3093;Nilotinib Impurity 36;Ethyl 3-Amino-p-toluate;Nicotinamide Impurity 111;3-aMino-4-Methyl-, ethyl ester;ethyl 3-amino-4-methylbenzoate;Ethyl3-Amino-4-methylbenzoate>3-Amino-p-toluic Acid Ethyl Ester;3-AMINO-4-METHYLBENZOIC ACID ETHYL ESTER;Benzoic acid, 3-aMino-4-Methyl-, ethyl ester
CBNumber
CB3823116
Molecular Formula
C10H13NO2
Formula Weight
179.22
MOL File
41191-92-8.mol
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Ethyl 3-Amino-4-methylbenzoate Property

Melting point:
48.6-50.1℃
Boiling point:
105°C/0.2mmHg(lit.)
Density 
1.103±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
solubility 
soluble in Methanol
form 
powder to crystal
pka
3.35±0.10(Predicted)
color 
White to Almost white
InChIKey
MCNBNDUVWQEKNZ-UHFFFAOYSA-N
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Safety

HS Code 
2922498590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
T303518
Product name
ETHYL 3-AMINO-4-METHYLBENZOATE
Purity
AldrichCPR
Packaging
1MG
Price
$144
Updated
2024/03/01
TCI Chemical
Product number
E1025
Product name
Ethyl 3-Amino-4-methylbenzoate
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$50
Updated
2024/03/01
TCI Chemical
Product number
E1025
Product name
Ethyl 3-Amino-4-methylbenzoate
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$176
Updated
2021/12/16
TRC
Product number
B433913
Product name
Ethyl 3-Amino-4-methylbenzoate
Packaging
250mg
Price
$45
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA71551
Product name
3-Amino-4-methylbenzoic acid ethyl ester
Packaging
2g
Price
$40
Updated
2021/12/16
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Ethyl 3-Amino-4-methylbenzoate Chemical Properties,Usage,Production

Synthesis

Dissolve 10 g of palladium on carbon (10%) and 140 g of ammonium formate in 400 ml of methanol, and then dissolve 136 g of ethyl 3-nitro-4-methylbenzoate (2) in 400 ml of methanol. Add the methanol solution of (2) dropwise to the reaction flask at room temperature. The reaction exotherms until the methanol boils. Continue the dropwise addition. After the dropwise addition, TLC detects the completion of the reaction and filters the palladium carbon. Concentrate the methanol, add 400ml of water, and filter to obtain 156g of white solid ethyl 3-amino-4-methylbenzoate (Ethyl 3-Amino-4-methylbenzoate) as a wet product, which can be used in the next step without drying.

Ethyl 3-Amino-4-methylbenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethyl 3-Amino-4-methylbenzoate manufacturers

Hebei Mojin Biotechnology Co., Ltd
Product
Ethyl 3-amino-4-methylbenzoate 41191-92-8
Price
US $0.00/ASSAYS
Min. Order
1Kg/Bag
Purity
99%
Supply Ability
20ton
Release date
2021-10-14
Career Henan Chemical Co
Product
3-Amino-4-methylbenzoic acid ethyl ester 41191-92-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20kg
Release date
2018-08-13