ChemicalBook > CAS DataBase List > Methyl 3-bromo-5-iodobenzoate

Methyl 3-bromo-5-iodobenzoate

Product Name: Methyl 3-bromo-5-iodobenzoate
CAS No.: 188813-07-2
Chemical Name: Methyl 3-bromo-5-iodobenzoate
Synonyms: Methyl 5-bromo-3-iodobenzoate;Methyl3-bromo-5-iodobenzoate97%;Methyl 3-bromo-5-iodobenzoate 97%;Benzoic acid, 3-bromo-5-iodo-, meth;3-BroMo-5-iodobenzoic acid Methyl ester;Benzoic acid,3-broMo-5-iodo-, Methyl ester
CBNumber: CB61106462
Molecular Formula: C8H6BrIO2
Formula Weight: 340.94
MOL File: 188813-07-2.mol

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Methyl 3-bromo-5-iodobenzoate Property

Melting point:: 62.0-63.0 °C
Boiling point:: 334.5±32.0 °C(Predicted)
Density: 2.059±0.06 g/cm3(Predicted)
storage temp.: RT, protect from light
form: Powder
Appearance: White to off-white Solid

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M296580
Product name: Methyl3-Bromo-5-iodobenzoate
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB67313
Product name: 3-Bromo-5-iodobenzoic acid methyl ester
Packaging: 500mg
Price: $60
Updated: 2021/12/16

ChemScene

Product number: CS-0044963
Product name: Methyl3-bromo-5-iodobenzoate
Packaging: 1g
Price: $60
Updated: 2021/12/16

Apolloscientific

Product number: OR17113
Product name: Methyl3-bromo-5-iodobenzoate
Purity: 97%
Packaging: 1g
Price: $145
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB67313
Product name: 3-Bromo-5-iodobenzoic acid methyl ester
Packaging: 2g
Price: $155
Updated: 2021/12/16

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Methyl 3-bromo-5-iodobenzoate Chemical Properties,Usage,Production

Synthesis

188815-32-9

74-88-4

188813-07-2

(a) Synthesis of methyl 3-bromo-5-iodobenzoate: In a dry reaction flask, 3-bromo-5-iodobenzoic acid (15 g, 45.9 mmol) was dissolved in a solvent mixture of tetrahydrofuran (20 mL) and N,N-dimethylformamide (75 mL). Sodium carbonate (9.7 g, 92 mmol) and iodomethane (5.7 mL, 92 mmol) were then added. The reaction mixture was stirred at room temperature for 20 hours. After completion of the reaction, most of the solvent was removed by concentration under reduced pressure. The residue was extracted with ethyl acetate and washed sequentially with water, saturated aqueous sodium bicarbonate solution and brine. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the title compound methyl 3-bromo-5-iodobenzoate. Yield: 15 g (99% yield).

References

[1] Patent: WO2010/103279, 2010, A1. Location in patent: Page/Page column 126
[2] Patent: WO2010/103297, 2010, A2. Location in patent: Page/Page column 71

Methyl 3-bromo-5-iodobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Methyl 3-bromo-5-iodobenzoate manufacturers

Qingdao RENAS Polymer Material Co., Ltd.

Product: methyl 3-bromo-5-iodobenzoate 188813-07-2
Price: US $0.00/kg
Min. Order: 20kg
Purity: 99%
Supply Ability: 20 tons
Release date: 2025-04-07

Hangzhou ICH Biofarm Co., Ltd

Product: Methyl 3-bromo-5-iodobenzoate 188813-07-2
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 2000kg
Release date: 2023-06-09

Career Henan Chemical Co

Product: Methyl 3-bromo-5-iodobenzoate 188813-07-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-31

188813-07-2, Methyl 3-bromo-5-iodobenzoateRelated Search:

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188813-07-2

Acids & Esters

Bromine Compounds

Iodine Compounds