1-N-Cbz-3-Methylpiperidine-3-carboxylic acid

Product Name: 1-N-Cbz-3-Methylpiperidine-3-carboxylic acid
CAS No.: 174543-78-3
Chemical Name: 1-N-Cbz-3-Methylpiperidine-3-carboxylic acid
Synonyms: 1-N-Cbz-3-Methylpiperidine-3-carboxylic;1-Cbz-3-Methylpiperidine-3-carboxylic Acid;1-Cbz-3-methyl-3-piperidinecarboxylic acid;N-Cbz-3-Methylpiperidine-3-carboxylic acid;1-N-Cbz-3-Methylpiperidine-3-carboxylic acid;1-Cbz-3-methyl-3-piperidinecarboxylic acid - [M13677];1-[(benzyloxy)carbonyl]-3-methylpiperidine-3-carboxylic acid;3-Methyl-1,3-piperidinedicarboxylic acid 1-(phenylmethyl) ester;1,3-Piperidinedicarboxylic acid, 3-methyl-, 1-(phenylmethyl) ester
CBNumber: CB61503942
Molecular Formula: C15H19NO4
Formula Weight: 277.32
MOL File: 174543-78-3.mol

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1-N-Cbz-3-Methylpiperidine-3-carboxylic acid Property

Boiling point:: 440.3±45.0 °C(Predicted)
Density: 1.224
storage temp.: Store at room temperature
pka: 4.52±0.20(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C227923
Product name: 1-N-Cbz-3-Methylpiperidine-3-carboxylicAcid
Packaging: 500mg
Price: $130
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H58-1-QX
Product name: 1-[(Benzyloxy)carbonyl]-3-methylpiperidine-3-carboxylic acid
Purity: 97.0%
Packaging: 250mg
Price: $140
Updated: 2021/12/16

AK Scientific

Product number: 5153AJ
Product name: 1-N-Cbz-3-methylpiperidine-3-carboxylicacid
Packaging: 5g
Price: $471
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0117377
Product name: 1-N-CBZ-3-METHYL-PIPERIDINE-3-CARBOXYLIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $501.62
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC150111
Product name: 1-N-Cbz-3-methyl-piperidine-3-carboxylicacid
Packaging: 1g
Price: $582
Updated: 2021/12/16

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1-N-Cbz-3-Methylpiperidine-3-carboxylic acid Chemical Properties,Usage,Production

Synthesis

664364-60-7

174543-78-3

Step C: 3-Benzyl 3-ethyl-3-methylpiperidine-1,3-dicarboxylate (3.0 g, 10.0 mmol) was dissolved in ethanol (15 mL) and aqueous LiOH solution (15.0 mL, 30.1 mmol) was added. The reaction mixture was stirred at 86 °C for 1 hour. After completion of the reaction, ethanol was removed by distillation under reduced pressure. Ether (30 mL) was added to the residue for extraction and the aqueous layer was separated. The aqueous layer was acidified to pH 3-4 with saturated potassium bisulfate solution and then extracted with ethyl acetate (50 mL). The organic layer was washed with brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure to give 1-(benzyloxycarbonyl)-3-methylpiperidine-3-carboxylic acid (2.6 g, 92% yield) as an oil.

References

[1] Patent: WO2009/140320, 2009, A1. Location in patent: Page/Page column 73
[2] Patent: US2006/149070, 2006, A1. Location in patent: Page/Page column 41

1-N-Cbz-3-Methylpiperidine-3-carboxylic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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1-N-Cbz-3-Methylpiperidine-3-carboxylic acid Suppliers

China 40 Germany 1 India 1 United Kingdom 1 United States 12 Global 55

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View Lastest Price from 1-N-Cbz-3-Methylpiperidine-3-carboxylic acid manufacturers

Shanghai Rlavie Technology Co ltd

Product: 1-Cbz-3-Methylpiperidine-3-carboxylic Acid 174543-78-3
Price: US $0.00/KG
Min. Order: 0.001KG
Purity: 98%min
Supply Ability: 100kgs/month
Release date: 2022-05-10

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1-N-Cbz-3-Methylpiperidine-3-carboxylic acid

3-Methyl-1,3-piperidinedicarboxylic acid 1-(phenylmethyl) ester

1-[(benzyloxy)carbonyl]-3-methylpiperidine-3-carboxylic acid

N-Cbz-3-Methylpiperidine-3-carboxylic acid

1-Cbz-3-methyl-3-piperidinecarboxylic acid

1-Cbz-3-Methylpiperidine-3-carboxylic Acid

1,3-Piperidinedicarboxylic acid, 3-methyl-, 1-(phenylmethyl) ester

1-N-Cbz-3-Methylpiperidine-3-carboxylic

1-Cbz-3-methyl-3-piperidinecarboxylic acid - [M13677]

174543-78-3