3-Hydroxy-4-methoxybenzonitrile
- Product Name
- 3-Hydroxy-4-methoxybenzonitrile
- CAS No.
- 52805-46-6
- Chemical Name
- 3-Hydroxy-4-methoxybenzonitrile
- Synonyms
- Benzonitrile, 3-hydroxy-4-Methoxy-;ISOVANILLONITRILE;CBI-BB ZERO/005397;2-methoxy-5-cyanophenol;5-Cyano-2-methoxyphenol;3-Hydroxy-4-methoxybenzonitril;3-HYDROXY-4-METHOXYBENZONITRILE;3-Hydroxy-4-methoxy benzonitrile 95+%;3-Hydroxy-4-methoxybenzonitrile ISO 9001：2015 REACH;3-HYDROXY-4-METHOXYBENZONITRILE (ISOVANILLONITRILE)
- CBNumber
- CB6287199
- Molecular Formula
- C8H7NO2
- Formula Weight
- 149.15
- MOL File
- 52805-46-6.mol
3-Hydroxy-4-methoxybenzonitrile Property
- Melting point:
- 124 °C
- Boiling point:
- 300.8±27.0 °C(Predicted)
- Density
- 1.24±0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 8.59±0.10(Predicted)
- Appearance
- White to off-white Solid
- CAS DataBase Reference
- 52805-46-6(CAS DataBase Reference)
Safety
- HS Code
- 29269090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- H972653
- Product name
- 3-Hydroxy-4-methoxybenzonitrile
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR345595
- Product name
- 3-Hydroxy-4-methoxybenzonitrile
- Purity
- 95+%
- Packaging
- 25g
- Price
- $70
- Updated
- 2021/12/16
- Product number
- CS-W002933
- Product name
- 3-Hydroxy-4-methoxybenzonitrile
- Purity
- 99.87%
- Packaging
- 100g
- Price
- $101
- Updated
- 2021/12/16
- Product number
- 074666
- Product name
- 3-Hydroxy-4-methoxybenzonitrile
- Purity
- 95+%
- Packaging
- 25g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 074666
- Product name
- 3-Hydroxy-4-methoxybenzonitrile
- Purity
- 95+%
- Packaging
- 100g
- Price
- $300
- Updated
- 2021/12/16
3-Hydroxy-4-methoxybenzonitrile Chemical Properties,Usage,Production
Synthesis
621-59-0
52805-46-6
The general procedure for synthesizing 3-hydroxy-4-methoxybenzonitrile from isovanillin was as follows: 14.2 g of isovanillin was dissolved in 75 mL of formic acid, 15 g of sodium formate was added, and stirred at 85 °C. Subsequently, 9 g of hydroxylamine hydrochloride was added in batches, and the reaction mixture was kept at 85 °C and continued to be stirred for 4 hours. Upon completion of the reaction, the mixture was poured into a nearly saturated sodium chloride solution and a precipitate was precipitated. The precipitate was separated by filtration, washed sequentially with water and petroleum ether, and dried to give the product. The yield was 14.2 g. The yield was 93% of the theoretical value. The product was analyzed by HPLC-MS (Method D) with a retention time (Rt) of 1.18 min.
References
[1] Patent: WO2011/92128, 2011, A1. Location in patent: Page/Page column 37
[2] Patent: US2012/28939, 2012, A1. Location in patent: Page/Page column 18
[3] Patent: CN105330586, 2016, A. Location in patent: Paragraph 0055; 0056
[4] Patent: CN105461602, 2016, A. Location in patent: Paragraph 0049; 0050
[5] Molecules, 2017, vol. 22, # 10,
3-Hydroxy-4-methoxybenzonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Hydroxy-4-methoxybenzonitrile manufacturers
- Product
- 3-Hydroxy-4-methoxybenzonitrile 52805-46-6
- Price
- US $8.80/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 100kg
- Release date
- 2019-07-12
- Product
- 3-Hydroxy-4-methoxybenzonitrile 52805-46-6
- Price
- US $8.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2018-12-15