3-BROMOISOQUINOLINE
- Product Name
- 3-BROMOISOQUINOLINE
- CAS No.
- 34784-02-6
- Chemical Name
- 3-BROMOISOQUINOLINE
- Synonyms
- 3-BROMOISOQUINOLINE;Isoquinoline, 3-bromo-;3-BROMOISOQUINOLINE 97%;3-Bromo-2-azanaphthalene;3-Bromoisoquinoline ,99%;3-BROMOISOQUINOLINE ISO 9001:2015 REACH
- CBNumber
- CB6447579
- Molecular Formula
- C9H6BrN
- Formula Weight
- 208.05
- MOL File
- 34784-02-6.mol
3-BROMOISOQUINOLINE Property
- Melting point:
- 63-64 °C
- Boiling point:
- 316.3±15.0 °C(Predicted)
- Density
- 1.564±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- pka
- 1.84±0.30(Predicted)
- Appearance
- White to light brown Solid
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-36/37/38
- Safety Statements
- 26-36/37/39
- WGK Germany
- 3
- HS Code
- 29334900
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 797030
- Product name
- 3-Bromoisoquinoline
- Purity
- 95%
- Packaging
- 1g
- Price
- $269
- Updated
- 2023/06/20
- Product number
- 069897
- Product name
- 3-Bromoisoquinoline
- Purity
- 97%
- Packaging
- 5g
- Price
- $310
- Updated
- 2021/12/16
- Product number
- OR40221
- Product name
- 3-Bromoisoquinoline
- Packaging
- 500mg
- Price
- $44
- Updated
- 2021/12/16
- Product number
- 3H32-9-T0
- Product name
- 3-Bromoisoquinoline
- Packaging
- 500mg
- Price
- $48
- Updated
- 2021/12/16
- Product number
- OR40221
- Product name
- 3-Bromoisoquinoline
- Packaging
- 1g
- Price
- $70
- Updated
- 2021/12/16
3-BROMOISOQUINOLINE Chemical Properties,Usage,Production
Chemical Properties
Yellow powder
Synthesis
119-65-3
34784-02-6
To a stirred solution of isoquinoline (24 g, 186 mmol) in acetic acid (50 mL) was slowly added N-bromosuccinimide (NBS, 36.2 g, 204.6 mmol) at room temperature. The reaction mixture was heated to 100 °C and kept at this temperature for the reaction overnight. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated under reduced pressure to remove the solvent. The resulting crude product was purified by fast column chromatography (eluent: 5% ethyl acetate/hexane) to give 3-bromoisoquinoline (9.2 g, 23.8% yield) as an oil.
References
[1] Patent: US2013/178457, 2013, A1. Location in patent: Paragraph 0219
3-BROMOISOQUINOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-BROMOISOQUINOLINE manufacturers
- Product
- 3-BROMOISOQUINOLINE 34784-02-6
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99.0%
- Supply Ability
- 100kg
- Release date
- 2020-01-09