3-BROMO-5-FLUOROBENZYL ALCOHOL
- Product Name
- 3-BROMO-5-FLUOROBENZYL ALCOHOL
- CAS No.
- 216755-56-5
- Chemical Name
- 3-BROMO-5-FLUOROBENZYL ALCOHOL
- Synonyms
- (3-Bromo-5-fluorophenyl);3-BROMO-5-FLUOROBENZYL ALCOHOL;(3-BroMo-5-fluorophenyl)Methanol;3-Bromo-5-fluorobenzylalcohol98%;3-Bromo-5-fluorobenzyl alcohol 98%;Benzenemethanol, 3-bromo-5-fluoro-;3-BROMO-5-FLUOROBENZYL ALCOHOL ISO 9001：2015 REACH
- CBNumber
- CB7157017
- Molecular Formula
- C7H6BrFO
- Formula Weight
- 205.02
- MOL File
- 216755-56-5.mol
3-BROMO-5-FLUOROBENZYL ALCOHOL Property
- Boiling point:
- 259.0±25.0 °C(Predicted)
- Density
- 1.658±0.06 g/cm3(Predicted)
- storage temp.
- Store at room temperature
- pka
- 13.94±0.10(Predicted)
- form
- Liquid
- color
- Colorless
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- B692110
- Product name
- 3-Bromo-5-fluorobenzylalcohol
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- PC2406
- Product name
- 3-Bromo-5-fluorobenzylalcohol
- Purity
- 98%
- Packaging
- 1g
- Price
- $38
- Updated
- 2021/12/16
- Product number
- 2601-B-X3
- Product name
- 3-Bromo-5-fluorobenzyl alcohol
- Purity
- 98%
- Packaging
- 1g
- Price
- $42
- Updated
- 2021/12/16
- Product number
- PC2406
- Product name
- 3-Bromo-5-fluorobenzylalcohol
- Purity
- 98%
- Packaging
- 5g
- Price
- $80
- Updated
- 2021/12/16
- Product number
- W4495
- Product name
- 3-Bromo-5-fluorobenzylalcohol
- Packaging
- 1g
- Price
- $83
- Updated
- 2021/12/16
3-BROMO-5-FLUOROBENZYL ALCOHOL Chemical Properties,Usage,Production
Synthesis
176548-70-2
216755-56-5
General procedure for the synthesis of (3-bromo-5-fluorophenyl)methanol from 3-bromo-5-fluorobenzoic acid: 3-bromo-5-fluorobenzoic acid (1.0 g, 4.52 mmol) was suspended in tetrahydrofuran (8 mL) and the mixture was cooled to 0°C. Borane tetrahydrofuran complex (1 M in tetrahydrofuran, 9 mL, 9.0 mmol) was added slowly and dropwise over 15 min. The reaction mixture was gradually warmed to room temperature and stirred overnight. Upon completion of the reaction, the mixture was cooled again to 0 °C and the reaction was quenched by careful addition of excess methanol. Subsequently, the reaction mixture was diluted with ethyl acetate and washed sequentially with 1 N sodium hydroxide solution (2×) and saturated brine (2×). The organic phase was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 0.88 g (95% yield) of the white solid product (3-bromo-5-fluorophenyl)methanol. The structure of the product was confirmed by 1H-NMR (CDCl3, 500 MHz): δ 7.29 (s, 1H), 7.16 (d, J = 7.9 Hz, 1H), 7.03 (d, J = 9.2 Hz, 1H), 4.66 (s, 2H).
References
[1] Patent: US2007/249607, 2007, A1. Location in patent: Page/Page column 81
[2] Patent: CN104447730, 2017, B. Location in patent: Paragraph 0146-0147
[3] Patent: WO2016/54728, 2016, A1. Location in patent: Paragraph 00127
[4] Patent: WO2016/74068, 2016, A1. Location in patent: Paragraph 00121
[5] Patent: WO2006/79791, 2006, A1. Location in patent: Page/Page column 44
3-BROMO-5-FLUOROBENZYL ALCOHOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-BROMO-5-FLUOROBENZYL ALCOHOL manufacturers
- Product
- 3-Bromo-5-fluorobenzyl alcohol 216755-56-5
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 2000kg
- Release date
- 2023-06-09
- Product
- 3-Bromo-5-fluorobenzyl alcohol 216755-56-5
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.1%
- Supply Ability
- 100 tons
- Release date
- 2022-01-26
- Product
- 3-BROMO-5-FLUOROBENZYL ALCOHOL 216755-56-5
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2020-01-09