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3-Amino-4-methoxybenzanilide

Product Name
3-Amino-4-methoxybenzanilide
CAS No.
120-35-4
Chemical Name
3-Amino-4-methoxybenzanilide
Synonyms
AMBA;AMAN;Red KD Base;Red based KD;FAST RED KD BASE;3-AMINO-P-ANISANILIDE;LABOTEST-BB LT01138545;4-Methoxy-3-aminobenzanilide;3-AMINO-4-METHOXYBENZANILIDE;3-amino-4-methoxy-benzanilid
CBNumber
CB7251074
Molecular Formula
C14H14N2O2
Formula Weight
242.27
MOL File
120-35-4.mol
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3-Amino-4-methoxybenzanilide Property

Melting point:
154-156°C
Boiling point:
385.1°C (rough estimate)
Density 
1.1338 (rough estimate)
vapor pressure 
0-0Pa at 25℃
refractive index 
1.6419 (estimate)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
DMSO (Slightly), Methanol (Slightly)
form 
Solid
pka
13.44±0.70(Predicted)
color 
White to Off-White
LogP
2.08 at 23℃ and pH7
CAS DataBase Reference
120-35-4(CAS DataBase Reference)
EPA Substance Registry System
Benzamide, 3-amino-4-methoxy-N-phenyl- (120-35-4)
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
RTECS 
CV7400000
TSCA 
Yes
HazardClass 
IRRITANT
HS Code 
2924297099
Toxicity
mouse,LD50,intravenous,320mg/kg (320mg/kg),U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#01183,
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
S373079
Product name
3-AMINO-4-METHOXYBENZANILIDE
Purity
Aldrich
Packaging
50mg
Price
$179
Updated
2024/03/01
TCI Chemical
Product number
A1954
Product name
3-Amino-4-methoxybenzanilide
Purity
>98.0%(T)
Packaging
25g
Price
$38
Updated
2024/03/01
TCI Chemical
Product number
A1954
Product name
3-Amino-4-methoxybenzanilide
Purity
>98.0%(T)
Packaging
250g
Price
$75
Updated
2024/03/01
Alfa Aesar
Product number
A19168
Product name
3-Amino-4-methoxybenzanilide, 98%
Packaging
50g
Price
$173
Updated
2021/12/16
Alfa Aesar
Product number
A19168
Product name
3-Amino-4-methoxybenzanilide, 98%
Packaging
10g
Price
$44.2
Updated
2021/12/16
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3-Amino-4-methoxybenzanilide Chemical Properties,Usage,Production

Chemical Properties

Gray powder.

Uses

3-Amino-4-methoxybenzanilide is used in preparation method of Cyanate resin-based near-zero expansion composite material truss rod.

Uses

Dyes, pharmaceuticals, and other organic chemicals.

Synthesis

3-Amino-4-methoxybenzanilide is prepared by the reaction of 3-amino-4-methoxybenzoic acid and aniline. The steps are as follows:
A total of 0.17 mL (0.18 mmol) of DIC and 0.24 g (0.18 mmol) of HOBt were added to a dichloromethane solution of 0.20 g (0.12 mmol) of 1 at room temperature, and the reaction mixture was stirred for 0.5 h. Then, 0.13 mL (0.14 mmol) of aniline was added to the mixture. After approximately 3 h, 0.5 N NaOH was added to the solution. The lower layer was isolated, and 0.5 N HCl was added until the aqueous solution was neutral. The dichloromethane layer was washed three times with 10 mL of water, and then MgSO4 was added. After 2 h, the solution was filtered, and the solvent was removed. The residue was purified by column chromatography on silica gel (eluent: petroleum ether:ethyl acetate = 3:1) to yield the desired 3-Amino-4-methoxybenzanilide as a white solid (yield: 76%). Mp: 197-198 °C. 1H NMR (400 MHz, DMSO-d6) δ (ppm): 9.92 (1H, s, NH), 7.74 (2H, d, J = 9.0 Hz, PhH), 7.32 (2H, m, PhH), 7.21 (2H, d, J = 8.0 Hz, PhH), 7.06 (1H, m, PhH), 6.88 (1H, d, J = 8.0 Hz, PhH), 4.90 (2H, br s, NH2), 3.83 (3H, s, OCH3). ESI-MS (m/z): 243 (M + H)+.

3-Amino-4-methoxybenzanilide Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Amino-4-methoxybenzanilide Suppliers

Xiangshui Henryda Tech Chemical Co., Ltd.
Tel
13771648447
Fax
+86-512-69233657
Email
sales@henryda-chem.com
Country
China
ProdList
61
Advantage
58
Hangzhou Jingyou Chemical Co., Ltd.
Tel
+86-0571-28350142 +86-13989804698
Fax
0571-87219532
Email
joy@jingyouchem.com
Country
China
ProdList
190
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
94657
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14103
Advantage
59
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42958
Advantage
64
XiaoGan ShenYuan ChemPharm co,ltd
Tel
15527768850
Email
1791901229@qq.com
Country
China
ProdList
8836
Advantage
52
Syntechem Co.,Ltd
Tel
Fax
E-Mail Inquiry
Email
info@syntechem.com
Country
China
ProdList
12984
Advantage
57
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View Lastest Price from 3-Amino-4-methoxybenzanilide manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
3-Amino-4-methoxybenzanilide 120-35-4
Price
US $0.00/Kg/Bag
Min. Order
1KG
Purity
99%min
Supply Ability
1000kg
Release date
2021-11-29
Hebei Weibang Biotechnology Co., Ltd
Product
3-Amino-4-methoxybenzanilide 120-35-4
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-12-04
Hebei Chuanghai Biotechnology Co,.LTD
Product
3-Amino-4-methoxybenzanilide 120-35-4
Price
US $12.60/KG
Min. Order
1KG
Purity
99%
Supply Ability
5000kg
Release date
2024-08-09

120-35-4, 3-Amino-4-methoxybenzanilideRelated Search:


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  • 3-AMINO-4-METHOXY-N'-PHENYL BENZAMIDE
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  • LABOTEST-BB LT01138545
  • FAST RED KD BASE
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  • 3-Amino-4-methoxybenzanilide ISO 9001:2015 REACH
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  • Intermediates of Dyes and Pigments
  • Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts