3-Amino-4-methoxybenzanilide

Product Name: 3-Amino-4-methoxybenzanilide
CAS No.: 120-35-4
Chemical Name: 3-Amino-4-methoxybenzanilide
Synonyms: AMBA;AMAN;Red KD Base;Red based KD;FAST RED KD BASE;3-AMINO-P-ANISANILIDE;LABOTEST-BB LT01138545;4-Methoxy-3-aminobenzanilide;3-AMINO-4-METHOXYBENZANILIDE;3-amino-4-methoxy-benzanilid
CBNumber: CB7251074
Molecular Formula: C14H14N2O2
Formula Weight: 242.27
MOL File: 120-35-4.mol

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3-Amino-4-methoxybenzanilide Property

Melting point:: 154-156°C
Boiling point:: 385.1°C (rough estimate)
Density: 1.1338 (rough estimate)
vapor pressure: 0-0Pa at 25℃
refractive index: 1.6419 (estimate)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: DMSO (Slightly), Methanol (Slightly)
pka: 13.44±0.70(Predicted)
form: Solid
color: White to Off-White
LogP: 2.08 at 23℃ and pH7
CAS DataBase Reference: 120-35-4(CAS DataBase Reference)
EPA Substance Registry System: Benzamide, 3-amino-4-methoxy-N-phenyl- (120-35-4)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
RTECS: CV7400000
TSCA: Yes
HazardClass: IRRITANT
HS Code: 2924297099
Toxicity: mouse,LD50,intravenous,320mg/kg (320mg/kg),U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#01183,

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S373079
Product name: 3-AMINO-4-METHOXYBENZANILIDE
Purity: Aldrich
Packaging: 50mg
Price: $179
Updated: 2024/03/01

TCI Chemical

Product number: A1954
Product name: 3-Amino-4-methoxybenzanilide
Purity: >98.0%(T)
Packaging: 25g
Price: $38
Updated: 2024/03/01

TCI Chemical

Product number: A1954
Product name: 3-Amino-4-methoxybenzanilide
Purity: >98.0%(T)
Packaging: 250g
Price: $75
Updated: 2024/03/01

Alfa Aesar

Product number: A19168
Product name: 3-Amino-4-methoxybenzanilide, 98%
Packaging: 50g
Price: $173
Updated: 2021/12/16

Alfa Aesar

Product number: A19168
Product name: 3-Amino-4-methoxybenzanilide, 98%
Packaging: 10g
Price: $44.2
Updated: 2021/12/16

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3-Amino-4-methoxybenzanilide Chemical Properties,Usage,Production

Chemical Properties

Gray powder.

Uses

3-Amino-4-methoxybenzanilide is used in preparation method of Cyanate resin-based near-zero expansion composite material truss rod.

Uses

Dyes, pharmaceuticals, and other organic chemicals.

Synthesis

3-Amino-4-methoxybenzanilide is prepared by the reaction of 3-amino-4-methoxybenzoic acid and aniline. The steps are as follows:
A total of 0.17 mL (0.18 mmol) of DIC and 0.24 g (0.18 mmol) of HOBt were added to a dichloromethane solution of 0.20 g (0.12 mmol) of 1 at room temperature, and the reaction mixture was stirred for 0.5 h. Then, 0.13 mL (0.14 mmol) of aniline was added to the mixture. After approximately 3 h, 0.5 N NaOH was added to the solution. The lower layer was isolated, and 0.5 N HCl was added until the aqueous solution was neutral. The dichloromethane layer was washed three times with 10 mL of water, and then MgSO4 was added. After 2 h, the solution was filtered, and the solvent was removed. The residue was purified by column chromatography on silica gel (eluent: petroleum ether:ethyl acetate = 3:1) to yield the desired 3-Amino-4-methoxybenzanilide as a white solid (yield: 76%). Mp: 197-198 °C. 1H NMR (400 MHz, DMSO-d6) δ (ppm): 9.92 (1H, s, NH), 7.74 (2H, d, J = 9.0 Hz, PhH), 7.32 (2H, m, PhH), 7.21 (2H, d, J = 8.0 Hz, PhH), 7.06 (1H, m, PhH), 6.88 (1H, d, J = 8.0 Hz, PhH), 4.90 (2H, br s, NH2), 3.83 (3H, s, OCH3). ESI-MS (m/z): 243 (M + H)+.

3-Amino-4-methoxybenzanilide Preparation Products And Raw materials

Raw materials

4-Chlorobenzoic acid 4-Methoxybenzoic acid Potassium permanganate Sodium hydrosulfide Dichloroethane Sulfuric acid

Preparation Products

Pigment Red 146 Pigment Red 32 Pigment Red 31

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3-Amino-4-methoxybenzanilide Suppliers

Americas 1 China 189 Czech Republic 1 Europe 1 Germany 3 India 21 Japan 4 Slovakia 1 The Netherlands 1 Ukraine 1 United Kingdom 16 United States 30 Global 269

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View Lastest Price from 3-Amino-4-methoxybenzanilide manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD

Product: 3-Amino-4-methoxybenzanilide 120-35-4
Price: US $0.00/Kg/Bag
Min. Order: 1KG
Purity: 99%min
Supply Ability: 1000kg
Release date: 2021-11-29

Hebei Chuanghai Biotechnology Co,.LTD

Product: 3-Amino-4-methoxybenzanilide 120-35-4
Price: US $12.60/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 5000kg
Release date: 2024-08-09

Hebei Weibang Biotechnology Co., Ltd

Product: 3-Amino-4-methoxybenzanilide 120-35-4
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2021-11-25

120-35-4, 3-Amino-4-methoxybenzanilideRelated Search:

N,N-Dimethyl-1,4-phenylenediamine (Trifluoromethoxy)benzene ALTRENOGEST p-Anisidine 2-Aminophenol 2-(Trifluoromethoxy)aniline Benzamide 4'-Methoxyacetophenone p-Anisaldehyde Tris(hydroxymethyl)aminomethane 4-Methoxybenzoic acid Glycine BENZANILIDE 4-Methoxyphenylacetone 4-(Trifluoromethoxy)aniline Anisole p-Aminobenzamide Chlorantraniliprole

AMAN

AMBA

3-AMINO-4-METHOXYBENZANILIDE

3-AMINO-4-METHOXY-N'-PHENYL BENZAMIDE

3-AMINO-P-ANISANILIDE

LABOTEST-BB LT01138545

FAST RED KD BASE

3-Amino-p-anisanilide,prac.,95%

N-(3-amino-4-methoxyphenyl)benzamide

4-Methoxy-3-aminobenzanilide

N-Phenyl-4-methoxy-3-aminobenzamide

3-amino-4-methoxy-benzanilid

1-hydroxy-6,8a-dimethylspiro[4a,6,7,8-tetrahydro-4H-naphthalene-5,2'-oxirane]-1,2-dicarboxaldehyde

3-amino-4-methoxy-n-phenyl-benzamid

Benzamide,3-amino-4-methoxy-N-phenyl-

3-Amino-4-methoxybenzanilide &gt

Red KD Base

3-Amino-4-methoxybenzanilide ISO 9001：2015 REACH

DB-40 (3-AMINO-4-METHOXYBENZANILIDE )

3-Amino-4-methoxybenzanilide 120-35-4

Red based KD

120-35-4

Intermediates of Dyes and Pigments

Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts