2-Chloro-5-nitropyrimidine
- Product Name
- 2-Chloro-5-nitropyrimidine
- CAS No.
- 10320-42-0
- Chemical Name
- 2-Chloro-5-nitropyrimidine
- Synonyms
- 2-CHLORO-5-NITRO-;CHLORO(2-)-5-NITROPYRIDINE;2-CHLORO-5-NITROPYRIMIDINE;PYRIDINE, 2-CHLORO-5-NITRO-;2-Chloro-5-nitro-1,3-diazine;PYRIMIDINE, 2-CHLORO-5-NITRO-;2-Chloro-5-nitropyrimidine 98%;2-Chloro-5-nitropyrimidine >2-Chloro-5-nitropyrimidine ,98%;2-Chloro-5-nitropyrimidine ISO 9001:2015 REACH
- CBNumber
- CB7307005
- Molecular Formula
- C4H2ClN3O2
- Formula Weight
- 159.53
- MOL File
- 10320-42-0.mol
2-Chloro-5-nitropyrimidine Property
- Melting point:
- 105-110 °C
- Boiling point:
- 345.4±15.0 °C(Predicted)
- Density
- 1.600±0.06 g/cm3(Predicted)
- storage temp.
- -20°C
- pka
- -4.60±0.22(Predicted)
- form
- powder to crystal
- color
- Light orange to Yellow to Green
- InChI
- InChI=1S/C4H2ClN3O2/c5-4-6-1-3(2-7-4)8(9)10/h1-2H
- InChIKey
- OFCBNMYNAHUDGE-UHFFFAOYSA-N
- SMILES
- C1(Cl)=NC=C([N+]([O-])=O)C=N1
- CAS DataBase Reference
- 10320-42-0(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38-43-41-37/38-22-20/21/22
- Safety Statements
- 26-36-37/39-36/37/39-36/37-24/25
- RIDADR
- UN 3335
- WGK Germany
- 3
- RTECS
- US7175000
- HazardClass
- IRRITANT
- HS Code
- 29335990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H317May cause an allergic skin reaction
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 720348
- Product name
- 2-Chloro-5-nitropyrimidine
- Purity
- 97%
- Packaging
- 250mg
- Price
- $101
- Updated
- 2023/06/20
- Product number
- 720348
- Product name
- 2-Chloro-5-nitropyrimidine
- Purity
- 97%
- Packaging
- 1g
- Price
- $209
- Updated
- 2023/06/20
- Product number
- C2507
- Product name
- 2-Chloro-5-nitropyrimidine
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $65
- Updated
- 2025/07/31
- Product number
- C2507
- Product name
- 2-Chloro-5-nitropyrimidine
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $319
- Updated
- 2025/07/31
- Product number
- C381310
- Product name
- 2-Chloro-5-nitropyrimidine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
2-Chloro-5-nitropyrimidine Chemical Properties,Usage,Production
Chemical Properties
Light yellow solid
Synthesis
540-80-7
3073-77-6
7447-39-4
10320-42-0
Example 1 Preparation of 2-chloro-5-nitropyrimidine: 5-nitropyrimidin-2-amine (0.98 g, 7 mmol, 1 eq.) was added to a solution of acetonitrile containing anhydrous copper(II) chloride (1.12 g, 8.4 mmol, 1.2 eq.), tert-butyl nitrite (1.24 mL, 10.5 mmol, 1.5 eq.), and MgSO4 (~300 mg) ( 40 mL) solution, and the reaction was stirred at 65-80 °C (bath temperature).After 30 min, the reaction mixture was cooled to room temperature and ether (100 mL) was added. The organic layer was separated and washed sequentially with aqueous 1N HCl (2 x 20 mL), H2O (50 mL) and brine (20 mL). The organic layer was dried over anhydrous Na2SO4 and concentrated under reduced pressure. The crude product was purified by column chromatography (eluent: hexane/ether=3:1) to afford the target product 2-chloro-5-nitropyrimidine as a light yellow solid (0.56 g, 50% yield).
References
[1] Patent: US2003/181465, 2003, A1
2-Chloro-5-nitropyrimidine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Chloro-5-nitropyrimidine manufacturers
- Product
- 2-Chloro-5-nitropyrimidine 10320-42-0
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-22
- Product
- 2-Chloro-5-nitropyrimidine 10320-42-0
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-12-14
- Product
- 2-Chloro-5-nitropyrimidine 10320-42-0
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-12-19