Methyl 6-HydroxypyriMidine-4-carboxylate

Product Name: Methyl 6-HydroxypyriMidine-4-carboxylate
CAS No.: 7399-93-1
Chemical Name: Methyl 6-HydroxypyriMidine-4-carboxylate
Synonyms: Methyl 6-oxo-1,6-dihydropyriMidine-4-carboxylate;methyl4-oxo-1H-pyrimidine-6-carboxylate;METHYL 6-HYDROXYPYRIMIDINE-4-CARBOXYLAT;Methyl 6-HydroxypyriMidine-4-carboxylate;Methyl 6-oxo-3,6-dihydropyriMidine-4-carboxylate;6-Oxo-3,6-dihydro-pyrimidine-4-carboxylic acid methyl ester;Methyl 6-HydroxypyriMidine-4-carboxylate ISO 9001：2015 REACH;4-PyriMidinecarboxylic acid, 1,6-dihydro-6-oxo-, Methyl ester
CBNumber: CB82570769
Molecular Formula: C6H6N2O3
Formula Weight: 154.12
MOL File: 7399-93-1.mol

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Methyl 6-HydroxypyriMidine-4-carboxylate Property

Boiling point:: 263.8±50.0 °C(Predicted)
Density: 1.39±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 6.88±0.40(Predicted)
Appearance: Off-white to light brown Solid

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M323463
Product name: Methyl6-hydroxypyrimidine-4-carboxylate
Packaging: 1g
Price: $215
Updated: 2021/12/16

Usbiological

Product number: 455804
Product name: Methyl 6-hydroxypyrimidine-4-carboxylate
Packaging: 100mg
Price: $312
Updated: 2021/12/16

ChemScene

Product number: CS-W002637
Product name: Methyl6-oxo-1,6-dihydropyrimidine-4-carboxylate
Packaging: 250mg
Price: $57
Updated: 2021/12/16

ChemScene

Product number: CS-W002637
Product name: Methyl6-oxo-1,6-dihydropyrimidine-4-carboxylate
Packaging: 1g
Price: $114
Updated: 2021/12/16

Apolloscientific

Product number: OR904554
Product name: Methyl6-hydroxypyrimidine-4-carboxylate
Purity: 98%
Packaging: 1g
Price: $189
Updated: 2021/12/16

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Methyl 6-HydroxypyriMidine-4-carboxylate Chemical Properties,Usage,Production

Synthesis

67-56-1

6299-87-2

7399-93-1

Step 9A: Synthesis of methyl 6-oxo-1,6-dihydropyrimidine-4-carboxylate. 6-Hydroxy-4-pyrimidinecarboxylic acid (36.0 g, 257 mmol) was dissolved in methanol (360 mL), and chlorotrimethylsilane (56 g, 554 mmol) was slowly added dropwise. The reaction mixture was stirred at room temperature for 8 hours. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure. The residual solid was mixed with 200 mL of methanol and refluxed for 30 minutes. After cooling to room temperature, the precipitated solid was collected by filtration and washed with a small amount of methanol. The product was dried under vacuum at 35 °C to give 27.9 g (70% yield) of methyl 6-oxo-3,6-dihydropyrimidine-4-carboxylate.1H NMR (300 MHz, DMSO-d6) data were as follows: δ (ppm) 12.50 (broad single peak, 1H), 8.23 (single peak, 1H), 6.83 (single peak, 1H), 3.80 (single peak, 3H).

References

[1] Patent: US2009/111821, 2009, A1. Location in patent: Page/Page column 23

Methyl 6-HydroxypyriMidine-4-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 6-HydroxypyriMidine-4-carboxylate Suppliers

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View Lastest Price from Methyl 6-HydroxypyriMidine-4-carboxylate manufacturers

Dideu Industries Group Limited

Product: Methyl 6-HydroxypyriMidine-4-carboxylate 7399-93-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-12-10

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Methyl 6-HydroxypyriMidine-4-carboxylate

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Methyl 6-oxo-3,6-dihydropyriMidine-4-carboxylate

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METHYL 6-HYDROXYPYRIMIDINE-4-CARBOXYLAT

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Methyl 6-HydroxypyriMidine-4-carboxylate ISO 9001：2015 REACH

7399-93-1