ChemicalBook > CAS DataBase List > 3-PYRID-2-YLBENZOIC ACID

3-PYRID-2-YLBENZOIC ACID

Product Name: 3-PYRID-2-YLBENZOIC ACID
CAS No.: 4467-07-6
Chemical Name: 3-PYRID-2-YLBENZOIC ACID
Synonyms: P-013;AKOS BAR-0487;3-Pyridin-2-ylbenzoate;3-(2-pyridinyl)benzoate;2-Pyridyl-3-benzoic acid;3-PYRID-2-YLBENZOIC ACID;3-(2-Pyridyl)benzoic acid;3-(2-PYRIDINYL)BENZOIC ACID;3-PYRIDIN-2-YL-BENZOIC ACID;Benzoic acid, 3-(2-pyridinyl)-
CBNumber: CB9106701
Molecular Formula: C12H9NO2
Formula Weight: 199.21
MOL File: 4467-07-6.mol

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3-PYRID-2-YLBENZOIC ACID Property

Melting point:: 207 °C
Boiling point:: 409.0±28.0 °C(Predicted)
Density: 1.241±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: solid
pka: 3.49±0.10(Predicted)
color: Off-white

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 071823
Product name: 3-Pyridin-2-yl-benzoic acid
Purity: 95+%
Packaging: 1g
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: W6344
Product name: 3-Pyridin-2-yl-benzoicacid
Packaging: 1g
Price: $104
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H58-1-286
Product name: 3-Pyridin-2-ylbenzoic acid
Packaging: 1g
Price: $128
Updated: 2021/12/16

AK Scientific

Product number: W6344
Product name: 3-Pyridin-2-yl-benzoicacid
Packaging: 5g
Price: $284
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H58-1-286
Product name: 3-Pyridin-2-ylbenzoic acid
Packaging: 5G
Price: $368
Updated: 2021/12/16

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3-PYRID-2-YLBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

109-04-6

25487-66-5

4467-07-6

General procedure for the synthesis of 3-(2-pyridyl)benzoic acid from 2-bromopyridine and 3-carboxyphenylboronic acid: to a mixed solution of acetonitrile (40 mL) and water (40 mL) containing 3-carboxyphenylboronic acid (1.66 g, 10 mmol) and 2-bromopyridine (1.72 g, 11 mmol), potassium carbonate (5.5 g, 40 mmol) and bis(triphenylphosphine) palladium(II) chloride (400 mg, 0.37 mmol). The reaction mixture was degassed and displaced three times with nitrogen. Subsequently, the mixture was stirred and reacted at 100 °C for 24 hours. After completion of the reaction, the reaction suspension was filtered while hot and the filtrate was concentrated to half of the original volume. The concentrated aqueous phase was washed with dichloromethane, and then the pH of the aqueous phase was adjusted to 3 with 1 M hydrochloric acid.The precipitated solid was collected by filtration, washed with water, and finally dried under vacuum to give 1.69 g of the white solid product 3-(2-pyridyl)benzoic acid in 85% yield. The product was detected by LC-MS (ESI), m/z: 200 (M + 1)+.

References

[1] Patent: US2009/197863, 2009, A1. Location in patent: Page/Page column 75

3-PYRID-2-YLBENZOIC ACID Preparation Products And Raw materials

Raw materials

3-Tolylboronic acid 2-Bromopyridine Sodium sulfate Sodium chloride Palladium Ethyl acetate Potassium permanganate Sodium hydroxide Dimethyl ether Sulfuric acid Sodium carbonate

Preparation Products

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View Lastest Price from 3-PYRID-2-YLBENZOIC ACID manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 3-(Pyridin-2-yl)benzoic acid 4467-07-6
Price: US $3.00-9.00/kg
Min. Order: 1kg
Purity: 99%min
Supply Ability: 50kg
Release date: 2025-07-28

4467-07-6, 3-PYRID-2-YLBENZOIC ACIDRelated Search:

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3-(2-pyridinyl)benzoate

3-Pyridin-2-yl-benzoic acid 97%

3-(2-PYRIDINYL)BENZOIC ACID

AKOS BAR-0487

3-PYRID-2-YLBENZOIC ACID

3-PYRIDIN-2-YL-BENZOIC ACID

2-Pyridyl-3-benzoic acid

Benzoic acid, 3-(2-pyridinyl)-

3-Pyridin-2-ylbenzoate

3-(3-Chloropyridin-2-yl)benzoic acid

3-(3-Cyanopyridin-2-yl)benzoic acid

3-(3-Fluoropyridin-2-yl)benzoic acid

3-(3-Methoxypyridin-2-yl)benzoic acid

3-(3-Nitropyridin-2-yl)benzoic acid

3-(4-Chloropyridin-2-yl)benoic acid

3-(4-Cyanopyridin-2-yl)benzoic acid

3-(4-Fluoropyridin-2-yl)benzoic acid

3-(4-Nitropyridin-2-yl)benzoic acid

3-(5-Chloropyridin-2-yl)benzoic acid

3-(5-Cyanopyridin-2-yl)benzoic acid

3-(5-Fluoropyridin-2-yl)benoic acid

3-(5-Methoxypyridin-2-yl)benzoic acid

3-(6-Chloropyridin-2-yl)benzoic acid

3-(6-Methoxypyridin-2-yl)benzoic acid

3-PYRIDIN-2-YL-BENZOIC ACID, 95+%

3-(2-Pyridyl)benzoic acid

P-013

4467-07-6

API intermediates