3-PYRID-2-YLBENZOIC ACID
- Product Name
- 3-PYRID-2-YLBENZOIC ACID
- CAS No.
- 4467-07-6
- Chemical Name
- 3-PYRID-2-YLBENZOIC ACID
- Synonyms
- P-013;AKOS BAR-0487;3-Pyridin-2-ylbenzoate;3-(2-pyridinyl)benzoate;2-Pyridyl-3-benzoic acid;3-PYRID-2-YLBENZOIC ACID;3-(2-Pyridyl)benzoic acid;3-(2-PYRIDINYL)BENZOIC ACID;3-PYRIDIN-2-YL-BENZOIC ACID;Benzoic acid, 3-(2-pyridinyl)-
- CBNumber
- CB9106701
- Molecular Formula
- C12H9NO2
- Formula Weight
- 199.21
- MOL File
- 4467-07-6.mol
3-PYRID-2-YLBENZOIC ACID Property
- Melting point:
- 207 °C
- Boiling point:
- 409.0±28.0 °C(Predicted)
- Density
- 1.241±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- pka
- 3.49±0.10(Predicted)
- color
- Off-white
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 071823
- Product name
- 3-Pyridin-2-yl-benzoic acid
- Purity
- 95+%
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- W6344
- Product name
- 3-Pyridin-2-yl-benzoicacid
- Packaging
- 1g
- Price
- $104
- Updated
- 2021/12/16
- Product number
- 4H58-1-286
- Product name
- 3-Pyridin-2-ylbenzoic acid
- Packaging
- 1g
- Price
- $128
- Updated
- 2021/12/16
- Product number
- W6344
- Product name
- 3-Pyridin-2-yl-benzoicacid
- Packaging
- 5g
- Price
- $284
- Updated
- 2021/12/16
- Product number
- 4H58-1-286
- Product name
- 3-Pyridin-2-ylbenzoic acid
- Packaging
- 5G
- Price
- $368
- Updated
- 2021/12/16
3-PYRID-2-YLBENZOIC ACID Chemical Properties,Usage,Production
Synthesis
109-04-6
25487-66-5
4467-07-6
General procedure for the synthesis of 3-(2-pyridyl)benzoic acid from 2-bromopyridine and 3-carboxyphenylboronic acid: to a mixed solution of acetonitrile (40 mL) and water (40 mL) containing 3-carboxyphenylboronic acid (1.66 g, 10 mmol) and 2-bromopyridine (1.72 g, 11 mmol), potassium carbonate (5.5 g, 40 mmol) and bis(triphenylphosphine) palladium(II) chloride (400 mg, 0.37 mmol). The reaction mixture was degassed and displaced three times with nitrogen. Subsequently, the mixture was stirred and reacted at 100 °C for 24 hours. After completion of the reaction, the reaction suspension was filtered while hot and the filtrate was concentrated to half of the original volume. The concentrated aqueous phase was washed with dichloromethane, and then the pH of the aqueous phase was adjusted to 3 with 1 M hydrochloric acid.The precipitated solid was collected by filtration, washed with water, and finally dried under vacuum to give 1.69 g of the white solid product 3-(2-pyridyl)benzoic acid in 85% yield. The product was detected by LC-MS (ESI), m/z: 200 (M + 1)+.
References
[1] Patent: US2009/197863, 2009, A1. Location in patent: Page/Page column 75
3-PYRID-2-YLBENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
3-PYRID-2-YLBENZOIC ACID Suppliers
- Tel
- --
- Fax
- --
- synthesis@chimmed.ru
- Country
- Russia
- ProdList
- 5006
- Advantage
- 81
View Lastest Price from 3-PYRID-2-YLBENZOIC ACID manufacturers
- Product
- 3-(Pyridin-2-yl)benzoic acid 4467-07-6
- Price
- US $3.00-9.00/kg
- Min. Order
- 1kg
- Purity
- 99%min
- Supply Ability
- 50kg
- Release date
- 2025-07-28