tBuXPhos-Pd-G3
- Product Name
- tBuXPhos-Pd-G3
- CAS No.
- 1447963-75-8
- Chemical Name
- tBuXPhos-Pd-G3
- Synonyms
- tBuXPhos Pd G3;ditert-butyl-[2-(2,4,6-triisopropylphenyl)phenyl]phosphane;tBuXPhos Pd G3 97%;[(2-Di-tert-butylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)-2-(2′-amino-1,1′-biphenyl)] palladium(II) methanesulfonate;tBuXPhos Palladacycle Gen.3;tBuXPhos Pd G3 tBuXPhos Pd G3;tBuXPhos Pd G3 95% (dried basis);Methanesulfonato(2-di-t-butylphosphino-2;METHANESULFONATO(2-DI-T-BUTYLPHOSPHINO-2,4,6-TRI-I-PROPYL-1,1-BIPHENY+;Methanesulfonato(2-di-t-butylphosphino-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II)
- CBNumber
- CB92686119
- Molecular Formula
- C42H58NO3PPdS
- Formula Weight
- 794.38
- MOL File
- 1447963-75-8.mol
tBuXPhos-Pd-G3 Property
- Melting point:
- 130-140°C
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- Powder
- color
- yellow
- InChI
- InChI=1S/C29H45P.C12H9N.CH4O3S.Pd/c1-19(2)22-17-24(20(3)4)27(25(18-22)21(5)6)23-15-13-14-16-26(23)30(28(7,8)9)29(10,11)12;13-12-9-5-4-8-11(12)10-6-2-1-3-7-10;1-5(2,3)4;/h13-21H,1-12H3;1-6,8-9,13H;1H3,(H,2,3,4);/q;-2;;+2
- InChIKey
- KKVLHKIBKWORMK-UHFFFAOYSA-N
- SMILES
- P(C1C=CC=CC=1C1C(=CC(C(C)C)=CC=1C(C)C)C(C)C)([Pd+2]1(NC2=CC=CC=C2C2=CC=CC=[C-]12)[O-]S(=O)(=O)C)(C(C)(C)C)C(C)(C)C
Safety
- WGK Germany
- 3
- HS Code
- 2843909000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 762229
- Product name
- tBuXPhos Pd G3
- Purity
- 95% (dried basis)
- Packaging
- 1g
- Price
- $174
- Updated
- 2024/03/01
- Product number
- 762229
- Product name
- tBuXPhos Pd G3
- Purity
- 95% (dried basis)
- Packaging
- 5g
- Price
- $647
- Updated
- 2024/03/01
- Product number
- 46-0323
- Product name
- Methanesulfonato(2-di-t-butylphosphino-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [t-BuXPhos Palladacycle Gen. 3]
- Packaging
- 250mg
- Price
- $50
- Updated
- 2024/03/01
- Product number
- 46-0323
- Product name
- Methanesulfonato(2-di-t-butylphosphino-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [t-BuXPhos Palladacycle Gen. 3]
- Packaging
- 1g
- Price
- $149
- Updated
- 2024/03/01
- Product number
- 762229
- Product name
- tBuXPhos Pd G3
- Purity
- 95% (dried basis)
- Packaging
- 250mg
- Price
- $73.9
- Updated
- 2024/03/01
tBuXPhos-Pd-G3 Chemical Properties,Usage,Production
Physical properties
tBuXPhos-Pd-G3 is in the form of a dark grey crystalline powder.
Uses
tBuXPhos Pd G3 may be used to synthesize 4-cyano-7-azaindole from 4-chloro-7-azaindole by cyanation reaction. It may also be used for the α-arylation reaction of acetate esters at room temperature.
Reactions
Mild palladium-catalyzed cyanation of (hetero)aryl halides and triflates in aqueous media.
General Description
tBuXPhos Pd G3 is a third generation (G3) Buchwald precatalyst. It is air, moisture and thermally-stable and is highly soluble in a wide range of common organic solvents. It has long life in solutions. tBuXPhos Pd G3 is an excellent reagent for Buchwald-Hartwig cross-coupling reaction. Some of its unique features include lower catalyst loadings, shorter reaction time, efficient formation of the active catalytic species and accurate control of ligand: palladium ratio.
storage
tBuXPhos Pd G3 should be stored in an airtight, dry and low temperature.
tBuXPhos-Pd-G3 Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from tBuXPhos-Pd-G3 manufacturers
- Product
- Methanesulfonato(2-di-t-butylphosphino-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II) 1447963-75-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2020-04-17
- Product
- Methanesulfonato(2-di-t-butylphosphino-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II) / tBuXPhos Pd G3 1447963-75-8
- Price
- US $10.00-10.00/g
- Min. Order
- 1g
- Purity
- 0.98
- Supply Ability
- 50kg
- Release date
- 2020-11-27
- Product
- tBuXPhos Pd G3 1447963-75-8
- Price
- US $180.00/KG
- Min. Order
- 1KG
- Purity
- 99
- Supply Ability
- 10000KG
- Release date
- 2020-11-11