ChemicalBook > CAS DataBase List > 3-Bromo-6-methoxy-2-picoline
3-Bromo-6-methoxy-2-picoline
- Product Name
- 3-Bromo-6-methoxy-2-picoline
- CAS No.
- 126717-59-7
- Chemical Name
- 3-Bromo-6-methoxy-2-picoline
- Synonyms
- 3-Bromo-6-methoxypicoline;3-Bromo-6-methoxy-2-methyL;5-Bromo-2-methoxy-6-picoline;2-METHOXY-5-BROMO-6-PICOLINE;3-BROMO-6-METHOXY-2-PICOLINE;2-methoxy-5-bromo-6-methylpyridine;5-Bromo-6-methyl-2-methoxypyridine;3-BROMO-6-METHOXY-2-METHYLPYRIDINE;5-Bromo-2-Methoxy-6-Methylpyridine;2-METHYL-3-BROMO-6-METHOXY PYRIDINE
- CBNumber
- CB9474316
- Molecular Formula
- C7H8BrNO
- Formula Weight
- 202.05
- MOL File
- 126717-59-7.mol
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3-Bromo-6-methoxy-2-picoline Property
- Boiling point:
- 86°C/10mmHg(lit.)
- Density
- 1.468g/mLat 25℃
- refractive index
- n20/D 1.548
- Flash point:
- 106°C
- storage temp.
- 2-8°C
- pka
- 1.76±0.10(Predicted)
- form
- Liquid
- color
- Colorless
- InChI
- InChI=1S/C7H8BrNO/c1-5-6(8)3-4-7(9-5)10-2/h3-4H,1-2H3
- InChIKey
- VWNXCCTWVAQAPL-UHFFFAOYSA-N
- SMILES
- C1(C)=NC(OC)=CC=C1Br
- CAS DataBase Reference
- 126717-59-7(CAS DataBase Reference)
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 758191
- Product name
- 3-Bromo-6-methoxy-2-methylpyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $41.9
- Updated
- 2023/06/20
TCI Chemical
- Product number
- B4460
- Product name
- 3-Bromo-6-methoxy-2-methylpyridine
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $21
- Updated
- 2025/07/31
TCI Chemical
- Product number
- B4460
- Product name
- 3-Bromo-6-methoxy-2-methylpyridine
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $50
- Updated
- 2025/07/31
TRC
- Product number
- B415528
- Product name
- 3-Bromo-6-methoxy-2-methylpyridine
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB33924
- Product name
- 3-Bromo-6-methoxy-2-picoline
- Packaging
- 5G
- Price
- $60
- Updated
- 2021/12/16
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3-Bromo-6-methoxy-2-picoline Chemical Properties,Usage,Production
Synthesis
A mixture of 5-bromo-6-methyl-1H-pyridin- 2-one (5.5 g, 29 mmol), silver carbonate (10.89 g, 39 mmol), iodomethane (13.6 mL, 217 mmol) and chloroform (115 mL) is stirred overnight in the dark at room temperature. Triethylamine (10 mL) is added, and stirring is continued for 1.5 hr. The reaction mixture is filtered through a pad of Hi-Flo, and the filtrate is washed with water (100 mL), dried, filtered and concentrated. The residue is purified by filtration through a pad of silica gel washing with cyclohexane-20percent ethyl acetate. The solvent is concentrated to afford 3-Bromo-6-methoxy-2-picoline (3.7 g, 63percent yield) as an oil.
References
[1] Patent: WO2005/51954, 2005, A2. Location in patent: Page/Page column 39; 40
3-Bromo-6-methoxy-2-picoline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Bromo-6-methoxy-2-picoline manufacturers
Shaanxi Dideu New Materials Co. Ltd
- Product
- 3-Bromo-6-methoxy-2-picoline 126717-59-7
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-29
Henan Fengda Chemical Co., Ltd
- Product
- 5-Bromo-2-methoxy-6-picoline 126717-59-7
- Price
- US $5.00-0.10/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-08
Hebei Zhanyao Biotechnology Co. Ltd
- Product
- 5-Bromo-2-methoxy-6-picoline 126717-59-7
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 Tons
- Release date
- 2021-10-15
126717-59-7, 3-Bromo-6-methoxy-2-picolineRelated Search:
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5-Bromo-2-methylpyridine
2,4,6-Collidine
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2-Methoxypyridine
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4-Methylpyridine
2-Methoxy-6-methylaminopyridine
2-Bromo-6-methoxypyridine
2-Methoxy-5-fluoropyridine
2,6-Lutidine
Azamethiphos
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2-Methoxy-4-methylpyridine