ChemicalBook > CAS DataBase List > 3-Bromo-6-methoxy-2-picoline

3-Bromo-6-methoxy-2-picoline

Product Name
3-Bromo-6-methoxy-2-picoline
CAS No.
126717-59-7
Chemical Name
3-Bromo-6-methoxy-2-picoline
Synonyms
3-Bromo-6-methoxypicoline;3-Bromo-6-methoxy-2-methyL;5-Bromo-2-methoxy-6-picoline;2-METHOXY-5-BROMO-6-PICOLINE;3-BROMO-6-METHOXY-2-PICOLINE;2-methoxy-5-bromo-6-methylpyridine;5-Bromo-6-methyl-2-methoxypyridine;3-BROMO-6-METHOXY-2-METHYLPYRIDINE;5-Bromo-2-Methoxy-6-Methylpyridine;2-METHYL-3-BROMO-6-METHOXY PYRIDINE
CBNumber
CB9474316
Molecular Formula
C7H8BrNO
Formula Weight
202.05
MOL File
126717-59-7.mol
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3-Bromo-6-methoxy-2-picoline Property

Boiling point:
86°C/10mmHg(lit.)
Density 
1.468g/mLat 25℃
refractive index 
n20/D 1.548
Flash point:
106°C
storage temp. 
2-8°C
pka
1.76±0.10(Predicted)
form 
Liquid
color 
Colorless
CAS DataBase Reference
126717-59-7(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
41-22
Safety Statements 
26-39
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
758191
Product name
3-Bromo-6-methoxy-2-methylpyridine
Purity
95%
Packaging
1g
Price
$41.9
Updated
2023/06/20
TCI Chemical
Product number
B4460
Product name
3-Bromo-6-methoxy-2-methylpyridine
Purity
>98.0%(GC)
Packaging
1g
Price
$21
Updated
2024/03/01
TCI Chemical
Product number
B4460
Product name
3-Bromo-6-methoxy-2-methylpyridine
Purity
>98.0%(GC)
Packaging
5g
Price
$50
Updated
2024/03/01
Alfa Aesar
Product number
H61962
Product name
3-Bromo-6-methoxy-2-methylpyridine, 98%
Packaging
5g
Price
$53.6
Updated
2021/12/16
Alfa Aesar
Product number
H61962
Product name
3-Bromo-6-methoxy-2-methylpyridine, 98%
Packaging
1g
Price
$13.8
Updated
2021/12/16
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3-Bromo-6-methoxy-2-picoline Chemical Properties,Usage,Production

Synthesis

A mixture of 5-bromo-6-methyl-1H-pyridin- 2-one (5.5 g, 29 mmol), silver carbonate (10.89 g, 39 mmol), iodomethane (13.6 mL, 217 mmol) and chloroform (115 mL) is stirred overnight in the dark at room temperature. Triethylamine (10 mL) is added, and stirring is continued for 1.5 hr. The reaction mixture is filtered through a pad of Hi-Flo, and the filtrate is washed with water (100 mL), dried, filtered and concentrated. The residue is purified by filtration through a pad of silica gel washing with cyclohexane-20percent ethyl acetate. The solvent is concentrated to afford 3-Bromo-6-methoxy-2-picoline (3.7 g, 63percent yield) as an oil.

3-Bromo-6-methoxy-2-picoline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Bromo-6-methoxy-2-picoline manufacturers

Henan Fengda Chemical Co., Ltd
Product
5-Bromo-2-methoxy-6-picoline 126717-59-7
Price
US $5.00-0.10/KG
Min. Order
1KG
Purity
98%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-08
Hebei Zhanyao Biotechnology Co. Ltd
Product
5-Bromo-2-methoxy-6-picoline 126717-59-7
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 Tons
Release date
2021-10-15
Dideu Industries Group Limited
Product
5-Bromo-2-methoxy-6-picoline 126717-59-7
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-26

126717-59-7, 3-Bromo-6-methoxy-2-picolineRelated Search:


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