ChemicalBook > CAS DataBase List > N-BOC-(R)-1-AMINO-2-PROPANOL

N-BOC-(R)-1-AMINO-2-PROPANOL

Product Name
N-BOC-(R)-1-AMINO-2-PROPANOL
CAS No.
119768-44-4
Chemical Name
N-BOC-(R)-1-AMINO-2-PROPANOL
Synonyms
N-Boc-(R)-isopropanolamine;BOC-(R)-1-AMINO-2-PROPANOL;N-BOC-(R)-1-AMINO-2-PROPANOL;(R)-1-(Boc-amino)-2-propanol;BOC-(R)-(-)-1-AMINO-2-PROPANOL;N-T-BOC-(R)-1-AMINO-2-PROPANOL;N-Boc-(R)-2-hydroxypropanamine;(R)-1-(Boc-amino)-2-propanol, 98%;(R)-tert-Butyl 2-hydroxypropylcarbaMate;tert-butyl (R)-2-hydroxypropylcarbamate
CBNumber
CB0463878
Molecular Formula
C8H17NO3
Formula Weight
175.23
MOL File
119768-44-4.mol
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N-BOC-(R)-1-AMINO-2-PROPANOL Property

Boiling point:
276.4±23.0 °C(Predicted)
Density 
1.025±0.06 g/cm3(Predicted)
refractive index 
1.4460
storage temp. 
2-8°C
pka
12.42±0.46(Predicted)
Appearance
Colorless to light yellow Viscous Liquid
InChI
InChI=1S/C8H17NO3/c1-6(10)5-9-7(11)12-8(2,3)4/h6,10H,5H2,1-4H3,(H,9,11)/t6-/m1/s1
InChIKey
YNJCFDAODGKHAV-ZCFIWIBFSA-N
SMILES
C(OC(C)(C)C)(=O)NC[C@H](O)C
CAS DataBase Reference
119768-44-4
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Safety

HS Code 
2924297099
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
AAA0001661
Product name
N-T-BOC-(R)-1-AMINO-2-PROPANOL
Purity
95.00%
Packaging
1G
Price
$190.05
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB50601
Product name
Boc-(R)-1-amino-2-propanol
Packaging
10g
Price
$128
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB50601
Product name
Boc-(R)-1-amino-2-propanol
Packaging
1g
Price
$45
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB50601
Product name
Boc-(R)-1-amino-2-propanol
Packaging
2g
Price
$64
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB50601
Product name
Boc-(R)-1-amino-2-propanol
Packaging
5G
Price
$80
Updated
2021/12/16
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N-BOC-(R)-1-AMINO-2-PROPANOL Chemical Properties,Usage,Production

Chemical Properties

Clear colorless liquid

Synthesis

24424-99-5

78-96-6

95656-86-3

Step 1: 1-Amino-2-propanol (compound 42.1; 3.53 g, 47.0 mmol) and triethylamine (25 mL) were dissolved in methanol (35 mL) under nitrogen protection. Subsequently, a solution of di-tert-butyl dicarbonate (10.3 g, 47.0 mmol) in methanol (15 mL) was added slowly and dropwise. The reaction mixture was stirred overnight at room temperature. Upon completion of the reaction, the mixture was concentrated and the residue was dried under high vacuum to give 8.23 g (quantitative yield) of clear oily product. This oily product was dissolved in tetrahydrofuran (100 mL) and triethylamine (13.1 mL, 94.0 mmol) was added. Methanesulfonyl chloride (3.82 mL, 49.3 mmol) was added dropwise to this solution at 0 °C. After 1 h of reaction, the mixture was diluted with ethyl acetate and washed sequentially with 1 M aqueous hydrochloric acid, aqueous sodium bicarbonate and brine. The organic phase was dried with anhydrous sodium sulfate and concentrated to give 10.5 g (88% yield) of a clear oily product (compound 42.2), which solidified on standing. Electrospray mass spectrometry (ES(+)MS) showed m/e = 254 ([M+H]+).

References

[1] Journal of Organic Chemistry, 2000, vol. 65, # 20, p. 6368 - 6380
[2] Patent: US2006/35908, 2006, A1. Location in patent: Page/Page column 108
[3] Patent: US2015/197493, 2015, A1. Location in patent: Paragraph 0744; 0745; 0746
[4] Patent: WO2014/173928, 2014, A1. Location in patent: Page/Page column 52; 53
[5] Patent: WO2006/104356, 2006, A1. Location in patent: Page/Page column 27

N-BOC-(R)-1-AMINO-2-PROPANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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N-BOC-(R)-1-AMINO-2-PROPANOL Suppliers

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View Lastest Price from N-BOC-(R)-1-AMINO-2-PROPANOL manufacturers

Career Henan Chemical Co
Product
N-BOC-(R)-1-AMINO-2-PROPANOL 119768-44-4
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-03

119768-44-4, N-BOC-(R)-1-AMINO-2-PROPANOLRelated Search:

tert-Butyl (2R,3S)-(-)-6-oxo-2,3-diphenyl-4-morpholinecarboxylate BOC-HYP(BZL)-OH Boc-Thr(Bzl)-OH Boc-Hyp-OH N-Boc-trans-4-Hydroxy-L-proline methyl ester BOC-THR(ME)-OH Boc-L-Threonine BOC-(R)-2-AMINO-1-PROPANOL BOC-(S)-2-AMINO-1-PROPANOL 1-(BOC-AMINO)-2-PROPANOL BOC-THR(P-CHLORO-BZL)-OH DCHA (2S,3R)-3-(BOC-AMINO)-2-HYDROXY-4-(4-NITROPHENYL)BUTYRIC ACID BOC-THR(BZL)-ONP BOC-EPI-STATINE BOC-HYP-OH DCHA BOC-HYP-OBZL BOC-THR-OH DCHA N-BOC-(2S,3R)-2-HYDROXY-3-AMINO-4-PHENYLBUTANOIC ACID

  • N-T-BOC-(R)-1-AMINO-2-PROPANOL
  • N-BOC-(R)-1-AMINO-2-PROPANOL
  • BOC-(R)-(-)-1-AMINO-2-PROPANOL
  • BOC-(R)-1-AMINO-2-PROPANOL
  • Carbamic acid, [(2R)-2-hydroxypropyl]-, 1,1-dimethylethyl ester (9CI)
  • (R)-tert-Butyl 2-hydroxypropylcarbaMate
  • (R)-1-(Boc-amino)-2-propanol, 98%
  • N-Boc-(R)-2-hydroxypropanamine
  • tert-butyl [(2R)-2-hydroxypropyl]carbamate
  • Boc-(R)-1-amino-2-propanol≥ 99% (Assay, Chiral purity)
  • N-Boc-(R)-isopropanolamine
  • tert-Butyl (R)-2-hydroxy-1-propylcarbamate
  • tert-butyl N-[(2R)-2-hydroxypropyl]carbamate
  • Carbamic acid, N-[(2R)-2-hydroxypropyl]-, 1,1-dimethylethyl ester
  • tert-butyl (R)-2-hydroxypropylcarbamate
  • N-[(R)-2-Hydroxypropyl]carbamic acid tert-butyl ester
  • (R)-1-(Boc-amino)-2-propanol
  • 119768-44-4
  • N-BOC