1-Bromo-3-fluoro-5-nitrobenzene

Product Name: 1-Bromo-3-fluoro-5-nitrobenzene
CAS No.: 7087-65-2
Chemical Name: 1-Bromo-3-fluoro-5-nitrobenzene
Synonyms: 3-Bromo-5-fluoroaniline;1-Bromo-3-fluoro-5-nitrobenzene;5-AMINO-1-BROMO-3-FLUOROBENZENE;3-Bromo-5-fluoronitrobenzene 97%;Benzene, 1-bromo-3-fluoro-5-nitro-;1-Bromo-3-fluoro-5-nitrobenzene,98%;1-Bromo-3-fluoro-5-nitrobenzene, 97%;1-Bromo-3-fluoro-5-nitrobenzene ISO 9001：2015 REACH
CBNumber: CB0775539
Molecular Formula: C6H3BrFNO2
Formula Weight: 220
MOL File: 7087-65-2.mol

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1-Bromo-3-fluoro-5-nitrobenzene Property

Boiling point:: 247.2±20.0 °C(Predicted)
Density: 1.808±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: Liquid
color: Yellow
CAS DataBase Reference: 7087-65-2

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Safety

RIDADR: UN2810
HazardClass: 6.1
HS Code: 2904990090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H331Toxic if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: B688643
Product name: 1-Bromo-3-fluoro-5-nitrobenzene
Packaging: 250mg
Price: $55
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-B-Y3
Product name: 3-Bromo-5-fluoronitrobenzene
Packaging: 1g
Price: $14
Updated: 2021/12/16

Matrix Scientific

Product number: 074506
Product name: 1-Bromo-3-fluoro-5-nitrobenzene
Purity: 95+%
Packaging: 1g
Price: $14
Updated: 2021/12/16

ChemScene

Product number: CS-W007693
Product name: 1-Bromo-3-fluoro-5-nitrobenzene
Purity: 98.18%
Packaging: 5g
Price: $42
Updated: 2021/12/16

Matrix Scientific

Product number: 074506
Product name: 1-Bromo-3-fluoro-5-nitrobenzene
Purity: 95+%
Packaging: 5g
Price: $51
Updated: 2021/12/16

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1-Bromo-3-fluoro-5-nitrobenzene Chemical Properties,Usage,Production

Synthesis

10472-88-5

7087-65-2

General procedure for the synthesis of 1-bromo-3-fluoro-5-nitrobenzene from 2-bromo-4-fluoro-6-nitroaniline: To a solution of 2-bromo-4-fluoro-6-nitroaniline (702 mg, 3 mmol) in ethanol (3 mL) was added 6 mL of 60% sulphuric acid at 0 °C, followed by the slow addition of sodium nitrite (414 mg, 6 mmol) in batches. After addition, stirring was continued for 1 hour while maintaining the reaction temperature at 0-5 °C. Subsequently, ferrous sulfate heptahydrate (4.38 g, 6 mmol) was added and the resulting mixture was continued to be stirred for 3 hours. After completion of the reaction, the mixture was concentrated, water was added and the aqueous phase was extracted with dichloromethane (20 mL x 3). The organic layers were combined, washed with brine (20 mL), dried over anhydrous sodium sulfate, filtered and concentrated. The residue was purified by preparative thin layer chromatography (TLC) with the eluent dichloromethane/methanol = 60/1 to afford the target product 1-bromo-3-fluoro-5-nitrobenzene (yellow solid, 448 mg, 68% yield).

References

[1] Patent: WO2016/161145, 2016, A1. Location in patent: Paragraph 00704
[2] Journal of Antibiotics, 1994, vol. 47, # 12, p. 1456 - 1465
[3] Bioorganic and Medicinal Chemistry Letters, 1998, vol. 8, # 23, p. 3397 - 3402
[4] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 11, p. 3243 - 3247

1-Bromo-3-fluoro-5-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Bromo-3-fluoro-5-nitrobenzene Suppliers

Canada 1 China 114 Germany 1 India 2 United Kingdom 4 United States 9 Global 131

Accela ChemBio Inc.

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View Lastest Price from 1-Bromo-3-fluoro-5-nitrobenzene manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 1-Bromo-3-fluoro-5-nitrobenzene 7087-65-2
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-12-10

Career Henan Chemical Co

Product: 2-Bromo-4-methylbenzoic acid 7087-65-2
Price: US $3.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-09

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7087-65-2

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