ChemicalBook > CAS DataBase List > 4-Iodo-2-nitroanisole

4-Iodo-2-nitroanisole

Product Name: 4-Iodo-2-nitroanisole
CAS No.: 52692-09-8
Chemical Name: 4-Iodo-2-nitroanisole
Synonyms: 4-IODO-2-NITROANISOLE;4-iodo-1-methoxy-2-nitrobenzene;Benzene, 4-iodo-1-methoxy-2-nitro-
CBNumber: CB3213674
Molecular Formula: C7H6INO3
Formula Weight: 279.03
MOL File: 52692-09-8.mol

Less

4-Iodo-2-nitroanisole Property

Melting point:: 96-98°C
Boiling point:: 330.8±27.0 °C(Predicted)
Density: 1.893±0.06 g/cm3(Predicted)
storage temp.: 2-8°C, protect from light
Appearance: Light yellow to yellow Solid
Sensitive: Light Sensitive

Less

Safety

Risk Statements: 23/24/25
Safety Statements: 36/37-45
HS Code: 2909309090

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

Less

N-Bromosuccinimide Price

TRC

Product number: I715735
Product name: 4-Iodo-2-nitroanisole
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: I715735
Product name: 4-Iodo-2-nitroanisole
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 119934
Product name: 4-Iodo-1-methoxy-2-nitrobenzene
Purity: 95+%
Packaging: 1g
Price: $72
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-H-15
Product name: 4-Iodo-2-nitroanisole
Packaging: 1g
Price: $116
Updated: 2021/12/16

AK Scientific

Product number: X5312
Product name: 4-Iodo-2-nitroanisole
Packaging: 5g
Price: $188
Updated: 2021/12/16

Less

4-Iodo-2-nitroanisole Chemical Properties,Usage,Production

Synthesis Reference(s)

Tetrahedron Letters, 10, p. 2427, 1969 DOI: 10.1017/S0009838800024678

Synthesis

91-23-6

52692-09-8

General procedure for the synthesis of 4-iodo-2-nitroanisole from 2-nitroanisole: To a stirred solution of 2-nitroanisole (1 mmol) in dichloromethane (CH2Cl2) or 1,2-dichloroethane ((CH2Cl)2) (0.1 M) was added sequentially Ph3PAuNTf2 (0.025 mmol, 19 mg; if using the 2:1 complex of Ph3PAuNTf2 with toluene) and N-iodosuccinimide (NIS, 1.1 mmol, 248 mg). The reaction mixture was stirred at room temperature or reacted under reflux conditions until complete conversion of the feedstock was confirmed by thin layer chromatography (TLC) monitoring. Upon completion of the reaction, the solvent was evaporated under reduced pressure and the resulting crude product was purified by fast column chromatography using different ratios of hexane and ethyl acetate (EtOAc) as eluents, resulting in pure 4-iodo-2-nitroanisole.

References

[1] Synlett, 2014, vol. 25, # 3, p. 399 - 402
[2] Journal of Organic Chemistry, 1990, vol. 55, # 11, p. 3552 - 3555
[3] Tetrahedron, 2004, vol. 60, # 41, p. 9113 - 9119
[4] Synthetic Communications, 2007, vol. 37, # 8, p. 1259 - 1265
[5] Synthesis, 2006, # 7, p. 1195 - 1199

4-Iodo-2-nitroanisole Preparation Products And Raw materials

Raw materials

Preparation Products

Less

4-Iodo-2-nitroanisole Suppliers

China 74 Germany 2 India 7 Switzerland 1 United Kingdom 3 United States 8 Global 95

Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
ProdList: 30123
Advantage: 84

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Adamas Reagent, Ltd.

Tel: 400-6009262 16621234537
Fax: 021-64823266
Email: chenyj@titansci.com
Country: China
ProdList: 14101
Advantage: 59

Shanghai Longsheng chemical Co.,Ltd.

Tel: 021-58099652-8005 13585536065
Fax: 021-58099609
Email: bin.wu@shlschem.com
Country: China
ProdList: 9883
Advantage: 59

Shandong Xiya Chemical Co., Ltd

Tel: 4009903999 13355009207
Fax: 0539-6365991
Email: 3007715519@qq.com
Country: China
ProdList: 18729
Advantage: 57

Shanghai Topbiochem Technology Co., Ltd

Tel: 021-58170097
Email: info@topbiochem.com
Country: China
ProdList: 9510
Advantage: 58

Candia Thamtech Company Limited

Tel: 0371-86615086 18203638366 0371-86159066 13526786601
Fax: 0371-86159066
Country: China
ProdList: 2015
Advantage: 60

Shanghai Aladdin Bio-Chem Technology Co.,LTD

Tel: 400-6206333 13167063860
Fax: 021-50323701
Email: anhua.mao@aladdin-e.com
Country: China
ProdList: 25003
Advantage: 65

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Shanghai Xingui Biotechnology Co., Ltd.

Tel: 15121041756
Email: xingui2022@126.com
Country: China
ProdList: 9979
Advantage: 58

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Nanjing Chalf-Pharm Technology Co., Ltd.

Tel: 025-57018978 18251899859
Fax: 025-57018008
Email: sales@chalf-pharm.com
Country: China
ProdList: 5674
Advantage: 50

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

AN PharmaTech Co Ltd

Tel: 86(21)68097365
Fax: 86(21)33321566
Email: sales@anpharma.net
Country: China
ProdList: 4891
Advantage: 55

Changzhou Anxuan Chemical, Co., Ltd.

Tel: 13912302692 13912302692;
Fax: 0519-88064678
Email: sales@anxuanchem.com
Country: China
ProdList: 4828
Advantage: 58

Shanghai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847; 18021002903
Fax: QQ:3008007432
Email: 3008007409@qq.com
Country: China
ProdList: 71826
Advantage: 60

Changzhou Hopschain Chemical Co.,Ltd.

Tel: 0519-85528066 13775048983
Fax: 0519-85528066
Email: sales@hopschem.com
Country: China
ProdList: 31553
Advantage: 55

Chengdu Huachun Technology Co., Ltd

Tel: 400-1166-196 15982826727
Fax: QQ：800101999
Email: cdhxsj@163.com
Country: China
ProdList: 14603
Advantage: 60

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Yantai ShengKailun Chemical Technology Co., Ltd.

Tel: 13356901049
Fax: QQ：1025383091
Email: 3119594100@qq.com
Country: China
ProdList: 7964
Advantage: 55

Shanghai CR Corporation Limited

Tel: 13062833949; 4006653949 4006653949
Fax: QQ: 2136646215
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 9757
Advantage: 58

Guangzhou Jhd Chemical Reagent Co., Ltd.

Tel: 020-84383047
Fax: 020-84380294
Email: sales@jhd.com.cn
Country: China
ProdList: 9186
Advantage: 65

Chemtarget Technologies Co., Ltd

Tel: 0816-2541516 13548425599
Fax: +86-816-2538509
Email: 626079707@qq.com
Country: China
ProdList: 163
Advantage: 58

Shanghai Zhen Li Biological Technology Co., Ltd

Tel: 021-16621358918; 18516310516
Fax: 13045646768
Email: zhenlipharma888@163.com
Country: China
ProdList: 19035
Advantage: 58

Aikon International Limited

Tel: 025-58859352 18068836627
Fax: 02557626880
Email: sales01@aikonchem.com
Country: China
ProdList: 15083
Advantage: 58

SHANGHAI FDC-CHEMICAL CO.,LTD

Tel: 021-61469567 13482353728
Fax: 021-61161605
Email: sales@fdc-chemical.com
Country: China
ProdList: 9717
Advantage: 58

Qingdao Sanrenxing Chemical Co., Ltd.

Tel: 18505321860
Fax: 18505321860
Email: qdsrxchem@163.com
Country: China
ProdList: 327
Advantage: 58

Shanghai SPAR pharmaceutical technology co., LTD

Tel: 021-000000 13917643586;
Email: admin@jingshipharmatech.com
Country: China
ProdList: 9856
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Xinyi Kaiwu Chemical Technology Co., Ltd.

Tel: 0516-0516-88997009 18651776937
Email: 4164357@qq.com
Country: China
ProdList: 3204
Advantage: 58

Henan Lien Chemical Products Co., Ltd.

Tel: 03716091-9097 13383857418
Fax: 03716091-9097
Email: 1520689222@qq.com
Country: China
ProdList: 4862
Advantage: 58

Hefei TNJ Chemical Industry Co.,Ltd.

Tel: +86-0551-65418671 +8618949823763
Fax: 0551-65418697
Email: sales@tnjchem.com
Country: China
ProdList: 34563
Advantage: 58

Dayang Chem (Hangzhou) Co.,Ltd.

Tel: +86-0571-88938639 +8617705817739
Fax: +86-571-88938652，+86-571- 88492614
Email: info@dycnchem.com
Country: China
ProdList: 52846
Advantage: 58

HUNAN CHEMFISH SCIENTIFIC CO.,LTD

Tel: +86-0731-85567275 13298656710
Fax: QQ:3554193828
Email: sales05@chemfish.com
Country: China
ProdList: 7448
Advantage: 58

Shanghai Lanle Bird Industrial Co., Ltd.

Tel: 15021845385
Email: 765325601@qq.com
Country: China
ProdList: 3609
Advantage: 58

Zhengzhou Edward Biology Co.,Ltd

Tel: 0371-63682289 15538176268
Fax: QQ：1875164801
Email: jacschem@163.com
Country: China
ProdList: 9926
Advantage: 58

CONIER CHEM AND PHARMA LIMITED

Tel: +8618523575427
Email: sales@conier.com
Country: China
ProdList: 49975
Advantage: 58

career henan chemical co

Tel: +86-0371-86658258 +8613203830695
Fax: 0086-371-86658258
Email: factory@coreychem.com
Country: China
ProdList: 29798
Advantage: 58

Fuxin Pharmaceutical

Tel: +86-021-021-50872116 +8613122107989
Email: contact@fuxinpharm.com
Country: China
ProdList: 10000
Advantage: 58

Taizhou Nanfeng Pharmaceutical Research Institute

Tel: nanfengdrug@163.com; 18616377689
Email: nanfengdrug@163.com
Country: China
ProdList: 20009
Advantage: 58

Changzhou Kechem Bio-Scientific Co., LTD.

Tel: 0519-68985668 13685222090
Fax: qq735434464
Email: sales@kechem.cn
Country: China
ProdList: 26028
Advantage: 58

Zhengzhou Convergence Chemical Co. LTD

Tel: 0371-0371-53736046 13393710386
Fax: QQ:2853979814
Email: 2853979814@qq.com
Country: China
ProdList: 9947
Advantage: 58

Shanghai Hongju Pharmaceutical Technology Co., LTD

Tel: 18001895509
Fax: QQ2934193566;
Email: 986383309@qq.com
Country: China
ProdList: 2680
Advantage: 58

Shandong Territorial sea Biological Technology Co., LTD

Tel: 15092083467
Email: 18660263263@163.com
Country: China
ProdList: 2810
Advantage: 58

Ningbo jinuo chemical co., LTD

Tel: 0574-87314919 057487319282
Email: info@nbinno.com
Country: China
ProdList: 7047
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39665
Advantage: 58

Jiaxing Zhejia Biotechnology Co., LTD

Tel: 0573-85609002 18367600069;
Email: zhejia01@163.com
Country: China
ProdList: 8886
Advantage: 58

Dongyang Qiusuo Medical Technology Co., LTD

Tel: 17502510579
Email: 2785299132@qq.com
Country: China
ProdList: 1558
Advantage: 58

Yantai Sheng Kai Lun Biological Products Co. , Ltd.

Tel: 13356901049
Email: mark@sklnchem.cn
Country: China
ProdList: 7998
Advantage: 58

Less

View Lastest Price from 4-Iodo-2-nitroanisole manufacturers

Career Henan Chemical Co

Product: 4-Iodo-2-nitroanisole 52692-09-8
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: G/KG/T
Release date: 2019-12-24

52692-09-8, 4-Iodo-2-nitroanisoleRelated Search:

4-Iodoanisole 4-Methyl-2-nitroanisole 4-Nitrobenzoic acid Sodium 3-nitrobenzenesulphonate 1-Chloro-3-nitrobenzene 1,3-Dinitrobenzene 3-Nitroanisole Nitrobenzene 4-Nitroanisole 5-IODO-2-METHOXYANILINE 2-IODO-4-NITROANISOLE 4-IODO-3-NITROANISOLE,4-Iodo-3-Nitroanisole 3-Nitro-4-Iodoanisole,4-IODO-3-NITROANISOLE, 98+% 2-IODO-5-NITROANISOLE 97%,2-IODO-5-NITROANISOLE 3-IODO-4-NITROANISOLE 2-Iodo-3-nitroanisole 4-IODO-2-NITROPHENOL 4-Iodo-2-nitroanisole Methoxy

4-IODO-2-NITROANISOLE

4-iodo-1-methoxy-2-nitrobenzene

Benzene, 4-iodo-1-methoxy-2-nitro-

52692-09-8