1-Bromoisoquinoline
- Product Name
- 1-Bromoisoquinoline
- CAS No.
- 1532-71-4
- Chemical Name
- 1-Bromoisoquinoline
- Synonyms
- 1-BROMOISOQUINOLINE;Isoquinoline, 1-broMo-;1-Bromoisoquinoline >1-Bromoisoquinoline 95%;1-BROMOISOQUINOLINE, 95+%;1-Bromoisoquinoline, White to amber;1-Bromoisoquinoline ISO 9001：2015 REACH;Carbamicacid,N-(2-bromoethyl)-N-methyl-,1,4-dimethylethylester;Isoquinoline, 1-broMo- Superlist NaMe：1-broMoisoquinoline
- CBNumber
- CB3711660
- Molecular Formula
- C9H6BrN
- Formula Weight
- 208.05
- MOL File
- 1532-71-4.mol
1-Bromoisoquinoline Property
- Melting point:
- 42.0 to 46.0 °C
- Boiling point:
- 316.3±15.0 °C(Predicted)
- Density
- 1.564±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- Low Melting Solid
- pka
- 2.03±0.30(Predicted)
- color
- Light yellow to light brown
- CAS DataBase Reference
- 1532-71-4(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H315Causes skin irritation
H318Causes serious eye damage
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 716510
- Product name
- 1-Bromoisoquinoline
- Purity
- 95%
- Packaging
- 1g
- Price
- $127
- Updated
- 2022/05/15
- Product number
- B3445
- Product name
- 1-Bromoisoquinoline
- Purity
- >98.0%(T)
- Packaging
- 1g
- Price
- $193
- Updated
- 2025/07/31
- Product number
- B3445
- Product name
- 1-Bromoisoquinoline
- Purity
- >98.0%(T)
- Packaging
- 5g
- Price
- $578
- Updated
- 2025/07/31
- Product number
- B686923
- Product name
- 1-Bromoisoquinoline
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR59454
- Product name
- 1-Bromoisoquinoline
- Packaging
- 1g
- Price
- $95
- Updated
- 2021/12/16
1-Bromoisoquinoline Chemical Properties,Usage,Production
Chemical Properties
Ligt yellow to light brown low melting solid
Synthesis
1532-72-5
1532-71-4
General method: To a stirred solution of isoquinoline-N-oxide (0.1 M in anhydrous CH2Cl2), POBr3 (1.2 eq.) was slowly added under argon protection at 0 °C, followed by dropwise addition of DMF (0.5 eq.). The reaction mixture was gradually warmed to 25 °C and stirred continuously until the reaction was complete (monitored by TLC). Upon completion of the reaction, saturated aqueous sodium carbonate solution was slowly added and the pH was adjusted to 7-8. The organic and aqueous phases were separated and the aqueous phase was fully extracted with CH2Cl2. All organic phases were combined, washed with brine, dried with anhydrous Na2SO4, filtered and concentrated under reduced pressure to obtain the crude product. The crude product was purified by fast column chromatography with the eluent of petroleum ether/ethyl acetate (100:1).
References
[1] Organic Letters, 2015, vol. 17, # 12, p. 2948 - 2951
[2] Organic Letters, 2013, vol. 15, # 4, p. 792 - 795
[3] Tetrahedron, 2016, vol. 72, # 38, p. 5762 - 5768
[4] Organic Letters, 2016, vol. 18, # 9, p. 1956 - 1959
1-Bromoisoquinoline Preparation Products And Raw materials
Raw materials
Preparation Products
1-Bromoisoquinoline Suppliers
- Tel
- 320-37350700
- Fax
- +32 (0)37350701
- sales@tcieurope.eu
- Country
- Europe
- ProdList
- 23671
- Advantage
- 75
- Tel
- --
- Fax
- --
- Sales@kemikalieimport.dk
- Country
- Europe
- ProdList
- 6685
- Advantage
- 47
View Lastest Price from 1-Bromoisoquinoline manufacturers
- Product
- 1-Bromoisoquinoline 1532-71-4
- Price
- US $9.80/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 tons
- Release date
- 2024-11-28
- Product
- 1-Bromoisoquinoline 1532-71-4
- Price
- US $8.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10tons
- Release date
- 2018-12-25