Methyl 3-bromo-5-iodobenzoate
- Product Name
- Methyl 3-bromo-5-iodobenzoate
- CAS No.
- 188813-07-2
- Chemical Name
- Methyl 3-bromo-5-iodobenzoate
- Synonyms
- Methyl 5-bromo-3-iodobenzoate;Methyl3-bromo-5-iodobenzoate97%;Methyl 3-bromo-5-iodobenzoate 97%;Benzoic acid, 3-bromo-5-iodo-, meth;3-BroMo-5-iodobenzoic acid Methyl ester;Benzoic acid,3-broMo-5-iodo-, Methyl ester
- CBNumber
- CB61106462
- Molecular Formula
- C8H6BrIO2
- Formula Weight
- 340.94
- MOL File
- 188813-07-2.mol
Methyl 3-bromo-5-iodobenzoate Property
- Melting point:
- 62.0-63.0 °C
- Boiling point:
- 334.5±32.0 °C(Predicted)
- Density
- 2.059±0.06 g/cm3(Predicted)
- storage temp.
- RT, protect from light
- form
- Powder
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2916399090
N-Bromosuccinimide Price
- Product number
- M296580
- Product name
- Methyl3-Bromo-5-iodobenzoate
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FB67313
- Product name
- 3-Bromo-5-iodobenzoic acid methyl ester
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- CS-0044963
- Product name
- Methyl3-bromo-5-iodobenzoate
- Packaging
- 1g
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB67313
- Product name
- 3-Bromo-5-iodobenzoic acid methyl ester
- Packaging
- 1g
- Price
- $95
- Updated
- 2021/12/16
- Product number
- OR17113
- Product name
- Methyl3-bromo-5-iodobenzoate
- Purity
- 97%
- Packaging
- 1g
- Price
- $145
- Updated
- 2021/12/16
Methyl 3-bromo-5-iodobenzoate Chemical Properties,Usage,Production
Synthesis
188815-32-9
74-88-4
188813-07-2
(a) Synthesis of methyl 3-bromo-5-iodobenzoate: In a dry reaction flask, 3-bromo-5-iodobenzoic acid (15 g, 45.9 mmol) was dissolved in a solvent mixture of tetrahydrofuran (20 mL) and N,N-dimethylformamide (75 mL). Sodium carbonate (9.7 g, 92 mmol) and iodomethane (5.7 mL, 92 mmol) were then added. The reaction mixture was stirred at room temperature for 20 hours. After completion of the reaction, most of the solvent was removed by concentration under reduced pressure. The residue was extracted with ethyl acetate and washed sequentially with water, saturated aqueous sodium bicarbonate solution and brine. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the title compound methyl 3-bromo-5-iodobenzoate. Yield: 15 g (99% yield).
References
[1] Patent: WO2010/103279, 2010, A1. Location in patent: Page/Page column 126
[2] Patent: WO2010/103297, 2010, A2. Location in patent: Page/Page column 71
Methyl 3-bromo-5-iodobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 3-bromo-5-iodobenzoate manufacturers
- Product
- methyl 3-bromo-5-iodobenzoate 188813-07-2
- Price
- US $0.00/kg
- Min. Order
- 20kg
- Purity
- 99%
- Supply Ability
- 20 tons
- Release date
- 2025-04-07
- Product
- Methyl 3-bromo-5-iodobenzoate 188813-07-2
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 2000kg
- Release date
- 2023-06-09
- Product
- Methyl 3-bromo-5-iodobenzoate 188813-07-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-31