Description References
ChemicalBook > CAS DataBase List > 4-Iodoanisole

4-Iodoanisole

Description References
Product Name
4-Iodoanisole
CAS No.
696-62-8
Chemical Name
4-Iodoanisole
Synonyms
1-IODO-4-METHOXYBENZENE;P-IODOANISOLE;4-IODOANISOL;Isoform;p-iodoanisol;4-IODANISOLE;4-lodoanisole;4-METHOXYIODOBENZENE;CREM-α;4-iodoether
CBNumber
CB6450614
Molecular Formula
C7H7IO
Formula Weight
234.03
MOL File
696-62-8.mol
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4-Iodoanisole Property

Melting point:
50-53 °C(lit.)
Boiling point:
237 °C726 mm Hg(lit.)
Density 
1.7904 (estimate)
Flash point:
>230 °F
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
Soluble in ethanol, ether, chloroform.
form 
Crystalline Powder and Chunks
color 
Off-white to brown
Sensitive 
Light Sensitive
BRN 
1906692
InChIKey
SYSZENVIJHPFNL-UHFFFAOYSA-N
CAS DataBase Reference
696-62-8(CAS DataBase Reference)
NIST Chemistry Reference
Benzene, 1-iodo-4-methoxy-(696-62-8)
EPA Substance Registry System
Benzene, 1-iodo-4-methoxy- (696-62-8)
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38
Safety Statements 
26-36-24/25
WGK Germany 
3
F 
8
TSCA 
Yes
HS Code 
29093090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
I7608
Product name
4-Iodoanisole
Purity
98%
Packaging
25g
Price
$46.8
Updated
2024/03/01
Sigma-Aldrich
Product number
I7608
Product name
4-Iodoanisole
Purity
98%
Packaging
100g
Price
$140
Updated
2024/03/01
TCI Chemical
Product number
I0378
Product name
4-Iodoanisole
Purity
>99.0%(GC)
Packaging
25g
Price
$30
Updated
2024/03/01
TCI Chemical
Product number
I0378
Product name
4-Iodoanisole
Purity
>99.0%(GC)
Packaging
100g
Price
$82
Updated
2024/03/01
Alfa Aesar
Product number
A12144
Product name
4-Iodoanisole, 98+%
Packaging
25g
Price
$34.1
Updated
2024/03/01
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4-Iodoanisole Chemical Properties,Usage,Production

Description

4-Iodoanisole (chemical formula: C7H7IO) is an organic compound being soluble in ethanol, ether and chloroform. It has a wide range of medicals industrial applications. For example, it can be used as human and animal nutrition products, antiseptics, disinfectants, pharmaceutical intermediates, polarizing films for liquid crystal display (LCD) chemicals. Its iodine derivatives can also be used as organic building blocks and analytic reagents.

References

https://www.fishersci.pt/shop/products/4-iodoanisole-98-7/11480113

Chemical Properties

off-white to brown crystalline powder and chunks. Melting point 51-52 ℃, boiling point 237 ℃ (96.8kPa). Soluble in organic solvents such as alcohol and ether, but insoluble in water. Iodine can be easily separated and analyzed by light.

Uses

4-Iodoanisole is used in wide range of medicals industrial applications as well as in human and animal nutrition products, pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals. Iodine derivatives are also used as organic building blocks, analytical reagents.

Preparation

4-Iodoanisole is synthesized by the reaction of anisole with iodine chloride. Add anisole to glacial acetic acid, stir and slowly add iodine chloride. After the addition was completed, the temperature was refluxed for 3.5h. Cool, pour into ice water, and precipitate p-iodoanisole. After it was separated, the free iodine was washed with 5% sodium sulfite, then washed with water, distilled under reduced pressure, and the fractions with a boiling point of 140-160 °C (5.33 kPa) were collected and cooled to 0 °C for filtration. Wash with methanol and recrystallize to obtain the finished product.

Definition

ChEBI: (alpha-D-mannosyl)7-beta-D-mannosyl-diacetylchitobiosyl-L-asparagine, isoform B (protein) is a member of methoxybenzenes.

Synthesis Reference(s)

The Journal of Organic Chemistry, 58, p. 2058, 1993 DOI: 10.1021/jo00060a020
Tetrahedron Letters, 27, p. 3497, 1986 DOI: 10.1016/S0040-4039(00)84832-7

Purification Methods

Crystallise 4-iodoanisole from aqueous EtOH and/or distil it under vacuum. [Beilstein 6 H 208, 6 I 109, 6 II 199, 6 III 744, 6 IV 1075.]

4-Iodoanisole Preparation Products And Raw materials

Raw materials

Sodium sulfite Iodine monochloride Dimethyl ether

Preparation Products

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4-Iodoanisole Suppliers

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View Lastest Price from 4-Iodoanisole manufacturers

Hebei Mujin Biotechnology Co.,Ltd
Product
4-Iodoanisole 696-62-8
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-09-06
Hebei Weibang Biotechnology Co., Ltd
Product
4-Iodoanisole 696-62-8
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-01
R&D Scientific Inc.
Product
4-Iodoanisole 696-62-8
Price
US $397.00/Kg
Min. Order
1Kg
Purity
98
Supply Ability
500 Kg
Release date
2024-05-12

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