ChemicalBook > CAS DataBase List > Boc-Glycine hydrazide

Boc-Glycine hydrazide

Product Name
Boc-Glycine hydrazide
CAS No.
6926-09-6
Chemical Name
Boc-Glycine hydrazide
Synonyms
BUTTPARK 77\04-08;BOC-GLYCINE HYDRAZIDE;Boc-Glycinehydrazide8%;Boc-Glycinehydrazide，98%;Butoxycarbonylglycine hydrazide;Boc-Glycine hydrazide USP/EP/BP;N-TERT-BUTOXYCARBONYLGLYCYLHYDRAZIDE;tert-Butyl (2-hydrazinyl-2-oxoethyl);2-Aminoacetohydrazide, 2-BOC protected;tert-butyl (2-hydrazino-2-oxoethyl)carbamate
CBNumber
CB9323340
Molecular Formula
C7H15N3O3
Formula Weight
189.21
MOL File
6926-09-6.mol
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Boc-Glycine hydrazide Property

Melting point:
111-115
Boiling point:
386.5±25.0 °C(Predicted)
Density 
1.139±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
solid
pka
11.40±0.46(Predicted)
color 
Beige
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
22
HazardClass 
IRRITANT
HS Code 
2928009090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
B809885
Product name
tert-ButylN-(2-Hydrazinyl-2-oxoethyl)carbamate
Packaging
50mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
E007
Product name
Boc-Glycinehydrazide
Packaging
1g
Price
$47
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB38781
Product name
Boc-glycine hydrazide
Packaging
2g
Price
$60
Updated
2021/12/16
Apolloscientific
Product number
OR2444
Product name
2-Aminoacetohydrazide,2-BOCprotected
Packaging
1g
Price
$83
Updated
2021/12/16
SynQuest Laboratories
Product number
4158-1-X1
Product name
N-tert-butoxycarbonylglycylhydrazide
Packaging
1g
Price
$92
Updated
2021/12/16
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Boc-Glycine hydrazide Chemical Properties,Usage,Production

Uses

Boc-Glycine hydrazide is used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis


N-Protected Hydrazides 2a-l; General Procedure The protected amino acid 1 (2 equiv) and EDAC (2 equiv) were dissolved in the minimum amount of CH2Cl2 at 0 ??C. The mixture was stirred at 0 ??C for 2 h. PhthNNH2 (1 equiv) was added and the mixture was stirred at 0 ??C for 1 h and then at r.t. overnight. Distillation of the solvent under reduced pressure gave a product which was dissolved in EtOAc and washed successively with 1 M KHSO4, sat. aq NaHCO3, and brine. The organic layer was then dried (Na2SO4), filtered, and concentrated in vacuo. The residue was precipitated with Et2O to yield compound 2. If necessary, the residue was purified by column chromatography (silica gel, hexane- EtOAc, 3:7 to 7:3). Compounds 4a-l; General Procedure Aminomethylated polystyrene resin (3 equiv; 1.1 mmol/g, 100-200 mesh) was conditioned for 10 min at r.t. in CH2Cl2. Then 2 (1 equiv) was added, and the mixture was slowly stirred for 24 h at r.t. The mixture was filtered and the solvent was evaporated in vacuo to give product 4. Compound 4h, yield 89%.

Boc-Glycine hydrazide Preparation Products And Raw materials

Raw materials

Preparation Products

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Boc-Glycine hydrazide Suppliers

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6926-09-6, Boc-Glycine hydrazideRelated Search:

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  • BOC-GLYCINE HYDRAZIDE
  • BUTTPARK 77\04-08
  • N-TERT-BUTOXYCARBONYLGLYCYLHYDRAZIDE
  • Butoxycarbonylglycine hydrazide
  • 2-Aminoacetohydrazide, 2-BOC protected
  • tert-Butyl (2-hydrazino-2-oxoethyl)carbamate, 2-[(tert-Butoxycarbonyl)amino]acetohydrazide
  • HydrazinocarbonylMethyl-carbaMic acid tert-butyl ester, 95%+
  • tert-butyl (2-hydrazino-2-oxoethyl)carbamate
  • tert-butyl N-(2-hydrazino-2-oxo-ethyl)carbamate
  • tert-butyl N-(2-hydrazinyl-2-oxoethyl)carbamate
  • tert-butyl N-(2-hydrazinyl-2-oxo-ethyl)carbamate
  • tert-Butyl (2-hydrazinyl-2-oxoethyl)
  • tert-butyl N-[(hydrazinecarbonyl)methyl]carbamate
  • Boc-Glycinehydrazide8%
  • N-(2-hydrazino-2-keto-ethyl)carbamic acid tert-butyl ester
  • N-(2-hydrazino-2-oxoethyl)carbamic acid tert-butyl ester
  • Boc-Glycinehydrazide，98%
  • Hydrazinocarbonylmethyl-carbamic acid tert-butyl ester
  • Glycine, N-[(1,1-dimethylethoxy)carbonyl]-, hydrazide
  • ert-butylN-(2-hydrazinyl-2-oxoethyl)carbamate
  • Boc-Glycine hydrazide USP/EP/BP
  • 6926-09-6
  • 926-09-6
  • 6926/9/6