Boc-Glycine hydrazide

Product Name: Boc-Glycine hydrazide
CAS No.: 6926-09-6
Chemical Name: Boc-Glycine hydrazide
Synonyms: BUTTPARK 77\04-08;BOC-GLYCINE HYDRAZIDE;Boc-Glycinehydrazide8%;Boc-Glycinehydrazide，98%;Butoxycarbonylglycine hydrazide;Boc-Glycine hydrazide USP/EP/BP;N-TERT-BUTOXYCARBONYLGLYCYLHYDRAZIDE;tert-Butyl (2-hydrazinyl-2-oxoethyl);2-Aminoacetohydrazide, 2-BOC protected;tert-butyl (2-hydrazino-2-oxoethyl)carbamate
CBNumber: CB9323340
Molecular Formula: C7H15N3O3
Formula Weight: 189.21
MOL File: 6926-09-6.mol

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Boc-Glycine hydrazide Property

Melting point:: 111-115
Boiling point:: 386.5±25.0 °C(Predicted)
Density: 1.139±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 11.40±0.46(Predicted)
color: Beige

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
HazardClass: IRRITANT
HS Code: 2928009090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B809885
Product name: tert-ButylN-(2-Hydrazinyl-2-oxoethyl)carbamate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: E007
Product name: Boc-Glycinehydrazide
Packaging: 1g
Price: $47
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB38781
Product name: Boc-glycine hydrazide
Packaging: 2g
Price: $60
Updated: 2021/12/16

Apolloscientific

Product number: OR2444
Product name: 2-Aminoacetohydrazide,2-BOCprotected
Packaging: 1g
Price: $83
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4158-1-X1
Product name: N-tert-butoxycarbonylglycylhydrazide
Packaging: 1g
Price: $92
Updated: 2021/12/16

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Boc-Glycine hydrazide Chemical Properties,Usage,Production

Uses

Boc-Glycine hydrazide is used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis

N-Protected Hydrazides 2a-l; General Procedure The protected amino acid 1 (2 equiv) and EDAC (2 equiv) were dissolved in the minimum amount of CH2Cl2 at 0 ??C. The mixture was stirred at 0 ??C for 2 h. PhthNNH2 (1 equiv) was added and the mixture was stirred at 0 ??C for 1 h and then at r.t. overnight. Distillation of the solvent under reduced pressure gave a product which was dissolved in EtOAc and washed successively with 1 M KHSO4, sat. aq NaHCO3, and brine. The organic layer was then dried (Na2SO4), filtered, and concentrated in vacuo. The residue was precipitated with Et2O to yield compound 2. If necessary, the residue was purified by column chromatography (silica gel, hexane- EtOAc, 3:7 to 7:3). Compounds 4a-l; General Procedure Aminomethylated polystyrene resin (3 equiv; 1.1 mmol/g, 100-200 mesh) was conditioned for 10 min at r.t. in CH2Cl2. Then 2 (1 equiv) was added, and the mixture was slowly stirred for 24 h at r.t. The mixture was filtered and the solvent was evaporated in vacuo to give product 4. Compound 4h, yield 89%.

Boc-Glycine hydrazide Preparation Products And Raw materials

Raw materials

Preparation Products

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Boc-Glycine hydrazide Suppliers

China 92 Germany 1 India 1 United Kingdom 6 United States 13 Global 113

Jinan Liheng Biotechnology Co., Ltd.

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BOC-GLYCINE HYDRAZIDE

BUTTPARK 77\04-08

N-TERT-BUTOXYCARBONYLGLYCYLHYDRAZIDE

Butoxycarbonylglycine hydrazide

2-Aminoacetohydrazide, 2-BOC protected

tert-Butyl (2-hydrazino-2-oxoethyl)carbamate, 2-[(tert-Butoxycarbonyl)amino]acetohydrazide

HydrazinocarbonylMethyl-carbaMic acid tert-butyl ester, 95%+

tert-butyl (2-hydrazino-2-oxoethyl)carbamate

tert-butyl N-(2-hydrazino-2-oxo-ethyl)carbamate

tert-butyl N-(2-hydrazinyl-2-oxoethyl)carbamate

tert-butyl N-(2-hydrazinyl-2-oxo-ethyl)carbamate

tert-Butyl (2-hydrazinyl-2-oxoethyl)

tert-butyl N-[(hydrazinecarbonyl)methyl]carbamate

Boc-Glycinehydrazide8%

N-(2-hydrazino-2-keto-ethyl)carbamic acid tert-butyl ester

N-(2-hydrazino-2-oxoethyl)carbamic acid tert-butyl ester

Boc-Glycinehydrazide，98%

Hydrazinocarbonylmethyl-carbamic acid tert-butyl ester

Glycine, N-[(1,1-dimethylethoxy)carbonyl]-, hydrazide

ert-butylN-(2-hydrazinyl-2-oxoethyl)carbamate

Boc-Glycine hydrazide USP/EP/BP

6926-09-6

926-09-6

6926/9/6