3-Cyanopyridine

Product Name: 3-Cyanopyridine
CAS No.: 100-54-9
Chemical Name: 3-Cyanopyridine
Synonyms: NICOTINONITRILE;3-PYRIDINECARBONITRILE;Pyridine-3-carbonitrile;3-Azabenzonitrile;BETA-CYANOPYRIDINE;NICOTINIC ACID NITRILE;3-CYANOPYRIDINE;b-Cyanopyridine;3-Cyjanopirydyna;AKOS BBS-00004487
CBNumber: CB9852589
Molecular Formula: C6H4N2
Formula Weight: 104.11
MOL File: 100-54-9.mol

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3-Cyanopyridine Property

Melting point:: 48-52 °C(lit.)
Boiling point:: 201 °C(lit.)
Density: 1.159
refractive index: 1.5242 (estimate)
Flash point:: 184 °F
storage temp.: Inert atmosphere,Room Temperature
solubility: 140g/l
form: Crystalline Mass, Crystals or Chunks
pka: pK1:1.45(+1) (25°C)
color: Colorless or white to yellow
Water Solubility: 140 g/L (20 ºC)
BRN: 107711
Exposure limits: NIOSH: IDLH 25 mg/m3
Stability:: Incompatible with strong oxidizing agents, strong reducing agents, strong acids, strong bases.
InChIKey: GZPHSAQLYPIAIN-UHFFFAOYSA-N
CAS DataBase Reference: 100-54-9(CAS DataBase Reference)
NIST Chemistry Reference: 3-Pyridinecarbonitrile(100-54-9)
EPA Substance Registry System: 3-Pyridinecarbonitrile (100-54-9)

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Safety

Hazard Codes: Xn
Risk Statements: 22-36/37/38
Safety Statements: 22-24/25-36/37/39-26
WGK Germany: 3
RTECS: QT3030000
TSCA: Yes
HS Code: 29333999
Hazardous Substances Data: 100-54-9(Hazardous Substances Data)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: C94807
Product name: 3-Pyridinecarbonitrile
Purity: 98%
Packaging: 5g
Price: $50.8
Updated: 2024/03/01

Sigma-Aldrich

Product number: C94807
Product name: 3-Pyridinecarbonitrile
Purity: 98%
Packaging: 100g
Price: $55.3
Updated: 2024/03/01

TCI Chemical

Product number: C0456
Product name: 3-Cyanopyridine
Purity: >98.0%(GC)
Packaging: 25g
Price: $20
Updated: 2024/03/01

TCI Chemical

Product number: C0456
Product name: 3-Cyanopyridine
Purity: >98.0%(GC)
Packaging: 500g
Price: $69
Updated: 2024/03/01

Alfa Aesar

Product number: A14850
Product name: 3-Cyanopyridine, 98%
Packaging: 100g
Price: $33.8
Updated: 2024/03/01

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3-Cyanopyridine Chemical Properties,Usage,Production

Chemical Properties

white to beige solid

Chemical Properties

The cyanopyridines are as follows: 2-cyano-: A white to tan liquid or solid. Almond odor. Boiling point=2213℃ ; freezing/melting point=27℃ ; flash point=89℃ . 3-cyano-: a colorless liquid or gray crystal- line solid.

Uses

3-Cyanopyridine is used in the preparation of arylthiazolines and arylimidazolines via dibromodimethylhydantoin-catalyzed condensation of aryl nitriles with ethylene diamine or aminoethanethiol.

Definition

ChEBI: A nitrile that is pyridine substituted by a cyano group at position 3.

Synthesis Reference(s)

Tetrahedron Letters, 29, p. 2155, 1988 DOI: 10.1016/S0040-4039(00)86697-6

Potential Exposure

Limits in Air NIOSH IDLH525 mg/m3 NIOSH REL: (nitriles) 2 ppm, Ceiling Concentration, not to be exceeded in any 15-minute work period.

Shipping

UN3276 Nitriles, liquid, toxic, n.o.s., Hazard Class: 6.1; Labels: 6.1-Poisonous materials, Technical Name Required, Potential Inhalation Hazard (Special Provision 5).

Purification Methods

It is recrystallised to constant melting point from o-xylene/hexane. [Beilstein 22/2 V 115.]

Incompatibilities

Oxidizing agents, such as perchlorates, peroxides, and permanganates. Nitriles may polymerize in the presence of metals and some metal compounds. They are incompatible with acids; mixing nitriles with strong oxidizing acids can lead to extremely violent reactions. Nitriles are generally incompatible with other oxidizing agents such as peroxides and epoxides. The combination of bases and nitriles can produce hydrogen cyanide. Nitriles are hydrolyzed in both aqueous acid and base to give car- boxylic acids (or salts of carboxylic acids). These reactions generate heat. Peroxides convert nitriles to amides. Nitriles can react vigorously with reducing agents. Acetonitrile and propionitrile are soluble in water, but nitriles higher than propionitrile have low aqueous solubility. They are also insoluble in aqueous acids .

Toxics Screening Level

The Initial Threshold Screening Level (ITSL) for 3-cyanopyridine (also known as nicotinonitrile) is 1.5 μg/m3 with annual averaging time.

3-Cyanopyridine Preparation Products And Raw materials

Raw materials

Nicotinamide N-PHENYL-1-NAPHTHYLAMINE HYDROBROMIDE 4-Chlorobenzaldehyde

Preparation Products

Nicotinic acid 3-(TERT-BUTOXYCARBONYLAMINO-METHYL)-PYRIDINE-2-CARBOXYLIC ACID Nicotinamide 2-(3-PYRIDYL)-1,3-THIAZOLE-4-CARBOXYLIC ACID 3-[(N-(TERT-BUTYLOXYCARBONYL)AMINO)METHYL]PYRIDINE 3-(Aminomethyl)pyridine 3-CYANOPYRIDIN-4-YLBORONIC ACID 3-PYRIDINECARBOXAMIDINE 3-AMINOMETHYL-PYRIDINE-2-CARBOXYLIC ACID 2-chloro-5-cyanopyridine 3-AMIDINOPYRIDINIUM CHLORIDE 3-Pyridinecarboxaldehyde ETHYL 4-(TRIFLUOROMETHYL)-2-(PYRIDIN-2-YL)PYRIMIDINE-5-CARBOXYLATE Benzyltriphenylphosphonium chloride 3-Pyridinemethanol 3-PYRIDYLAMIDOXIME 3-(AMINOMETHYL)PYRIDINE 2-(2-PYRIDINYL)-4-(TRIFLUOROMETHYL)-5-PYRIMIDINECARBOXYLIC ACID 3,3'-DIPICOLYLAMINE

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3-Cyanopyridine Suppliers

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View Lastest Price from 3-Cyanopyridine manufacturers

Hebei Zhuanglai Chemical Trading Co.,Ltd

Product: 3-Cyanopyridine 100-54-9
Price: US $30.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 5000kg/week
Release date: 2024-05-28

Hebei Mujin Biotechnology Co.,Ltd

Product: 3-Cyanopyridine 100-54-9
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-07-25

HEBEI SHENGSUAN CHEMICAL INDUSTRY CO.,LTD

Product: 3-Cyanopyridine 100-54-9
Price: US $999.00-666.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 5000
Release date: 2024-08-14

100-54-9, 3-CyanopyridineRelated Search:

ETHYL 2-CYANOACRYLATE Methylene dithiocyanate 3-Cyano-4-methylpyridine 2-Chloro-3-cyanopyridine Sodium cyanoborohydride 3-Aminopyridine Nicotinic acid Nicotinamide NAD+ β-Nicotinamide Mononucleotide PYRIDINE-2-CARBOXAMIDE Nicotinamide-N-oxide Isonicotinamide 2-CYANOPYRIDINE 99%,2-Cyanopyridine, Picolinonitrile 4-Cyanopyridine, Isonicotinic acid nitrile, Isonicotinonitrile ETHYL 2-CHLORO-3-CYANO-6-METHYLISONICOTINATE PYRIDINE-3,4-DICARBONITRILE 5-CYANO-2-METHYLPYRIDINE

NICOTINIC ACID NITRILE

NICOTINONITRILE

NICOTINE ACID NITRILE

SPECS AC-907/25014098

TIMTEC-BB SBB007554

IFLAB-BB F2108-0102

BETA-CYANOPYRIDINE

3-Azabenzonitrile

3-Cyjanopirydyna

AKOS BBS-00004487

3-CYANOPYRIDINE

3-PYRIDINECARBONITRILE

Pyridine-3-carbonitrile

3-PYRIDINECARBONITRILE FOR SYNTHESIS

3-Cyanopyridine, Nicotinic acid nitrile, Nicotinonitrile

3-Cyanopyridine,98%

3-CYANOPYRIDINE CRYSTALLINE

3-Pyridinecarbonitrile,3-Cyanopyridine, Nicotinic acid nitrile, Nicotinonitrile

3-Cyanopyridine, 98% 100GR

3-pyridinecarboxylicacid,nitrile

3-Pyridinenitrile

3-Pyridyl cyanide

3-Pyridylcarbonitrile

b-Cyanopyridine

Nitryl kwasu nikotynowego

nitrylkwasunikotynowego

3-Pyridinecarbonitrile 98%

3-Pyridinecarbonitrile, 99.5%

Nicotinamide Impurity 2(Nicotinamide EP Impurity B)

3-Cyanopyridine/3-Azabenzonitrile

Nicotinic Acid Impurity 3

Isoniazid Impurity C

Nicotinamide EP Impurity B

Cyanopyridine Cyanopyridine

3-Cyanopyridine&gt

Nicorinic acid nitrile

Fampridine Impurity 5 (3-Cyanopyridine)

3-Cyanopyridine, puriss, 98%

Nicotinamide EP Impurity B（3-Cyanopyridine）

100-54-9

Building Blocks

C6

Heterocyclic Building Blocks

Pyridines

Pharmaceutical intermediates

Pyridines derivates

Heterocyclic Compounds

bc0001