2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER
- Product Name
- 2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER
- CAS No.
- 5552-44-3
- Chemical Name
- 2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER
- Synonyms
- Nsc79261;Diethyl isocinchomeronate;ethyl 2,5-pyridinedicarboxylate;DIETHYL 2,5-PYRIDINEDICARBOXYLATE;Diethyl pyridine-2,5-dicarboxylate;Isocinchomeronic acid diethyl ester;2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER;Pyridine-2,5-dicarboxylic acid diethyl ester;2,5-Pyridinedicarboxylic acid, 2,5-diethyl ester;2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER 98+%
- CBNumber
- CB3122828
- Molecular Formula
- C11H13NO4
- Formula Weight
- 223.23
- MOL File
- 5552-44-3.mol
2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER Property
- Melting point:
- 46 °C
- Boiling point:
- 181 °C / 17mmHg
- Density
- 1.165±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- powder to crystal
- pka
- -0.10±0.10(Predicted)
- color
- White to Gray to Brown
Safety
- HS Code
- 2933.39.9200
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- P1094
- Product name
- Diethyl 2,5-Pyridinedicarboxylate
- Purity
- >98.0%(GC)
- Packaging
- 10g
- Price
- $135
- Updated
- 2025/07/31
- Product number
- D476998
- Product name
- DiethylPyridine-2,5-dicarboxylate
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- W6951
- Product name
- Diethylpyridine-2,5-dicarboxylate
- Packaging
- 10g
- Price
- $307
- Updated
- 2021/12/16
- Product number
- CHM0008161
- Product name
- 2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.68
- Updated
- 2021/12/16
- Product number
- JL-11C-003
- Product name
- Pyridine-2,5-dicarboxylicaciddiethylester
- Purity
- 95%+
- Packaging
- 1g
- Price
- $29
- Updated
- 2021/12/16
2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER Chemical Properties,Usage,Production
Synthesis
100-26-5
64-17-5
5552-44-3
Concentrated sulfuric acid (3.9 mL, 71.6 mmol) was slowly added dropwise to a stirred suspension of 2,5-pyridinedicarboxylic acid (3.0 g, 17.9 mmol) in anhydrous ethanol (10 mL) over 15 minutes. Subsequently, the reaction mixture was heated to reflux for 18 hours. Upon completion of the reaction, the solution was cooled to room temperature and the solvent was removed by evaporation under reduced pressure. Saturated sodium bicarbonate (NaHCO3) solution was added to the residue and the pH was adjusted to 7-8. Next, the aqueous phase was extracted with ethyl acetate (EtOAc, 4 x 50 mL). All organic extracts were combined and washed with brine (30 mL) and subsequently dried with anhydrous sodium sulfate (Na2SO4). Finally, the solvent was evaporated under reduced pressure to afford diethyl 2,5-pyridinedicarboxylate (3.0 g, 75% yield), which could be used for subsequent experiments without further purification.
References
[1] Bioorganic and Medicinal Chemistry Letters, 1996, vol. 6, # 24, p. 3025 - 3028
[2] Journal of Porphyrins and Phthalocyanines, 2010, vol. 14, # 6, p. 469 - 480
[3] Dalton Transactions, 2015, vol. 44, # 35, p. 15391 - 15395
[4] European Journal of Organic Chemistry, 2010, # 1, p. 174 - 182
[5] CrystEngComm, 2011, vol. 13, # 8, p. 2915 - 2922
2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER manufacturers
- Product
- 2,5-Pyridinedicarboxylicacid, 2,5-diethyl ester 5552-44-3
- Price
- US $2.00-5.00/KG
- Min. Order
- 0.1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons
- Release date
- 2025-07-10
- Product
- 2,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER 5552-44-3
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08