Ethyl 1-benzylpiperidine-4-carboxylate

Synthesis

Product Name: Ethyl 1-benzylpiperidine-4-carboxylate
CAS No.: 24228-40-8
Chemical Name: Ethyl 1-benzylpiperidine-4-carboxylate
Synonyms: AKOS 225-01;BUTTPARK 33\04-91;RSYY（Avanafil)-28;RARECHEM AH CK 0037;SDCCGMLS-0066147.P001;Ethyl 1-Benzylisonipecotate;Ethyl N-benzylisonipecotate;1-benzyl-ethyl Isonipecotate;Ethyl N-benzylisonipecotinate;1-Benzyl-4-piperidinecarboxyli
CBNumber: CB4276544
Molecular Formula: C15H21NO2
Formula Weight: 247.33
MOL File: 24228-40-8.mol

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Ethyl 1-benzylpiperidine-4-carboxylate Property

Boiling point:: 122°C (0.5 mmHg)
Density: 1.037 g/mL at 25 °C
refractive index: 1.5120-1.5160
Flash point:: >110℃
storage temp.: Inert atmosphere,Room Temperature
solubility: Chloroform (Slightly), Hexanes (Slightly), Methanol (Slightly)
form: clear liquid
pka: 7.93±0.10(Predicted)
color: Colorless to Light red
CAS DataBase Reference: 24228-40-8(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,T
Risk Statements: 36/37/38-25
Safety Statements: 24/25-45
RIDADR: UN 2810 6.1 / PGIII
Hazard Note: Irritant
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Danger
Hazard statements: H301Toxic if swalloed
Precautionary statements: P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TCI Chemical

Product number: E0862
Product name: Ethyl 1-Benzyl-4-piperidinecarboxylate
Purity: >95.0%(GC)(T)
Packaging: 5g
Price: $57
Updated: 2023/06/20

TCI Chemical

Product number: E0862
Product name: Ethyl 1-Benzyl-4-piperidinecarboxylate
Purity: >95.0%(GC)(T)
Packaging: 25g
Price: $203
Updated: 2021/12/16

Alfa Aesar

Product number: H52374
Product name: Ethyl 1-benzylpiperidine-4-carboxylate, 97+%
Packaging: 5g
Price: $87.7
Updated: 2021/12/16

Alfa Aesar

Product number: H52374
Product name: Ethyl 1-benzylpiperidine-4-carboxylate, 97+%
Packaging: 1g
Price: $26.5
Updated: 2021/12/16

Alfa Aesar

Product number: H52374
Product name: Ethyl 1-benzylpiperidine-4-carboxylate, 97+%
Packaging: 250mg
Price: $9.6
Updated: 2021/12/16

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Ethyl 1-benzylpiperidine-4-carboxylate Chemical Properties,Usage,Production

Synthesis

Ethyl isonipecotate (50 g, 0.31 mol) was dissolved in toluene (150 mL) in a round bottom flask, charged with potassium carbonate (60 g, 0.43 mol) and stirred for 15 min. Benzyl chloride (42 g, 0.31 mol) was charged and the reaction mass was refluxed for 4 h at 100 °C. Upon completion of the reaction as marked by TLC (hexane:ethyl acetate; 2:1), the reaction mass was cooled to room temperature and quenched with water (100 mL), stirred and the organic phase was separated. The aqueous phase was again extracted with toluene (100 mL). Combined organic phase was washed twice with saturated brine solution (50 mL). Remove toluene in vacuo to obtain Ethyl N-benzylpiperidine-4-carboxylate ( 6.97 g, 91 %) as a yellow liquid.

Chemical Properties

Colourless Oil

Ethyl 1-benzylpiperidine-4-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethyl 1-benzylpiperidine-4-carboxylate manufacturers

Hebei Kingfiner Technology Development Co.Ltd

Product: Ethyl N-benzylpiperidine-4-carboxylate 24228-40-8
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 50000kg
Release date: 2023-12-12

Wuhan Xinhao Biotechnology Co., Ltd

Product: Ethyl 1-benzylpiperidine-4-carboxylate 24228-40-8
Price: US $10.00-100.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 5000 Metric Ton/Month
Release date: 2024-03-20

Hebei Fengqiang Trading Co., LTD

Product: Ethyl N-benzyl piperidine-4-carboxylate 24228-40-8
Price: US $100.00/bag
Min. Order: 1bag
Purity: 99
Supply Ability: 5000
Release date: 2023-09-11

24228-40-8, Ethyl 1-benzylpiperidine-4-carboxylateRelated Search:

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RARECHEM AH CK 0037

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Ethyl N-benzylpiperidine-4-carboxylate

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Ethyl N-benzyl-4-piperidinecarboxylate

CAS NO.24228-40-8 Ethyl N-benzylpiperidine-4-carboxylate

SDCCGMLS-0066147.P001

Ethyl1-Benzyl-4-piperidinecarboxylate&gt

Ethyl N-benzylisonipecotinate

N-benzyl isonipecotic ethyl ester

N-benzylpiperidine-4-carboxylate, ethyl ester

1-Benzylisonipecotic Acid Ethyl Ester

1-benzyl-ethyl Isonipecotate

1-Benzyl-piperidine-4-carboxylic a

RSYY（Avanafil)-28

Ethyl N-benzylisonipecotate

24228-40-8

24228-04-8

12001-70-3

C24H29NO3HCl

Piperidine

Heterocyclic Compounds

Aromatics

Heterocycles