4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester

Product Name: 4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester
CAS No.: 158407-04-6
Chemical Name: 4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester
Synonyms: tert-Butyl 4-(bromomethyl)piperidine-1-carboxylate;4-BROMOMETHYL-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;1-Boc-4-BromomethyL;1-Boc-4-broMoMethylpiperi...;1-BOC-4-BROMOMETHYLPIPERIDINE;N-BOC-4-BROMOMETHYL-PIPERIDINE;1-N-BOC-4-BROMOMETHYLPIPERIDINE;1-Boc-4-(bromoMmethyl)piperidine;4-Bromomethyl-1-(tert-butoxycarbonyl)piperidine;4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester
CBNumber: CB6404026
Molecular Formula: C11H20BrNO2
Formula Weight: 278.19
MOL File: 158407-04-6.mol

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4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester Property

Boiling point:: 318.3±15.0 °C(Predicted)
Density: 1.270±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: -1.91±0.40(Predicted)
InChIKey: YGJXBTRLYHCWGD-UHFFFAOYSA-N

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Safety

Risk Statements: 36/37/38-36
Safety Statements: 26-36/37/39
WGK Germany: 3
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 796719
Product name: 4-Bromomethyl-piperidine-1-carboxylic acid tert-butyl ester
Purity: 95%
Packaging: 1g
Price: $334
Updated: 2024/03/01

Usbiological

Product number: 265791
Product name: 1-Boc-4-bromomethylpiperidine
Packaging: 500mg
Price: $340
Updated: 2021/12/16

TRC

Product number: T135603
Product name: tert-Butyl4-(Bromomethyl)piperidine-1-carboxylate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB51392
Product name: 1-Boc-4-bromomethylpiperidine
Packaging: 2g
Price: $50
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB51392
Product name: 1-Boc-4-bromomethylpiperidine
Packaging: 25g
Price: $400
Updated: 2021/12/16

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4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester Chemical Properties,Usage,Production

Uses

4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly in laboratory research and development process and chemical production process.

Synthesis

4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester. 4-N-Boc-piperidine-methanol (200 mg, 0.93 mmol) was dissolved in diethyl ether (9 mL) and carbon tetrabromide (370 mg, 1.1 mmol) and PPh3 (292 mg, 1.1 mmol) were added at rt. The reaction was allowed to stir for 18 h at rt and filtered over a pad of celite. The filtrate was concentrated and purified by flash chromatography (hexane/EtOAc, 1:0 ?ú 4:1) to give the title compound. Yield 55 mg. 1 (400 MHz, DMSO-d6) |? ppm 4.02-3.98 (m, 2 H), 3.47 (d, 2 H), 2.78-2.65 (m, 2 H), 1.89-1.74 (m, 3 H), 1.45 (s, 9 H), 1.12-0.98 (m, 2 H).

4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester Suppliers

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View Lastest Price from 4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester manufacturers

Career Henan Chemical Co

Product: 4-BROMOMETHYL-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 158407-04-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2018-12-24

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4-Bromomethylpiperidine-1-carboxylic acid tert-butyl ester 95%

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4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester

158407-04-6

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pharmacetical