ChemicalBook > CAS DataBase List > 4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester

4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester

Product Name
4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester
CAS No.
158407-04-6
Chemical Name
4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester
Synonyms
tert-Butyl 4-(bromomethyl)piperidine-1-carboxylate;4-BROMOMETHYL-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;1-Boc-4-BromomethyL;1-Boc-4-broMoMethylpiperi...;1-BOC-4-BROMOMETHYLPIPERIDINE;N-BOC-4-BROMOMETHYL-PIPERIDINE;1-N-BOC-4-BROMOMETHYLPIPERIDINE;1-Boc-4-(bromoMmethyl)piperidine;4-Bromomethyl-1-(tert-butoxycarbonyl)piperidine;4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester
CBNumber
CB6404026
Molecular Formula
C11H20BrNO2
Formula Weight
278.19
MOL File
158407-04-6.mol
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4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester Property

Boiling point:
318.3±15.0 °C(Predicted)
Density 
1.270±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
form 
solid
pka
-1.91±0.40(Predicted)
InChIKey
YGJXBTRLYHCWGD-UHFFFAOYSA-N
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Safety

Risk Statements 
36/37/38-36
Safety Statements 
26-36/37/39
WGK Germany 
3
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
796719
Product name
4-Bromomethyl-piperidine-1-carboxylic acid tert-butyl ester
Purity
95%
Packaging
1g
Price
$334
Updated
2024/03/01
Usbiological
Product number
265791
Product name
1-Boc-4-bromomethylpiperidine
Packaging
500mg
Price
$340
Updated
2021/12/16
TRC
Product number
T135603
Product name
tert-Butyl4-(Bromomethyl)piperidine-1-carboxylate
Packaging
50mg
Price
$45
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB51392
Product name
1-Boc-4-bromomethylpiperidine
Packaging
2g
Price
$50
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB51392
Product name
1-Boc-4-bromomethylpiperidine
Packaging
25g
Price
$400
Updated
2021/12/16
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4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester Chemical Properties,Usage,Production

Uses

4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly in laboratory research and development process and chemical production process.

Synthesis


4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester. 4-N-Boc-piperidine-methanol (200 mg, 0.93 mmol) was dissolved in diethyl ether (9 mL) and carbon tetrabromide (370 mg, 1.1 mmol) and PPh3 (292 mg, 1.1 mmol) were added at rt. The reaction was allowed to stir for 18 h at rt and filtered over a pad of celite. The filtrate was concentrated and purified by flash chromatography (hexane/EtOAc, 1:0 ?ú 4:1) to give the title compound. Yield 55 mg. 1 (400 MHz, DMSO-d6) |? ppm 4.02-3.98 (m, 2 H), 3.47 (d, 2 H), 2.78-2.65 (m, 2 H), 1.89-1.74 (m, 3 H), 1.45 (s, 9 H), 1.12-0.98 (m, 2 H).

4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester manufacturers

Career Henan Chemical Co
Product
4-BROMOMETHYL-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 158407-04-6
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100KG
Release date
2018-12-24

158407-04-6, 4-Bromomethypiperidine-1-carboxylic acid tert-butyl esterRelated Search:

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  • 1-Piperidinecarboxylic acid, 4-(bromomethyl)-, 1,1-dimethylethyl ester
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  • 4-Bromomethylpiperidine-1-carboxylic acid tert-butyl ester 95%
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  • 4-Bromomethypiperidine-1-carboxylic acid tert-butyl ester
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  • pharmacetical