ChemicalBook > CAS DataBase List > 5-BROMO-2-(METHYLTHIO)PYRIMIDINE
5-BROMO-2-(METHYLTHIO)PYRIMIDINE
- Product Name
- 5-BROMO-2-(METHYLTHIO)PYRIMIDINE
- CAS No.
- 14001-67-3
- Chemical Name
- 5-BROMO-2-(METHYLTHIO)PYRIMIDINE
- Synonyms
- 5-BROMO-2-(METHYLTHIO)PYRIMIDINE;5-BROMO-2-METHYLSULFANYLPYRIMIDINE;2-Methylsulfanyl-5-broMopyriMidine;5-broMo-2-MethylpyriMidine-1-thiol;Pyrimidine, 5-bromo-2-(methylthio)-;5-Bromo-2-(methylthio)pyrimidine ,98%;5-BROMO-2-(METHYLTHIO)PYRIMIDINE ISO 9001：2015 REACH;5-
BroMo- 2- (Methylthio) pyriMidine - CBNumber
- CB8452506
- Molecular Formula
- C5H5BrN2S
- Formula Weight
- 205.08
- MOL File
- 14001-67-3.mol
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5-BROMO-2-(METHYLTHIO)PYRIMIDINE Property
- Melting point:
- 63-68℃
- Boiling point:
- 281.2±13.0 °C(Predicted)
- Density
- 1.72±0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- -0.56±0.22(Predicted)
- form
- Crystalline Powder of Flakes
- color
- White
- InChI
- InChI=1S/C5H5BrN2S/c1-9-5-7-2-4(6)3-8-5/h2-3H,1H3
- InChIKey
- WFLSPLBDSJLPFW-UHFFFAOYSA-N
- SMILES
- C1(SC)=NC=C(Br)C=N1
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Safety
- Hazard Codes
- Xi,Xn,C
- Risk Statements
- 22-34
- Safety Statements
- 26-36/37/39-45
- RIDADR
- UN 1759 8/PG 2
- WGK Germany
- 3
- Hazard Note
- Irritant
- HazardClass
- 8
- PackingGroup
- Ⅱ
- HS Code
- 29335995
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 705896
- Product name
- 5-Bromo-2-(methylthio)pyrimidine
- Purity
- 97%
- Packaging
- 1g
- Price
- $79.7
- Updated
- 2022/05/15
TRC
- Product number
- B697830
- Product name
- 5-Bromo-2-(methylthio)pyrimidine
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
TRC
- Product number
- B697830
- Product name
- 5-Bromo-2-(methylthio)pyrimidine
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 069495
- Product name
- 5-Bromo-2-(methylthio)pyrimidine
- Purity
- 98%
- Packaging
- 5g
- Price
- $78
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB139356
- Product name
- 5-Bromo-2-(methylthio)pyrimidine
- Packaging
- 5G
- Price
- $79
- Updated
- 2021/12/16
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5-BROMO-2-(METHYLTHIO)PYRIMIDINE Chemical Properties,Usage,Production
Synthesis
74-93-1
32779-36-5
14001-67-3
Step 1: Synthesis of 5-bromo-2-methylmercaptopyrimidine To a stirred solution of 5-bromo-2-chloropyrimidine (0.3 g, 1.563 mmol) in dimethylformamide (DMF, 10 mL) was slowly added methyl mercaptan (0.1 mL, 1.563 mmol) at room temperature. The reaction mixture was then heated to 50 °C with continuous stirring for 3 hours. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was quenched by addition of water and extracted with ethyl acetate (EtOAc). The organic phases were combined and dried over anhydrous sodium sulfate (Na2SO4), followed by evaporation of the solvent under reduced pressure to give the crude product. The crude product was purified by silica gel (100-200 mesh) column chromatography using 5% ethyl acetate/hexane as eluent, resulting in purified 5-bromo-2-methylmercaptopyrimidine (0.240 g, 75% yield) as a white solid. Mass spectrometry (MS) analysis showed that [M++1] was 205.1.
References
[1] Patent: US2017/291910, 2017, A1. Location in patent: Paragraph 0496-0498
5-BROMO-2-(METHYLTHIO)PYRIMIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-BROMO-2-(METHYLTHIO)PYRIMIDINE manufacturers
Hebei Zhuanglai Chemical Trading Co Ltd
- Product
- 5-Bromo-2-(methylthio)pyrimidine 14001-67-3
- Price
- US $10.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 ton
- Release date
- 2024-11-13
Shanghai Rlavie Technology Co ltd
- Product
- 5-Bromo-2-(methylthio)pyrimidine 14001-67-3
- Price
- US $0.00-0.00/KG
- Min. Order
- 1g
- Purity
- 98%minHPLC
- Supply Ability
- 100kgs/month
- Release date
- 2021-11-17
Dideu Industries Group Limited
- Product
- 5-BROMO-2-(METHYLTHIO)PYRIMIDINE 14001-67-3
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-12-01
14001-67-3, 5-BROMO-2-(METHYLTHIO)PYRIMIDINERelated Search:
5-Bromo-2-methylpyridine
5-Bromo-2-hydroxymethylpyridine
5-Bromo-2-methoxypyridine
5-BROMO-4-CHLORO-2-METHYLSULFANYL-PYRIMIDINE
4-Bromo-2-(methylthio)pyrimidine
5-BROMO-2-(METHYLTHIO)PYRIMIDINE-4-CARBOXYLIC ACID,5-BROMO-2-(METHYLTHIO)PYRIMIDINE-4-CARB&,5-Bromo-2-(methylthio)pyrimidine-4-carboxylic acid ,97%
Methyl 5-bromo-2-(methylthio)pyrimidine-4-carboxylate ,97%
5-BROMO-2-(METHYLTHIO)PYRIMIDINE
5-BROMO-2-METHANESULFONYL-PYRIMIDINE
6-AMINO-5-BROMO-2-(ETHYLTHIO)PYRIMIDIN-4-OL
5-bromo-2-(methylsulfanyl)pyrimidin-4-ol
4-[(5-BROMOPYRIMIDIN-2-YL)THIO]ANILINE
((5-BROMOPYRIMIDIN-2-YL)THIO)ACETIC ACID
2-[(5-BROMOPYRIMIDIN-2-YL)THIO]ANILINE
IFLAB-BB F2124-0044
5-Bromo-4-methoxy-2-(methylthio)pyrimidine
METHYL [(5-BROMO-4-HYDROXY-6-METHYLPYRIMIDIN-2-YL)THIO]ACETATE
2-(2-thenyl)sulfonyl-5-bromopyrimidine