4-NITRO-PYRIDIN-3-YLAMINE
- Product Name
- 4-NITRO-PYRIDIN-3-YLAMINE
- CAS No.
- 13505-02-7
- Chemical Name
- 4-NITRO-PYRIDIN-3-YLAMINE
- Synonyms
- 4-Nitropyridin-3-amine;4-nitro-3-PyridinaMine;4-NITRO-3-AMINOPYRIDINE;3-AMINO-4-NITROPYRIDINE;3-Pyridinamine, 4-nitro-;4-NITRO-PYRIDIN-3-YLAMINE;3-Amino-4-nitropyridine97%;3-AMINO-4-NITROPYRIDINE 97%;3-Pyridinamine,4-nitro-(9CI);4-NITRO-PYRIDIN-3-YLAMINE ISO 9001：2015 REACH
- CBNumber
- CB2481182
- Molecular Formula
- C5H5N3O2
- Formula Weight
- 139.11
- MOL File
- 13505-02-7.mol
4-NITRO-PYRIDIN-3-YLAMINE Property
- Melting point:
- 138 °C(Solv: water (7732-18-5))
- Boiling point:
- 358.2±22.0 °C(Predicted)
- Density
- 1.437±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 2.25±0.18(Predicted)
- Appearance
- Yellow to orange Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- N901118
- Product name
- 4-Nitro-pyridin-3-ylamine
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- FA148597
- Product name
- 3-Amino-4-nitropyridine
- Packaging
- 50mg
- Price
- $106
- Updated
- 2021/12/16
- Product number
- FA148597
- Product name
- 3-Amino-4-nitropyridine
- Packaging
- 25mg
- Price
- $61
- Updated
- 2021/12/16
- Product number
- FA148597
- Product name
- 3-Amino-4-nitropyridine
- Packaging
- 100mg
- Price
- $185
- Updated
- 2021/12/16
- Product number
- 4H55-1-56
- Product name
- 4-Nitro-pyridin-3-ylamine
- Packaging
- 1g
- Price
- $632
- Updated
- 2021/12/16
4-NITRO-PYRIDIN-3-YLAMINE Chemical Properties,Usage,Production
Synthesis
67-62-9
1122-61-8
7646-85-7
13505-02-7
Example 15: 4-Nitropyridine (124 mg, 1 mmol) and O-methylhydroxylamine (71 mg, 1.5 mmol) were dissolved in N,N-dimethylformamide (DMF, 2 mL) and the resultant solution was added dropwise to a DMF solution containing tert-butanol (3 mL). Potassium tert-butoxide (336 mg, 3 mmol) and zinc(II) chloride (136 mg, 1 mmol) were sequentially added to the reaction system at 25 °C. After the addition was completed, the reaction mixture was stirred at 25 °C for 1 hour. After completion of the reaction, saturated aqueous ammonium chloride solution (50 mL) was added to the mixture and then extracted with ethyl acetate (80 mL). The organic layers were combined, dried with anhydrous magnesium sulfate, filtered and concentrated. The crude product was separated and purified by silica gel thin layer chromatography (eluent: ethyl acetate/hexane=1/1, v/v) to afford 35 mg of 3-amino-4-nitropyridine in 25% yield.
References
[1] Patent: US5648496, 1997, A
4-NITRO-PYRIDIN-3-YLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-NITRO-PYRIDIN-3-YLAMINE manufacturers
- Product
- 4-NITRO-PYRIDIN-3-YLAMINE 13505-02-7
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-09-07
- Product
- 4-NITRO-PYRIDIN-3-YLAMINE 13505-02-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98% HPLC
- Supply Ability
- 10 tons
- Release date
- 2020-02-01