ChemicalBook > CAS DataBase List > 4-NITRO-PYRIDIN-3-YLAMINE

4-NITRO-PYRIDIN-3-YLAMINE

Product Name
4-NITRO-PYRIDIN-3-YLAMINE
CAS No.
13505-02-7
Chemical Name
4-NITRO-PYRIDIN-3-YLAMINE
Synonyms
4-Nitropyridin-3-amine;4-nitro-3-PyridinaMine;4-NITRO-3-AMINOPYRIDINE;3-AMINO-4-NITROPYRIDINE;3-Pyridinamine, 4-nitro-;4-NITRO-PYRIDIN-3-YLAMINE;3-Amino-4-nitropyridine97%;3-AMINO-4-NITROPYRIDINE 97%;3-Pyridinamine,4-nitro-(9CI);4-NITRO-PYRIDIN-3-YLAMINE ISO 9001:2015 REACH
CBNumber
CB2481182
Molecular Formula
C5H5N3O2
Formula Weight
139.11
MOL File
13505-02-7.mol
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4-NITRO-PYRIDIN-3-YLAMINE Property

Melting point:
138 °C(Solv: water (7732-18-5))
Boiling point:
358.2±22.0 °C(Predicted)
Density 
1.437±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
2.25±0.18(Predicted)
Appearance
Yellow to orange Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
N901118
Product name
4-Nitro-pyridin-3-ylamine
Packaging
50mg
Price
$90
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA148597
Product name
3-Amino-4-nitropyridine
Packaging
50mg
Price
$106
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA148597
Product name
3-Amino-4-nitropyridine
Packaging
25mg
Price
$61
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA148597
Product name
3-Amino-4-nitropyridine
Packaging
100mg
Price
$185
Updated
2021/12/16
SynQuest Laboratories
Product number
4H55-1-56
Product name
4-Nitro-pyridin-3-ylamine
Packaging
1g
Price
$632
Updated
2021/12/16
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4-NITRO-PYRIDIN-3-YLAMINE Chemical Properties,Usage,Production

Synthesis

67-62-9

1122-61-8

7646-85-7

13505-02-7

Example 15: 4-Nitropyridine (124 mg, 1 mmol) and O-methylhydroxylamine (71 mg, 1.5 mmol) were dissolved in N,N-dimethylformamide (DMF, 2 mL) and the resultant solution was added dropwise to a DMF solution containing tert-butanol (3 mL). Potassium tert-butoxide (336 mg, 3 mmol) and zinc(II) chloride (136 mg, 1 mmol) were sequentially added to the reaction system at 25 °C. After the addition was completed, the reaction mixture was stirred at 25 °C for 1 hour. After completion of the reaction, saturated aqueous ammonium chloride solution (50 mL) was added to the mixture and then extracted with ethyl acetate (80 mL). The organic layers were combined, dried with anhydrous magnesium sulfate, filtered and concentrated. The crude product was separated and purified by silica gel thin layer chromatography (eluent: ethyl acetate/hexane=1/1, v/v) to afford 35 mg of 3-amino-4-nitropyridine in 25% yield.

References

[1] Patent: US5648496, 1997, A

4-NITRO-PYRIDIN-3-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-NITRO-PYRIDIN-3-YLAMINE Suppliers

A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 4-NITRO-PYRIDIN-3-YLAMINE manufacturers

Dideu Industries Group Limited
Product
4-NITRO-PYRIDIN-3-YLAMINE 13505-02-7
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-07
Career Henan Chemical Co
Product
4-NITRO-PYRIDIN-3-YLAMINE 13505-02-7
Price
US $1.00/KG
Min. Order
1KG
Purity
98% HPLC
Supply Ability
10 tons
Release date
2020-02-01

13505-02-7, 4-NITRO-PYRIDIN-3-YLAMINERelated Search:


  • 3-AMINO-4-NITROPYRIDINE
  • 4-NITRO-PYRIDIN-3-YLAMINE
  • 3-Amino-4-nitropyridine97%
  • 4-NITRO-3-AMINOPYRIDINE
  • 3-Pyridinamine,4-nitro-(9CI)
  • 3-AMINO-4-NITROPYRIDINE 97%
  • 4-Nitropyridin-3-amine
  • 3-Pyridinamine, 4-nitro-
  • 4-nitro-3-PyridinaMine
  • 4-NITRO-PYRIDIN-3-YLAMINE ISO 9001:2015 REACH
  • 13505-02-7
  • Pyridines
  • Pyridine
  • API intermediates
  • NITRO