ChemicalBook > CAS DataBase List > Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)

Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)

Product Name: Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.: 170384-29-9
Chemical Name: Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)
Synonyms: Boc-Gly-Me;Boc-aminoacetone;N-Boc-1-aMinopropan-2-one;1-(Boc-amino)-2-propanone;1-(Boc-amino)-2-oxopropane;tert-Butyl N-acetonylcarbaMate;tert-butyl 2-oxopropylcarbaMate;tert-Butyl-(2-oxopropyl)carbamat;tert-butyl N-(2-oxopropyl)carbaMate;(2-Oxopropyl)carbamic acid tert-butyl ester
CBNumber: CB91057219
Molecular Formula: C8H15NO3
Formula Weight: 173.21
MOL File: 170384-29-9.mol

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Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) Property

Melting point:: 48-49 °C
Boiling point:: 80-85 °C(Press: 0.1 Torr)
Density: 1.018±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
solubility: Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
pka: 11.18±0.46(Predicted)
form: liquid
color: Light yellow
InChI: InChI=1S/C8H15NO3/c1-6(10)5-9-7(11)12-8(2,3)4/h5H2,1-4H3,(H,9,11)
InChIKey: OZGMUQGCAFEQOX-UHFFFAOYSA-N
SMILES: C(OC(C)(C)C)(=O)NCC(=O)C

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

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N-Bromosuccinimide Price

TRC

Product number: O990068
Product name: (2-Oxopropyl)carbamicAcidtert-ButylEster
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Ark Pharm

Product number: AK-25487
Product name: tert-Butyl(2-oxopropyl)carbamate
Purity: 97%
Packaging: 25g
Price: $185
Updated: 2021/12/16

Matrix Scientific

Product number: 072739
Product name: (2-Oxopropyl)carbamic acid tert-butyl ester
Purity: 95+%
Packaging: 5g
Price: $295
Updated: 2021/12/16

AK Scientific

Product number: W3716
Product name: (2-Oxopropyl)carbamicacidtert-butylester
Packaging: 10g
Price: $573
Updated: 2021/12/16

Matrix Scientific

Product number: 072739
Product name: (2-Oxopropyl)carbamic acid tert-butyl ester
Purity: 95+%
Packaging: 1g
Price: $99
Updated: 2021/12/16

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Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) Chemical Properties,Usage,Production

Synthesis

95656-86-3

170384-29-9

General procedure for the synthesis of N-Boc-1-aminoacetone from 1-(Boc-amino)-2-propanol: 1-(Boc-amino)-2-propanol (16.0 g, 92.0 mmol) was slowly added to a solution of pyridinium dichromate (PDC) (68.9 g, 183 mmol) in N,N-dimethylformamide (DMF) (50 mL) at 0 °C. ) to a solution of DMF (42 mL). The reaction mixture was stirred at 0 °C for 16 h and gradually warmed up to 23 °C. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth plug and rinsed with ether (Et2O) solution. Subsequently, the reaction was quenched with brine (200 mL) and diluted with ether (700 mL). The combined ether layers were washed sequentially with aqueous ammonium chloride (2 x 200 mL), water (2 x 200 mL) and brine (2 x 200 mL), dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated to give N-Boc-1-aminoacetone as a yellow oil; Yield: 10.6 g (61.0 mmol, 61% yield).

References

[1] Organic Letters, 2011, vol. 13, # 11, p. 2932 - 2935
[2] Journal of the Chemical Society. Perkin Transactions 1, 2001, # 16, p. 1916 - 1928
[3] Russian Chemical Bulletin, 2005, vol. 54, # 6, p. 1535 - 1536
[4] Synthesis (Germany), 2015, vol. 47, # 18, p. 2756 - 2766
[5] Patent: WO2006/104356, 2006, A1. Location in patent: Page/Page column 27

Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: tert-Butyl-(2-oxopropyl)carbamat 170384-29-9
Price: US $8.80-2.20/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-06-27

Shaanxi Dideu New Materials Co. Ltd

Product: Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) 170384-29-9
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2025-03-20

Career Henan Chemical Co

Product: me: Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) 170384-29-9
Price: US $1.00/KG
Min. Order: 1KG
Purity: 97%-98%
Supply Ability: 200KG
Release date: 2019-09-03

170384-29-9, Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)Related Search:

INDEX NAME NOT YET ASSIGNED N-BOC-3-Aminopiperidine N-BOC-1,2,3,6-TETRAHYDROPYRIDINE N-Boc-4-iodopiperidine tert-Butyl 3-bromopropylcarbamate N-Boc-pyrroline N-Boc-1,2,5,6-tetrahydropyridine-4-boronic acid pinacol ester N-Boc-2-piperidinecarboxylic acid N-Boc-1,4-cyclohexanediamine BOC-L-THIAZOLIDINE-4-CARBOXYLIC ACID 1-Boc-3-piperidinecarboxylic acid 1-Boc-3-cyano-4-oxopyrrolidine PIPERIDIN-3-ONE HYDROCHLORIDE 1-(TERT-BUTOXYCARBONYL)-4-OXOPYRROLIDINE-2-CARBOXYLIC ACID N-Boc-4-oxo-L-proline tert-Butyl 3-oxoazetidine-1-carboxylate N-Boc-4-oxo-L-Proline methyl ester N-Boc-3-pyrrolidinone

Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)

(2-ocopropyl)carbamic acid tert-butyl ester

(2-Oxopropyl)carbamic acid tert-butyl ester

ethyl 3-(tert-butoxycarbonylaMino)-2- oxopropanoate

tert-butyl 2-oxopropylcarbaMate

CarbaMic acid, (2-oxopropyl)-, 1,1-diMethylethyl ester

N-Boc-1-aMinopropan-2-one

tert-butyl N-(2-oxopropyl)carbaMate

tert-Butyl N-acetonylcarbaMate

Boc-aminoacetone

1-(Boc-amino)-2-oxopropane

1-(Boc-amino)-2-propanone

me: Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)

Boc-Gly-Me

Carbamic acid, N-(2-oxopropyl)-, 1,1-dimethylethyl ester

tert-Butyl-(2-oxopropyl)carbamat

170384-29-9

N-BOC