ChemicalBook > CAS DataBase List > 1-(BOC-AMINO)-2-PROPANOL

1-(BOC-AMINO)-2-PROPANOL

Product Name: 1-(BOC-AMINO)-2-PROPANOL
CAS No.: 95656-86-3
Chemical Name: 1-(BOC-AMINO)-2-PROPANOL
Synonyms: 1-(BOC-AMINO)-2-PROPANOL;tert-Butyl (2-hydroxypropyl)carbaMate;1-(tert-Buoxycarbonyamino)-2-propanol;TERT-BUTYL N-(2-HYDROXYPROPYL)CARBAMATE;1-(TERT-BUTOXYCARBONYLAMINO)-2-PROPANOL;tert-ButylN-(2-Hydroxypropyl)carbamate>N-(2-Hydroxypropyl)carbmic acid tert-Butyl ester;N-(2-HYDROXYPROPYL)CARBAMIC ACID TERT-BUTYL ESTER;(2-Hydroxy-propyl)-carbaMic acid tert-butyl ester;tert-Butyl N-(2-Hydroxypropyl)carbamate
CBNumber: CB9452679
Molecular Formula: C8H17NO3
Formula Weight: 175.23
MOL File: 95656-86-3.mol

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1-(BOC-AMINO)-2-PROPANOL Property

Boiling point:: 276.4±23.0 °C(Predicted)
Density: 1.02
refractive index: 1.4450-1.4490
storage temp.: 2-8°C
form: clear liquid
pka: 12.42±0.46(Predicted)
color: Colorless to Light yellow

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Safety

Hazard Codes: T
Risk Statements: 25-41
Safety Statements: 26-39
HS Code: 2924.19.8000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B2418
Product name: tert-Butyl N-(2-Hydroxypropyl)carbamate
Purity: >98.0%(N)
Packaging: 5g
Price: $107
Updated: 2025/07/31

TCI Chemical

Product number: B2418
Product name: tert-Butyl N-(2-Hydroxypropyl)carbamate
Purity: >98.0%(N)
Packaging: 25g
Price: $350
Updated: 2025/07/31

TRC

Product number: B810260
Product name: tert-Butyl N-(2-Hydroxypropyl)carbamate
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 160520
Product name: tert-Butyl (2-hydroxypropyl)carbamate
Packaging: 5g
Price: $160
Updated: 2021/12/16

AK Scientific

Product number: V9633
Product name: tert-Butyl N-(2-Hydroxypropyl)carbamate
Packaging: 5g
Price: $184
Updated: 2021/12/16

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1-(BOC-AMINO)-2-PROPANOL Chemical Properties,Usage,Production

Synthesis

24424-99-5

78-96-6

95656-86-3

Step 1: 1-Amino-2-propanol (compound 42.1; 3.53 g, 47.0 mmol) and triethylamine (25 mL) were dissolved in methanol (35 mL) under nitrogen protection, and a solution of di-tert-butyl dicarbonate (10.3 g, 47.0 mmol) in methanol (15 mL) was slowly added dropwise. The reaction mixture was stirred at room temperature overnight. Subsequently, the reaction solution was concentrated and the residue was dried under high vacuum to give 8.23 g (quantitative yield) of clear oily product. This oily product was dissolved in tetrahydrofuran (100 mL) and triethylamine (13.1 mL, 94.0 mmol) was added. Methanesulfonyl chloride (3.82 mL, 49.3 mmol) was slowly added dropwise to this solution at 0 °C. After 1 hour of reaction, the reaction mixture was diluted with ethyl acetate and washed sequentially with 1 M aqueous hydrochloric acid, aqueous sodium bicarbonate and saturated saline. The organic phase was dried with anhydrous sodium sulfate and concentrated to give 10.5 g (88% yield) of a clear oily substance (compound 42.2), which solidified after standing. Electrospray mass spectrometry (ES(+)MS) showed m/e = 254 ([M+H]+).

References

[1] Journal of Organic Chemistry, 2000, vol. 65, # 20, p. 6368 - 6380
[2] Patent: US2006/35908, 2006, A1. Location in patent: Page/Page column 108
[3] Patent: US2015/197493, 2015, A1. Location in patent: Paragraph 0744; 0745; 0746
[4] Patent: WO2014/173928, 2014, A1. Location in patent: Page/Page column 52; 53
[5] Patent: WO2006/104356, 2006, A1. Location in patent: Page/Page column 27

1-(BOC-AMINO)-2-PROPANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(BOC-AMINO)-2-PROPANOL Suppliers

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View Lastest Price from 1-(BOC-AMINO)-2-PROPANOL manufacturers

Career Henan Chemical Co

Product: 1-(BOC-AMINO)-2-PROPANOL 95656-86-3
Price: US $1.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 200kg
Release date: 2018-12-24

95656-86-3, 1-(BOC-AMINO)-2-PROPANOLRelated Search:

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1-(TERT-BUTOXYCARBONYLAMINO)-2-PROPANOL

1-(BOC-AMINO)-2-PROPANOL

1-(tert-Buoxycarbonyamino)-2-propanol

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(2-Hydroxy-propyl)-carbaMic acid tert-butyl ester

1-(Boc-amino)-2-propanol 1-(tert-Butoxycarbonylamino)-2-propanol N-(2-Hydroxypropyl)carbamic Acid tert-Butyl Ester

tert-Butyl (2-hydroxypropyl)carbaMate

<i>tert</i>-Butyl <i>N</i>-(2-Hydroxypropyl)carbamate

Carbamic acid, (2-hydroxypropyl)-, 1,1-dimethylethyl ester (9CI)

tert-ButylN-(2-Hydroxypropyl)carbamate&gt

Carbamic acid, N-(2-hydroxypropyl)-, 1,1-dimethylethyl ester

95656-86-3

N-BOC