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Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)

Product Name
Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.
170384-29-9
Chemical Name
Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)
Synonyms
Boc-Gly-Me;Boc-aminoacetone;N-Boc-1-aMinopropan-2-one;1-(Boc-amino)-2-propanone;1-(Boc-amino)-2-oxopropane;tert-Butyl N-acetonylcarbaMate;tert-butyl 2-oxopropylcarbaMate;tert-Butyl-(2-oxopropyl)carbamat;tert-butyl N-(2-oxopropyl)carbaMate;(2-Oxopropyl)carbamic acid tert-butyl ester
CBNumber
CB91057219
Molecular Formula
C8H15NO3
Formula Weight
173.21
MOL File
170384-29-9.mol
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Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) Property

Melting point:
48-49 °C
Boiling point:
80-85 °C(Press: 0.1 Torr)
Density 
1.018±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
solubility 
Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
pka
11.18±0.46(Predicted)
form 
liquid
color 
Light yellow
InChI
InChI=1S/C8H15NO3/c1-6(10)5-9-7(11)12-8(2,3)4/h5H2,1-4H3,(H,9,11)
InChIKey
OZGMUQGCAFEQOX-UHFFFAOYSA-N
SMILES
C(OC(C)(C)C)(=O)NCC(=O)C
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Safety

Hazard Codes 
Xn
Risk Statements 
22
HS Code 
2924297099
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

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N-Bromosuccinimide Price

TRC
Product number
O990068
Product name
(2-Oxopropyl)carbamicAcidtert-ButylEster
Packaging
100mg
Price
$60
Updated
2021/12/16
Ark Pharm
Product number
AK-25487
Product name
tert-Butyl(2-oxopropyl)carbamate
Purity
97%
Packaging
25g
Price
$185
Updated
2021/12/16
Matrix Scientific
Product number
072739
Product name
(2-Oxopropyl)carbamic acid tert-butyl ester
Purity
95+%
Packaging
5g
Price
$295
Updated
2021/12/16
AK Scientific
Product number
W3716
Product name
(2-Oxopropyl)carbamicacidtert-butylester
Packaging
10g
Price
$573
Updated
2021/12/16
Matrix Scientific
Product number
072739
Product name
(2-Oxopropyl)carbamic acid tert-butyl ester
Purity
95+%
Packaging
1g
Price
$99
Updated
2021/12/16
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Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) Chemical Properties,Usage,Production

Synthesis

95656-86-3

170384-29-9

General procedure for the synthesis of N-Boc-1-aminoacetone from 1-(Boc-amino)-2-propanol: 1-(Boc-amino)-2-propanol (16.0 g, 92.0 mmol) was slowly added to a solution of pyridinium dichromate (PDC) (68.9 g, 183 mmol) in N,N-dimethylformamide (DMF) (50 mL) at 0 °C. ) to a solution of DMF (42 mL). The reaction mixture was stirred at 0 °C for 16 h and gradually warmed up to 23 °C. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth plug and rinsed with ether (Et2O) solution. Subsequently, the reaction was quenched with brine (200 mL) and diluted with ether (700 mL). The combined ether layers were washed sequentially with aqueous ammonium chloride (2 x 200 mL), water (2 x 200 mL) and brine (2 x 200 mL), dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated to give N-Boc-1-aminoacetone as a yellow oil; Yield: 10.6 g (61.0 mmol, 61% yield).

References

[1] Organic Letters, 2011, vol. 13, # 11, p. 2932 - 2935
[2] Journal of the Chemical Society. Perkin Transactions 1, 2001, # 16, p. 1916 - 1928
[3] Russian Chemical Bulletin, 2005, vol. 54, # 6, p. 1535 - 1536
[4] Synthesis (Germany), 2015, vol. 47, # 18, p. 2756 - 2766
[5] Patent: WO2006/104356, 2006, A1. Location in patent: Page/Page column 27

Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) Suppliers

China 90 Europe 1 India 1 United States 9 Global 101
Suzhou Highfine Biotech Co., Ltd
Tel
0512-69209928 18796809688
Email
zhouyingxiang@highfine.com
Country
China
ProdList
1356
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58
Chongqing Xingcan Pharmaceutical Technology Co., Ltd.
Tel
023-13650506873 19923294409
Email
xingcanyaoye@sina.com
Country
China
ProdList
1604
Advantage
58
Tongchuang Pharma(Suzhou). Co., Ltd.
Tel
0512-63263366 18912765016
Fax
0512-6326 3366
Email
tongtf110@sina.com
Country
China
ProdList
993
Advantage
62
Shanghai Kaiwei Chemical Technology Co., Ltd.
Tel
021-58461859 15821823057
Email
service@aiviche.com
Country
China
ProdList
49312
Advantage
58
Shanghai Chiral Chemicals Inc.
Tel
021-37285021 13472570865
Fax
86-021-51714507
Email
tym7xi@aliyun.com
Country
China
ProdList
308
Advantage
64
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
Advantage
61
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14101
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59
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11035
Advantage
64
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
Shanghai Sunway Pharmaceutical Technology Co., Ltd
Tel
18270980682
Fax
021 51613951
Email
mlcheng@sunwaypharm.cn
Country
China
ProdList
8669
Advantage
57
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View Lastest Price from Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
tert-Butyl-(2-oxopropyl)carbamat 170384-29-9
Price
US $8.80-2.20/kg
Min. Order
1kg
Purity
99%
Supply Ability
100kg
Release date
2025-06-27
Shaanxi Dideu New Materials Co. Ltd
Product
Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) 170384-29-9
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98.0%
Supply Ability
10000KGS
Release date
2025-03-20
Career Henan Chemical Co
Product
me: Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI) 170384-29-9
Price
US $1.00/KG
Min. Order
1KG
Purity
97%-98%
Supply Ability
200KG
Release date
2019-09-03

170384-29-9, Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)Related Search:

INDEX NAME NOT YET ASSIGNED N-BOC-3-Aminopiperidine N-BOC-1,2,3,6-TETRAHYDROPYRIDINE N-Boc-4-iodopiperidine tert-Butyl 3-bromopropylcarbamate N-Boc-pyrroline N-Boc-1,2,5,6-tetrahydropyridine-4-boronic acid pinacol ester N-Boc-2-piperidinecarboxylic acid N-Boc-1,4-cyclohexanediamine BOC-L-THIAZOLIDINE-4-CARBOXYLIC ACID 1-Boc-3-piperidinecarboxylic acid 1-Boc-3-cyano-4-oxopyrrolidine PIPERIDIN-3-ONE HYDROCHLORIDE 1-(TERT-BUTOXYCARBONYL)-4-OXOPYRROLIDINE-2-CARBOXYLIC ACID N-Boc-4-oxo-L-proline tert-Butyl 3-oxoazetidine-1-carboxylate N-Boc-4-oxo-L-Proline methyl ester N-Boc-3-pyrrolidinone

  • Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)
  • (2-ocopropyl)carbamic acid tert-butyl ester
  • (2-Oxopropyl)carbamic acid tert-butyl ester
  • ethyl 3-(tert-butoxycarbonylaMino)-2- oxopropanoate
  • tert-butyl 2-oxopropylcarbaMate
  • CarbaMic acid, (2-oxopropyl)-, 1,1-diMethylethyl ester
  • N-Boc-1-aMinopropan-2-one
  • tert-butyl N-(2-oxopropyl)carbaMate
  • tert-Butyl N-acetonylcarbaMate
  • Boc-aminoacetone
  • 1-(Boc-amino)-2-oxopropane
  • 1-(Boc-amino)-2-propanone
  • me: Carbamic acid, (2-oxopropyl)-, 1,1-dimethylethyl ester (9CI)
  • Boc-Gly-Me
  • Carbamic acid, N-(2-oxopropyl)-, 1,1-dimethylethyl ester
  • tert-Butyl-(2-oxopropyl)carbamat
  • 170384-29-9
  • N-BOC