Organic reagents
From early AD to mid-19 century, people mainly use the natural organic substance (such as animal and plant extracts) for qualitative analysis or quantitative analysis. From the second half of the 19th century to the 1920s, it had begun to appear of artificially synthetic organic reagent such as using potassium acetate xanthan for test of nickel, copper, and molybdenum; using morin for test of aluminum; using diazo coupling reaction for the detection of Nitrite; using α-β-nitroso naphthol for detection of cobalt; using dimethyglyoxime for nickel test.
After the proposal of the special-effects group in the 1930s and the proposal of theoretical analysis of functional groups theory in 1950s, people had carried out large-scale screen of organic reagents in search of special-effects analysis groups for different ions and had successfully synthesized a lot of agents of practical value (such as copper reagents, new copper agent, cadmium reagents, beryllium reagent, thorium reagents, etc.). Before the 1950s, the complex compound, in analytic chemistry, is mainly used in the aspects of the precipitation reaction of a binary chelate for the qualitative detection, precipitate isolation and gravimetric separation and other aspects. In the early 1950s and 1960, it is mainly in the form of complexometric titration. From the beginning of the late 1960s, the main focus has been moved to the photometric analysis. Meanwhile, it has been also developed of chelate organic solvent extraction.
8-hydroxy quinoline, hydrazones, oximes, hydroxamic acids, polyphenols, 1, 10-phenanthroline, phosphorus-oxygen extractant, β- diketones, triphenylmethane acid dye, xanthene dyes and azo dyes and other agents has all been widely studied and applied. On the other hand, the structural theoretical research (such as electronic effects, spatial effects and substituent effects) of the organic reagent can further facilitate the development of new-type organic reagents such as heterocyclic azo reagent. During this period, it has been also developed of monoazo chromotropic acid-type and disazo chromotropic acid-type reagent. During the mid-1970s, the chelating resin and adsorbents have achieved rapid development. Since the 1980s, Chinese researchers of analytical chemistry have made progress in the field of the synthesis and application of asymmetric disazo chromotropic acid.
Organic chemical reagents have wide application in analytic chemistry and are mainly used in solvents, precipitation agents, complexing agents, indicator, coloring reagent and surface active agent, etc. In order to adapt to a variety of analytical needs, sometimes it is required to purify certain reagents. For example, liquid organic reagent is often purified by distillation while solid substance is often purified through crystallization and sublimation. Substance having a high vapor pressure, namely having low purification boiling point and undergoing no decomposition under boiling temperature commonly applied atmospheric distillation; for less volatile and water-insoluble substance, namely having high purification point or undergoing decomposition under boiling temperature, we can apply vacuum distillation or steam distillation for purification of it.
Distillation is a commonly used method for laboratory purification of organic reagent. Conventional distillation apparatus generally comprises distiller, condenser and receiver, three parts with auxiliary section also containing heater, a thermometer, a wetted tube and cork.
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- Structure:
- Chemical Name:
- DL-ALPHA-(METHYLAMINOMETHYL)BENZYL ALCOHOL
- CAS:
- 6589-55-5
- MF:
- C9H13NO
- Structure:
- Chemical Name:
- CYCLOHEXANO-15-CROWN-5
- CAS:
- 17454-48-7
- MF:
- C14H26O5
- Structure:
- Chemical Name:
- VALEROPHENONE TOSYLHYDRAZONE MIXTURE O&
- CAS:
- 69015-74-3
- MF:
- C18H22N2O2S
- Structure:
- Chemical Name:
- 2-(MORPHOLINE-4-CARBONYL)-BENZOIC ACID
- CAS:
- 73728-40-2
- MF:
- C12H13NO4
- Structure:
- Chemical Name:
- ANTHRAQUINONE-2,6-DISULFONIC ACID, DISODIUM SALT, MIXTURE OF ISOMERS, TECH., 90
- CAS:
- 84-50-4
- MF:
- C14H8O8S2
- Structure:
- Chemical Name:
- 2,4-DICHLOROBENZYL MERCAPTAN
- CAS:
- 65909-82-2
- MF:
- C7H6Cl2S
- Structure:
- Chemical Name:
- 2-BROMO-3-PYRIDYL TRIFLUOROMETHANESULFO&
- CAS:
- 157373-97-2
- MF:
- C6H3BrF3NO3S
- Structure:
- Chemical Name:
- 1-HEXYL-2,3-DIMETHYLIMIDAZOLIUM TETRAFLUOROBORATE
- CAS:
- 384347-21-1
- MF:
- C11H21N2.BF4
- Structure:
- Chemical Name:
- (3-NITROBENZYL)MERCAPTAN 97
- CAS:
- 77472-39-0
- MF:
- O2NC6H4CH2SH
- Structure:
- Chemical Name:
- (S)-1-Phenylethylhydroxylamine
- CAS:
- 53933-47-4
- MF:
- C8H11NO
- Structure:
- Chemical Name:
- BENZYLTRIMETHYLAMMONIUM METHOXIDE
- CAS:
- 122-08-7
- MF:
- C11H19NO
- Structure:
- Chemical Name:
- 1-IODOUNDECANE
- CAS:
- 4282-44-4
- MF:
- C11H23I
- Structure:
- Chemical Name:
- 4-BENZYLOXY-3-METHOXYBENZYL ALCOHOL
- CAS:
- 33693-48-0
- MF:
- C15H16O3
- Structure:
- Chemical Name:
- TRIHEXYL(TETRADECYL)PHOSPHONIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE
- CAS:
- 460092-03-9
- MF:
- C34H68F6NO4PS2
- Structure:
- Chemical Name:
- 4-HYDROXY-3-NITROCOUMARIN
- CAS:
- 20261-31-8
- MF:
- C9H5NO5
- Structure:
- Chemical Name:
- (4-CYANOBENZYL)TRIPHENYLPHOSPHONIUM CHLORIDE
- CAS:
- 20430-33-5
- MF:
- C26H21ClNP
- Structure:
- Chemical Name:
- DIPHENYL SELENIDE
- CAS:
- 1132-39-4
- MF:
- C12H10Se
- Structure:
- Chemical Name:
- METHYL 4-METHYL-4-NITROPENTANOATE
- CAS:
- 16507-02-1
- MF:
- C7H13NO4
- Structure:
- Chemical Name:
- 2-DIETHYLAMINOETHANETHIOL HYDROCHLORIDE
- CAS:
- 1942-52-5
- MF:
- C6H16ClNS
- Structure:
- Chemical Name:
- 5-(4-CHLOROPHENYL)-1-METHYL-1H-IMIDAZOLE-2-THIOL
- CAS:
- 17452-31-2
- MF:
- C10H9ClN2S
- Structure:
- Chemical Name:
- DODECANE
- CAS:
- 93685-81-5
- MF:
- C12H26
- Structure:
- Chemical Name:
- METHYLTRIPHENOXYPHOSPHONIUM IODIDE
- CAS:
- 17579-99-6
- MF:
- C19H18IO3P
- Structure:
- Chemical Name:
- 4-ETHOXY-3-METHOXYBENZYL ALCOHOL
- CAS:
- 61813-58-9
- MF:
- C10H14O3
- Structure:
- Chemical Name:
- 3,5-DIMETHOXYPHENYL ISOTHIOCYANATE
- CAS:
- 104968-58-3
- MF:
- C9H9NO2S
- Structure:
- Chemical Name:
- Neodecanoic acid
- CAS:
- 26896-20-8
- MF:
- C10H20O2
- Structure:
- Chemical Name:
- 7-METHOXY-3,7-DIMETHYLOCTANAL
- CAS:
- 3613-30-7
- MF:
- C11H22O2
- Structure:
- Chemical Name:
- (-)-1,2-BIS((2R,5R)-2,5-DIETHYLPHOSPHOLANO)BENZENE
- CAS:
- 136705-64-1
- MF:
- C22H36P2
- Structure:
- Chemical Name:
- METHYL 4-NITROBUTYRATE
- CAS:
- 13013-02-0
- MF:
- C5H9NO4
- Structure:
- Chemical Name:
- 5-(phenylazo)salicylic acid
- CAS:
- 3147-53-3
- MF:
- C13H10N2O3
- Structure:
- Chemical Name:
- 7-Hydroxyisoflavone
- CAS:
- 13057-72-2
- MF:
- C15H10O3
- Chemical Name:
- 2-hydroxypropyl-α-cyclodextrin
- CAS:
- 128446-33-3
- Structure:
- Chemical Name:
- O-(2-AMINOETHYL)-O-(2-AZIDOETHYL)HEPTAETHYLENE GLYCOL
- CAS:
- 857891-82-8
- MF:
- C18H38N4O8
- Structure:
- Chemical Name:
- ETHYL FORMIMIDATE HYDROCHLORIDE
- CAS:
- 16694-46-5
- MF:
- C3H8ClNO
- Structure:
- Chemical Name:
- Montelukast Sulfoxide (Mixture of diastereomers)
- CAS:
- 909849-96-3
- MF:
- C35H36ClNO4S
- Structure:
- Chemical Name:
- 2-(4-CHLOROPHENYL)-THIOACETAMIDE
- CAS:
- 17518-48-8
- MF:
- C8H8ClNS
- Structure:
- Chemical Name:
- (CARBOETHOXYMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDE HYDRATE
- CAS:
- 17577-28-5
- MF:
- C22H22O2P.Cl
- Structure:
- Chemical Name:
- 3-PYRIDIN-3-YL-PROPIONAMIDINE
- CAS:
- 887578-73-6
- MF:
- C8H11N3
- Structure:
- Chemical Name:
- (S)-(-)-LACTAMIDE
- CAS:
- 89673-71-2
- MF:
- C3H7NO2
- Structure:
- Chemical Name:
- 5-M-TOLYLAMINO-[1,3,4]THIADIAZOLE-2-THIOL
- CAS:
- 52494-32-3
- MF:
- C9H9N3S2
- Structure:
- Chemical Name:
- CYCLOPENTYL-METHYL-AMINE
- CAS:
- 2439-56-7
- MF:
- C6H13N
- Structure:
- Chemical Name:
- 1-BROMO-2,2-DIMETHOXYPROPANE
- CAS:
- 126-38-5
- MF:
- C5H11BrO2
- Structure:
- Chemical Name:
- 2,2,6-TRIMETHYLCYCLOHEXANONE
- CAS:
- 2408-37-9
- MF:
- C9H16O
- Structure:
- Chemical Name:
- 2,3-DIMETHYL-2-BUTANOL
- CAS:
- 594-60-5
- MF:
- C6H14O
- Structure:
- Chemical Name:
- (R)-(-)-CITRAMALIC ACID
- CAS:
- 6236-10-8
- MF:
- C5H8O5
- Structure:
- Chemical Name:
- 3-NITROFLUORANTHENE
- CAS:
- 892-21-7
- MF:
- C16H9NO2
- Structure:
- Chemical Name:
- 2,3-DIMETHYLSUCCINIC ACID
- CAS:
- 13545-04-5
- MF:
- C6H10O4
- Structure:
- Chemical Name:
- TRANS-1,4-CYCLOHEXANE DIISOCYANATE
- CAS:
- 7517-76-2
- MF:
- C8H10N2O2
- Structure:
- Chemical Name:
- Pyrazin-2-yl-boronic acid
- CAS:
- 762263-64-9
- MF:
- C4H5BN2O2
- Structure:
- Chemical Name:
- 3,3-Diphenyltetrahydrofuran-2-ylidene(dimethyl)ammonium bromide
- CAS:
- 37743-18-3
- MF:
- C18H20NO.Br
- Structure:
- Chemical Name:
- ETHYL CIS-2-AMINO-1-CYCLOHEXANECARBOXYLATE HYDROCHLORIDE
- CAS:
- 1127-99-7
- MF:
- C9H18ClNO2
- Structure:
- Chemical Name:
- 2,3,3,3-TETRAFLUOROPROPANOIC ACID
- CAS:
- 359-49-9
- MF:
- C3H2F4O2
- Structure:
- Chemical Name:
- TRUXENE
- CAS:
- 548-35-6
- MF:
- C27H18
- Structure:
- Chemical Name:
- SODIUM 4-(T-BUTYLCARBONYLOXY)-BENZENSULFONATE
- CAS:
- 188114-91-2
- MF:
- C11H13NaO5S
- Structure:
- Chemical Name:
- QUINOLIN-7-YLBORONIC ACID
- CAS:
- 629644-82-2
- MF:
- C9H8BNO2
- Structure:
- Chemical Name:
- TETRAHEXYLAMMONIUM BENZOATE
- CAS:
- 16436-29-6
- MF:
- C31H57NO2
- Structure:
- Chemical Name:
- 2-(2,4-DIFLUORO-PHENYL)-ACETAMIDINE
- CAS:
- 723730-74-3
- MF:
- C8H8F2N2
- Structure:
- Chemical Name:
- DIAMYLAMMONIUM ACETATE
- MF:
- C12H27NO2
- Structure:
- Chemical Name:
- 4-Ethoxymethylphenylboronic acid
- CAS:
- 279262-31-6
- MF:
- C9H13BO3
- Structure:
- Chemical Name:
- (2,4,6-trimethoxyphenyl)methanethiol
- CAS:
- 212555-23-2
- MF:
- C10H14O3S
- Structure:
- Chemical Name:
- Pyridazine-3-thiol
- CAS:
- 28544-77-6
- MF:
- C4H4N2S
- Structure:
- Chemical Name:
- 2-(4-Methylphenyl)propan-2-ol
- CAS:
- 1197-01-9
- MF:
- C10H14O
- Structure:
- Chemical Name:
- 2-(2-CHLORO-PHENYL)-ACETAMIDINE
- CAS:
- 55154-88-6
- MF:
- C8H9ClN2
- Structure:
- Chemical Name:
- 5-broMobenzofuran-2-carboxaMide
- CAS:
- 35351-21-4
- MF:
- C9H6BrNO2
- Structure:
- Chemical Name:
- ETHYL 3-CHLOROPHENYLACETATE
- CAS:
- 14062-29-4
- MF:
- C10H11ClO2
- Structure:
- Chemical Name:
- GLYOXYLIC ACID ETHYL ESTER DIETHYL MERCAPTAL
- CAS:
- 20461-95-4
- MF:
- C8H16O2S2
- Structure:
- Chemical Name:
- 3-(HEPTAFLUOROISOPROPOXY)PROPYLTRIMETHOXYSILANE
- CAS:
- 19116-61-1
- MF:
- C9H15F7O4Si
- Structure:
- Chemical Name:
- 2-PHENYLMALONAMIDE
- CAS:
- 10255-95-5
- MF:
- C9H10N2O2
- Structure:
- Chemical Name:
- (+)-B-METHOXYDIISOPINOCAMPHEYLBORANE
- CAS:
- 85134-98-1
- MF:
- C21H37BO
- Structure:
- Chemical Name:
- 4-METHOXYBENZAMIDINE, HYDROCHLORIDE
- CAS:
- 51721-68-7
- MF:
- C8H11ClN2O
- Structure:
- Chemical Name:
- 3,5-BIS(TERT-BUTYLDIPHENYLSILYLOXY)BENZOIC ACID METHYL ESTER
- CAS:
- 182250-68-6
- MF:
- C40H44O4Si2
- Structure:
- Chemical Name:
- (R)-(-)-1-[(S)-2-(DI(3,5-BIS-TRIFLUOROMETHYLPHENYL)PHOSPHINO)FERROCENYL]ETHYLDI(3,5-DIMETHYLPHENYL)PHOSPHINE
- CAS:
- 166172-63-0
- MF:
- C44H36F12FeP210*
- Structure:
- Chemical Name:
- 8-HYDROXYQUINOLINE-5-SULFONIC ACID MONOHYDRATE
- CAS:
- 283158-18-9
- MF:
- C9H9NO5S
- Structure:
- Chemical Name:
- DIBUTYLAMMONIUM ACETATE
- CAS:
- 19070-91-8
- MF:
- C10H23NO2
- Structure:
- Chemical Name:
- 2-Benzylpropionic acid
- CAS:
- 1009-67-2
- MF:
- C10H12O2
- Structure:
- Chemical Name:
- Coumarin 2
- CAS:
- 26078-25-1
- MF:
- C13H15NO2
- Structure:
- Chemical Name:
- INDOLE-7-BORONIC ACID
- CAS:
- 210889-31-9
- MF:
- C8H8BNO2
- Structure:
- Chemical Name:
- Octyl(phenyl)-N,N-diisobutylcarbamoylmethylphosphine oxide
- CAS:
- 83242-95-9
- MF:
- C24H42NO2P
- Structure:
- Chemical Name:
- HEXAFLUOROACETONE SESQUIHYDRATE
- CAS:
- 13098-39-0
- MF:
- C3H2F6O2
- Structure:
- Chemical Name:
- Propyl bromoacetate
- CAS:
- 35223-80-4
- MF:
- C5H9BrO2
- Structure:
- Chemical Name:
- O-BROMOPHENOXYACETIC ACID
- CAS:
- 1879-56-7
- MF:
- C8H7BrO3
- Structure:
- Chemical Name:
- 2,3,4-TRIFLUOROPHENYL ISOTHIOCYANATE
- CAS:
- 119474-40-7
- MF:
- C7H2F3NS
- Structure:
- Chemical Name:
- 5-METHYL-2-NITROANISOLE
- CAS:
- 38512-82-2
- MF:
- C8H9NO3
- Structure:
- Chemical Name:
- N-HYDROXYNAPHTHALIMIDE SODIUM SALT
- CAS:
- 6207-89-2
- MF:
- C12H6NNaO3
- Structure:
- Chemical Name:
- N-METHOXYCARBONYLMALEIMIDE
- CAS:
- 55750-48-6
- MF:
- C6H5NO4
- Structure:
- Chemical Name:
- 4-PYRIDIN-3-YL-BUTYRAMIDINE
- CAS:
- 887578-93-0
- MF:
- C9H13N3
- Structure:
- Chemical Name:
- HEPTADECAFLUOROOCTANESULFONIC ACID TETRABUTYLAMMONIUM SALT
- CAS:
- 111873-33-7
- MF:
- C24H36F17NO3S
- Structure:
- Chemical Name:
- METHYL ALPHA-CHLOROACRYLATE
- CAS:
- 80-63-7
- MF:
- C4H5ClO2
- Structure:
- Chemical Name:
- Sodium 3-chloro-2-hydroxypropanesulphonate hemihydrate
- CAS:
- 143218-48-8
- MF:
- C3H8ClNaO5S
- Structure:
- Chemical Name:
- 2-HYDROXYETHYL BENZYL SULFIDE
- CAS:
- 3878-41-9
- MF:
- C9H12OS
- Structure:
- Chemical Name:
- PINONIC ACID
- CAS:
- 61826-55-9
- MF:
- C10H16O3
- Structure:
- Chemical Name:
- 1,2-DIAMINOANTHRAQUINONE
- CAS:
- 1758-68-5
- MF:
- C14H10N2O2
- Structure:
- Chemical Name:
- 3-METHYL-1-BUTANETHIOL
- CAS:
- 16630-56-1
- MF:
- C5H12OS
- Structure:
- Chemical Name:
- CYCLOHEXANONE 2,4-DINITROPHENYLHYDRAZONE
- CAS:
- 1589-62-4
- MF:
- C12H14N4O4
- Structure:
- Chemical Name:
- 2,4,6-TRIMETHYL DIPHENYL SULFIDE
- CAS:
- 33667-80-0
- MF:
- C15H16S
- Structure:
- Chemical Name:
- ACETONE AZINE
- CAS:
- 627-70-3
- MF:
- C6H12N2
- Structure:
- Chemical Name:
- (R)-1,2-DECANEDIOL
- CAS:
- 87827-60-9
- MF:
- C10H22O2
- Structure:
- Chemical Name:
- (ALPHAR,ALPHAR)-1,1'-BIS[ALPHA-(DIMETHYLAMINO)BENZYL]-(S,S)-,2'-BIS[BIS[3,5-BIS(TRIFLUOROMETHYL)PHENYL]PHOSPHINO]FERROCENE
- CAS:
- 494227-36-0
- MF:
- C60H42F24FeN2P210*
- Structure:
- Chemical Name:
- 1-(PYRROLIDINE-2-CARBONYL)-PIPERIDINE-4-CARBOXYLIC ACID AMIDE
- MF:
- C11H19N3O2
- Structure:
- Chemical Name:
- 2-AMINO-4-(ETHYLSULFONYL)PHENOL
- CAS:
- 43115-40-8
- MF:
- C8H11NO3S
- Structure:
- Chemical Name:
- TETRAHYDROPYRAN-4-BORONIC ACID
- CAS:
- 1072952-46-5
- MF:
- C5H11BO3